CN104774118A - Liquid fertilizer mulching film for corn capable of enhancing nitrogen and carbon resources in soil and preparation method thereof - Google Patents

Liquid fertilizer mulching film for corn capable of enhancing nitrogen and carbon resources in soil and preparation method thereof Download PDF

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Publication number
CN104774118A
CN104774118A CN201510198055.2A CN201510198055A CN104774118A CN 104774118 A CN104774118 A CN 104774118A CN 201510198055 A CN201510198055 A CN 201510198055A CN 104774118 A CN104774118 A CN 104774118A
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Prior art keywords
soil
parts
liquid fertilizer
coffee
water
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CN201510198055.2A
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Chinese (zh)
Inventor
朱正娟
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Hefei Kangling Curing Technology Co Ltd
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Hefei Kangling Curing Technology Co Ltd
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Priority to CN201510198055.2A priority Critical patent/CN104774118A/en
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Abstract

The invention discloses a liquid fertilizer mulching film for corn capable of enhancing nitrogen and carbon resources in soil, which is prepared from the following raw materials in parts by weight: 13-17 parts of chitosan, 11-15 parts of coffee bean, 45-55 parts of sesame cake, 4-6 parts of composite microbial inoculant, 15-19 parts of modified starch solution, 8-10 parts of glucose, 35-39 parts of grass carbon and a right amount of water. The liquid fertilizer mulching film has the advantages of favorable film-forming property, high stability and obvious water-retaining effect for soil, and can provide carbon, nitrogen and many other resources for soil after being degraded. The added grass carbon, chitosan and the like provide abundant absorbable nutrients for corn. The liquid fertilizer mulching film is a plant growth regulator, and has favorable promotion actions on soil protection and corn yield increase after use.

