CN104770704A - Preparation method of wolfberry health table salt - Google Patents
Preparation method of wolfberry health table salt Download PDFInfo
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- CN104770704A CN104770704A CN201410384503.3A CN201410384503A CN104770704A CN 104770704 A CN104770704 A CN 104770704A CN 201410384503 A CN201410384503 A CN 201410384503A CN 104770704 A CN104770704 A CN 104770704A
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Abstract
The invention discloses a preparation method of wolfberry health table salt. The preparation method comprises the following steps of 1, wolfberry pretreatment, 2, supercritical CO2 extraction: carrying out supercritical CO2 extraction on the wolfberry powder obtained by the step 1 to obtain a wolfberry functional component, and 3, recrystallization: dissolving the wolfberry functional component obtained by the step 2 in a pure aqueous solution at a normal temperature under normal pressure, dissolving common salt in the solution until saturation and carrying out pressure reduction evaporation to obtain the wolfberry health table salt crystals. The preparation method uses wolfberry powder extract in commercial table salt, maximumly utilizes wolfberry health care effects and realizes seasoning and health improvement.
Description
Technical field
The invention belongs to food dressing field, health-care salt relating to vegetable ingredients and preparation method thereof, be in particular a kind of by Chinese wolfberry fruit through certain PROCESS FOR TREATMENT, prepare a kind of preparation method realizing the edible salt of health-care effect while ensureing seasoning.
Background technology
As the saying goes: " salt-free do not go out taste ", salt is requisite during people live since today from ancient, to one of most important material of human survival, also be the most frequently used flavoring in culinary art, suitably put in dish and order salt, not only seasoning but also favourable health, but traditional salt only has seasoning effect usually, function ratio is more single, and sodium content is higher, takes in and too much easily causes human body to occur the chronic diseases such as hypertension, oedema, coronary heart disease, angiocardiopathy.Therefore, while the seasoning of guarantee salt, the study hotspot that its health-care efficacy has become food dressing field is increased.Green tea powder is added in commercial salt and prepares health-care salt by existing patent report at present, but this health-care salt also exists the defect of mouthfeel difference, and the health care effectiveness of green tea powder is not obvious.
The fruit of Chinese wolfberry is the fruit of matrimony vine of solanaceae plant drying and ripening; matrimony vine is as a kind of food; can not be treated and directly eat; containing abundant LBP-X, fat, protein, free amino acid, taurine, betaine, vitamin B1, vitamin B2, vitamin E, vitamin C in it, particularly carotenoid content is very high.Simultaneously, the trace minerals such as potassium, sodium, calcium, magnesium, iron, copper, manganese, zinc, selenium are also rich in the fruit of Chinese wolfberry, therefore, matrimony vine there is good Promote immunity, reduce blood sugar, anti-oxidant, delay senility, promote the effect such as apoptosis of tumor cells, Antiradiation injury, reducing blood lipid.
According to the inventors knowledge, there is no report at present and matrimony vine is added in salt, or prepare Patents and the document of mouthfeel and all excellent vegetalitas edible salt of health-care effect.
Summary of the invention
The object of the invention is, in order to provide a kind of Wolfberry fruit health salt and preparation method thereof, the extract of fruit of Chinese wolfberry powder to be added in commercial salt.
The present invention solves the problems of the technologies described above adopted technical scheme:
A preparation method for Chinese wolfberry health-care salt, comprises the steps:
1) matrimony vine pretreatment: matrimony vine is dried 4 ~ 6hr at 60 ~ 100 DEG C, controlling water content is 5 ~ 10%, and stoning, is crushed to 60 ~ 100 orders, 75 ~ 100 DEG C of hot-water soak 30min ~ 3hr; Filter, washing, dry, obtain total sugar content and be less than 10%, the wolfberry fruit powder that water content is less than 10%;
2) supercritical CO
2extraction: by step 1) described in wolfberry fruit powder pass through supercritical CO
2extraction obtains the functional component of matrimony vine, comprises following extraction step:
A, pressure are 25 ~ 35MPa, temperature 25 ~ 40 DEG C, time 30 ~ 60min, remove residues of pesticides;
B, pressure are 25 ~ 35MPa, temperature 30 ~ 33 DEG C, time 30min ~ 6hr, obtain cAMP, colors;
C, pressure are 30 ~ 35MPa, temperature 30 ~ 37 DEG C, time 2 ~ 5hr, obtain vitamin and triterpenic acid;
D, pressure are 33 ~ 35MPa, temperature 35 ~ 45 DEG C, time 2 ~ 5hr, obtain protein;
3) be recrystallized: under normal temperature and pressure, by step 2) being dissolved in pure water solution of the matrimony vine function component of described B, C, D, then adding sodium chloride and dissolve until saturated, is then 0.5x10 at pressure
5pa ~ 1x10
5pa, temperature is 4 ~ 35 DEG C, and namely reduction vaporization obtains Chinese wolfberry health-care salt crystal.