Description

A kind of corn liquid fertilizer mulch film improving Soil Nitrogen carbon resource and preparation method thereof
Technical field
The present invention relates to a kind of agricultural film technical field, particularly a kind of corn liquid fertilizer mulch film improving Soil Nitrogen carbon resource and preparation method thereof.
Background technology
Mulch film has the effects such as insulation, water conservation, frost protection to crop, the application of ground membrane technique improves and the output and the benefit that add farm crop greatly, but traditional mulch film is a kind of macromolecular compound of synthetic, degradable hardly in its natural state, after using, place to go is not comprehended and is caused very large pollution to edatope, affects crop root growth, and the mulch film of process is because of moist, damaged, also not reusable edible, can only as refuse reclamation, and work consuming is consuming time.
For this reason, the present inventor provides a kind of liquid fertilizer mulch film for corn, not only there is the water-retaining effect performance that common ground film is outstanding, have higher fertilizer simultaneously, material choice mostly is organic matter of easily degrading, simultaneously containing soil probiotics, by spraying the gel-like film formed in soil surface, provide protection is provided to corn planting, the use of collocation fertilizer, the dissolution rate of the nutrients such as Nitrogen, Phosphorus potassium can be improved, thus improve corn to the receptivity of fertilizer, its degraded product then forms the abundant humic acids of fertility, carbonic acid gas and water, not only pollution-free to soil, the physico-chemical property of soil can also be improved, as the substitute of common ground film, there is good application prospect.
Summary of the invention
The present invention compensate for the deficiencies in the prior art, provides a kind of corn liquid fertilizer mulch film improving Soil Nitrogen carbon resource and preparation method thereof.
Technical scheme of the present invention is as follows:
Mulch film of the present invention is made up of the raw material of following weight part: chitosan 13-17, coffee berry 11-15, sesame cake meal 45-55, complex micro organism fungicide 4-6, modified starch solution 15-19, glucose 8-10, peat composed of rotten mosses 35-39, water are appropriate;
Described complex micro organism fungicide is silicate bacteria microbial inoculum, bacillus subtilis microbial agent and photosynthetic bacteria microbial inoculum, and proportion is 2:1:1;
Described modified starch solution is made up of the raw material of following weight part: potato starch 45-55, calcium acetate 2-4, potassium permanganate solution 2-3, vinylformic acid 15-20, sodium hydroxide 3-4, N,N methylene bis acrylamide 0.1-0.3, ferrous sulfate 8-10, zinc sulfate 6-8, manganous sulfate 7-9, its preparation method is dissolved in by potato starch to double in the water of its quality, be heated to 70-90 DEG C of gelatinization 30-60 minute, add potassium permanganate solution oxidation 50-70 minute again, period constantly stirs, vinylformic acid and sodium hydroxide is added again in solution, then N is added, N-methylene-bisacrylamide is cross-linked 20-30 minute, add calcium acetate again and stir, ferrous sulfate is added after reaction system being heated to 50-60 DEG C, chelating 15 minutes also stirs, add zinc sulfate more afterwards, chelating 15 minutes, finally add manganous sulfate, reaction system is warmed up to 60-80 DEG C, chelating 20-30 minute, namely chelating iron is obtained, zinc, the Modified soil bean starch solution of manganese.
The concrete steps of the preparation of described mulch film are as follows:
(1) peat composed of rotten mosses, glucose, sesame cake meal mixing are placed in fermentation vat, in fermentation vat, add suitable quantity of water keep fermentation heap water content to be 55%-60%, take out fermentation materials after fermentation 4-5 week and squeeze, obtaining fermented liquid for subsequent use;
(2) coffee berry is dried at 50-60 DEG C, regrind into fine powder, in coffee fine powder, add a small amount of water, be heated to 80-90 DEG C, stir 10-20 minute, when coffee liquid is cooled to 30 DEG C, silicate bacteria microbial inoculum, bacillus subtilis microbial agent, photosynthetic bacteria microbial inoculum are joined in coffee liquid, after stirring, gained coffee liquid is filtered, filtrate is levigate at 40-50 DEG C of leeward dry doubling with gas blower, be fixed the soluble coffee fine powder of microbiobacterial agent, for subsequent use;
(3) mixed with modified starch solution by step 1 gained fermented liquid and stir, join in stoving oven, at 100-120 DEG C, dry 30-40 minute, cooling crush crosses 200 mesh sieves, for subsequent use;
(4) step 2 gained coffee fine powder, step 3 gained powder, chitosan and leftover materials are mixed, dry at 60-80 DEG C, namely obtain liquid fertilizer mulch film of the present invention after metering packing;
(5) liquid fertilizer mulch film using method of the present invention is that carry out the sprinkling of soil surface with atomizer, every mu of diluent usage quantity is 20-25 kilogram by after pulvis and water in mass ratio 1:9 mixed dissolution.
Beneficial effect of the present invention:
Modified starch solution is medium trace element needed for multiple corn growth as chelating while liquid-state mulch film membrane-forming agent, is more easily absorbed than common fertilizer.
Coffee berry is as edible product, and its powder has outstanding adsorptive power, is carried out immobilized microbiobacterial agent by the adsorptivity of coffee powder and strong solubility and is added in liquid fertilizer mulch film, can produce optimize improving effect significantly to the plantation of corn and soil.
Liquid fertilizer mulch film good film-forming property of the present invention; stability is strong; remarkable to the Water-saving effect of soil; can be soil after degraded simultaneously and the multiple resources such as carbon, nitrogen is provided; the peat composed of rotten mosses, chitosan etc. that add; provide not only a large amount of corn Absorbable rod nutrient, is also simultaneously a plant growth regulators, and using has good promoter action afterwards to the protection of soil, the volume increase of corn.
Specific embodiments
Below in conjunction with following embodiment, the present invention is described in further detail:
The raw material taking following weight (kg) is made: chitosan 15, coffee berry 13, sesame cake meal 50, complex micro organism fungicide 5, modified starch solution 17, glucose 9, the peat composed of rotten mosses 37, water are appropriate;
Described complex micro organism fungicide is silicate bacteria microbial inoculum, bacillus subtilis microbial agent and photosynthetic bacteria microbial inoculum, and proportion is 2:1:1;
Described modified starch solution is made up of the raw material of following weight part: potato starch 50, calcium acetate 3, potassium permanganate solution 2, vinylformic acid 18, sodium hydroxide 3, N,N methylene bis acrylamide 0.1, ferrous sulfate 10, zinc sulfate 7, manganous sulfate 8, its preparation method is dissolved in by potato starch to double in the water of its quality, be heated to 80 DEG C of gelatinizations 40 minutes, add potassium permanganate solution again and be oxidized 60 minutes, period constantly stirs, vinylformic acid and sodium hydroxide is added again in solution, then N is added, crosslinked 20 minutes of N-methylene-bisacrylamide, add calcium acetate again and stir, ferrous sulfate is added after reaction system being heated to 50 DEG C, chelating 15 minutes also stirs, add zinc sulfate more afterwards, chelating 15 minutes, finally add manganous sulfate, reaction system is warmed up to 70 DEG C, chelating 20 minutes, namely chelating iron is obtained, zinc, the Modified soil bean starch solution of manganese.
The concrete steps of the preparation of described mulch film are as follows:
(1) peat composed of rotten mosses, glucose, sesame cake meal mixing are placed in fermentation vat, in fermentation vat, add suitable quantity of water keep fermentation heap water content to be 60%, take out fermentation materials after fermenting 5 weeks and squeeze, obtaining fermented liquid for subsequent use;
(2) coffee berry is dried at 55 DEG C, regrind into fine powder, in coffee fine powder, add a small amount of water, be heated to 85 DEG C, stir 15 minutes, when coffee liquid is cooled to 30 DEG C, silicate bacteria microbial inoculum, bacillus subtilis microbial agent, photosynthetic bacteria microbial inoculum are joined in coffee liquid, after stirring, gained coffee liquid is filtered, filtrate is levigate at 45 DEG C of leeward dry doublings with gas blower, be fixed the soluble coffee fine powder of microbiobacterial agent, for subsequent use;
(3) mixed with modified starch solution by step 1 gained fermented liquid and stir, joining in stoving oven, dry 40 minutes at 100 DEG C, cooling crush crosses 200 mesh sieves, for subsequent use;
(4) step 2 gained coffee fine powder, step 3 gained powder, chitosan and leftover materials are mixed, dry at 70 DEG C, namely obtain liquid fertilizer mulch film of the present invention after metering packing;
(5) liquid fertilizer mulch film using method of the present invention is that carry out the sprinkling of soil surface with atomizer, every mu of diluent usage quantity is 22 kilograms by after pulvis and water in mass ratio 1:9 mixed dissolution.
In order to further illustrate using value of the present invention, contriver have chosen the corn of 10 mu of field plantation same breed, wherein 5 mu spray liquid fertilizer mulch film 20kg of the present invention as experimental group every mu, use commercially available common fertilizer as base manure simultaneously, other 5 mu only use commercially available common fertilizer as base manure as a control group, between planting season, the management mode of two groups is identical, and the mensuration of the soil temperature, soil nutrient content, soil water-retaining situation etc. of different time sections between planting season having been carried out in data, result is as follows:
Project Control group Experimental group
The 8:00 soil moisture (DEG C) 20.01 21.19
The 18:00 soil moisture (DEG C) 25.49 26.91
Soil alkali-hydrolyzable nitrogen content (mg/kg) 44.06 62.52
Soil available phosphorus content (mg/kg) 69.82 107.35
Available potassium in soils content (mg/kg) 266.33 329.28
Soil moisture content (%) after watering 16.8 20.2
Soil moisture content (%) after watering one day 8.7 15.7
Average water retention (%) 51.8 77.7
Corn yield (kg/ mu) 577 625
Plastic-film disintegration situation —— Degradable after 60 days
After can finding out employ liquid fertilizer mulch film of the present invention from above experimental data, soil is all better than the plot being used alone fertilizer in insulation water conservation, soil fertility etc., and finally improves corn yield, is suitable for promoting the use of of corn planting industry.

Claims (2)

1. one kind is improved the corn liquid fertilizer mulch film of Soil Nitrogen carbon resource, it is characterized in that, be made up of the raw material of following weight part: chitosan 13-17, coffee berry 11-15, sesame cake meal 45-55, complex micro organism fungicide 4-6, modified starch solution 15-19, glucose 8-10, peat composed of rotten mosses 35-39, water are appropriate;
Described complex micro organism fungicide is silicate bacteria microbial inoculum, bacillus subtilis microbial agent and photosynthetic bacteria microbial inoculum, and proportion is 2:1:1;
Described modified starch solution is made up of the raw material of following weight part: potato starch 45-55, calcium acetate 2-4, potassium permanganate solution 2-3, vinylformic acid 15-20, sodium hydroxide 3-4, N,N methylene bis acrylamide 0.1-0.3, ferrous sulfate 8-10, zinc sulfate 6-8, manganous sulfate 7-9, its preparation method is dissolved in by potato starch to double in the water of its quality, be heated to 70-90 DEG C of gelatinization 30-60 minute, add potassium permanganate solution oxidation 50-70 minute again, period constantly stirs, vinylformic acid and sodium hydroxide is added again in solution, then N is added, N-methylene-bisacrylamide is cross-linked 20-30 minute, add calcium acetate again and stir, ferrous sulfate is added after reaction system being heated to 50-60 DEG C, chelating 15 minutes also stirs, add zinc sulfate more afterwards, chelating 15 minutes, finally add manganous sulfate, reaction system is warmed up to 60-80 DEG C, chelating 20-30 minute, namely chelating iron is obtained, zinc, the Modified soil bean starch solution of manganese.
2. the corn liquid fertilizer mulch film of the raising Soil Nitrogen carbon resource according to claims 1, it is characterized in that, the concrete steps of preparation method are as follows:
(1) peat composed of rotten mosses, glucose, sesame cake meal mixing are placed in fermentation vat, in fermentation vat, add suitable quantity of water keep fermentation heap water content to be 55%-60%, take out fermentation materials after fermentation 4-5 week and squeeze, obtaining fermented liquid for subsequent use;
(2) coffee berry is dried at 50-60 DEG C, regrind into fine powder, in coffee fine powder, add a small amount of water, be heated to 80-90 DEG C, stir 10-20 minute, when coffee liquid is cooled to 30 DEG C, silicate bacteria microbial inoculum, bacillus subtilis microbial agent, photosynthetic bacteria microbial inoculum are joined in coffee liquid, after stirring, gained coffee liquid is filtered, filtrate is levigate at 40-50 DEG C of leeward dry doubling with gas blower, be fixed the soluble coffee fine powder of microbiobacterial agent, for subsequent use;
(3) mixed with modified starch solution by step 1 gained fermented liquid and stir, join in stoving oven, at 100-120 DEG C, dry 30-40 minute, cooling crush crosses 200 mesh sieves, for subsequent use;
(4) step 2 gained coffee fine powder, step 3 gained powder, chitosan and leftover materials are mixed, dry at 60-80 DEG C, namely obtain liquid fertilizer mulch film of the present invention after metering packing;
(5) liquid fertilizer mulch film using method of the present invention is that carry out the sprinkling of soil surface with atomizer, every mu of diluent usage quantity is 20-25 kilogram by after pulvis and water in mass ratio 1:9 mixed dissolution.
CN201510198055.2A 2015-04-24 2015-04-24 Liquid fertilizer mulching film for corn capable of enhancing nitrogen and carbon resources in soil and preparation method thereof Pending CN104774118A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108503489A (en) * 2018-05-14 2018-09-07 王宁 A kind of compound fertilizer and preparation method thereof

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1559227A (en) * 2004-03-08 2005-01-05 邹红梅 Method for producing yield increaser
CN101007903A (en) * 2007-01-23 2007-08-01 亓欣 All-degradable liquid mulch film
CN101481508A (en) * 2008-01-11 2009-07-15 山东科技大学 Humic acid multifunctional degradable black mulch film
CN101642771A (en) * 2009-09-02 2010-02-10 张培举 Microbial soil restorative and preparation method thereof
CN101935237A (en) * 2009-07-02 2011-01-05 上海绿乐生物科技有限公司 Composite microbial fertilizer using fermented filter cakes as medium and production method thereof
CN104381062A (en) * 2014-11-26 2015-03-04 烟台大学 Agricultural biological mulch forming material and covering method and tool thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1559227A (en) * 2004-03-08 2005-01-05 邹红梅 Method for producing yield increaser
CN101007903A (en) * 2007-01-23 2007-08-01 亓欣 All-degradable liquid mulch film
CN101481508A (en) * 2008-01-11 2009-07-15 山东科技大学 Humic acid multifunctional degradable black mulch film
CN101935237A (en) * 2009-07-02 2011-01-05 上海绿乐生物科技有限公司 Composite microbial fertilizer using fermented filter cakes as medium and production method thereof
CN101642771A (en) * 2009-09-02 2010-02-10 张培举 Microbial soil restorative and preparation method thereof
CN104381062A (en) * 2014-11-26 2015-03-04 烟台大学 Agricultural biological mulch forming material and covering method and tool thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108503489A (en) * 2018-05-14 2018-09-07 王宁 A kind of compound fertilizer and preparation method thereof

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Application publication date: 20150715