Preferably, in order to ensure that obtained Chinese wolfberry health-care salt has less impurity, Chinese wolfberry health-care salt is better prepared; The purity of described sodium chloride is 98% ~ 99.94%, and particle diameter is 0.1 ~ 0.85mm, whiteness 55% ~ 95% microcrystal grain.
Preferably, in order to the matrimony vine function component content that obtains and purity higher, described supercritical CO
2cO is used in extraction
2it is the high-purity CO of 99.90% ~ 99.99%
2, all the other components are the inert gas not participating in reaction.
The nucleus of the Chinese wolfberry health-care salt crystal prepared is the functional component of matrimony vine, and the nucleus of described Chinese wolfberry health-care salt crystal is the functional component of matrimony vine, the hexahedron structure of crystal particle diameter 0.15 ~ 0.65mm; Described Chinese wolfberry health-care salt crystal, after every bag of 1000g ± 5g package encapsulation, stackedly put 30 days, its crystal particle diameter is between 0.12 ~ 0.75mm.
The invention has the beneficial effects as follows:
1, this invention proposes the health-care components fruit of Chinese wolfberry to be added in articles for daily use salt first, has filled up this field in a way blank.
2, by adding health-care components-fruit of Chinese wolfberry in daily flavouring salt, avoid taking in separately mouthfeel that the fruit of Chinese wolfberry produces single and be difficult to ensure persistent drawback, in the long run, the edible health care of this health-care salt to human body more has continuation.
3, wolfberry fruit nutritious abundant; be rich in the Organic nutrient such as LBP-X, free amino acid, taurine, protein, vitamin, carotenoid; be rich in the various trace elements such as calcium, magnesium, zinc, iron, potassium simultaneously; continue the edible prevention and the treatment that are particularly conducive to health and relevant disease; thus meet people and more and more focus on the reasonably combined demand of nutrition, reduce the risk that Excess free enthalpy sodium salt causes the disease such as hypertension, coronary heart disease.
4, distribute in matrimony vine the widest flavonoid compound, has cough-relieving, flat rapid, the effect of eliminating the phlegm, and can coronary artery dilator and reduce cholesterolemia, has to strengthen heart contraction, reduce heartbeat number and the significantly effect such as anti-oxidant.Contain the abundant antioxidant content such as vitamin C, vitamin E, carotenoid, polyunsaturated fatty acid, polysaccharide in the fruit of Chinese wolfberry simultaneously, there is stronger oxidation resistance and the ability of scavenging free radicals, therefore this health-care salt edible also has anti-senescence function for a long time, improves the effect of body immunity.
5, too much eat as the acid foods such as meat, poultry, fish, dairy products are easy to cause acidic constitution, and containing more as the alkaline matter such as vegetable soda, betaine in the fruit of Chinese wolfberry, therefore, with unnecessary acidic materials in body during long-term this health-care salt edible contributes to, to maintain the acid-base balance of human body, be conducive to the permanent health of consumer.
6, the distinctive delicate flavour of the fruit of Chinese wolfberry, the food that can be culinary art is carried fresh.
The invention has the beneficial effects as follows the preparation method providing a kind of Wolfberry fruit health salt, the extract of fruit of Chinese wolfberry powder is added in commercial salt, farthest can play the health-care effect of the fruit of Chinese wolfberry, make people while use salt reaches seasoning object, facilitate the health of self.
Detailed description of the invention
Following examples are used for the present invention is described, but are not used for limiting the scope of the invention.
The preparation of embodiment 1, a kind of Chinese wolfberry health-care salt
A preparation method for Chinese wolfberry health-care salt, comprises the steps:
1) matrimony vine pretreatment: matrimony vine is dried 4hr at 100 DEG C, controlling water content is 5%, and stoning, is crushed to 60 orders, 75 DEG C of hot-water soak 3hr; Filter, washing, dry, obtain total sugar content and be less than 8%, the wolfberry fruit powder that water content is less than 5%;
2) supercritical CO
2extraction: by step 1) described in wolfberry fruit powder pass through supercritical CO
2extraction obtains the functional component of matrimony vine, comprises following extraction step:
A, pressure are 25MPa, temperature 40 DEG C, time 60min, remove residues of pesticides;
B, pressure are 25MPa, temperature 33 DEG C, time 3hr, obtain cAMP, colors;
C, pressure are 30MPa, temperature 37 DEG C, time 3hr, obtain vitamin and triterpenic acid;
D, pressure are 33MPa, temperature 45 C, time 3hr, obtain protein;
3) be recrystallized: under normal temperature and pressure, by step 2) being dissolved in pure water solution of the matrimony vine function component of described B, C, D, then adding sodium chloride and dissolve until saturated, is then 0.5x10 at pressure
5pa, temperature is 10 DEG C, and namely reduction vaporization obtains Chinese wolfberry health-care salt crystal.
The purity of described sodium chloride is 98% ~ 99.94%, and particle diameter is 0.1 ~ 0.85mm, whiteness 55% ~ 95% microcrystal grain.
Described supercritical CO
2cO is used in extraction
2it is the high-purity CO of 99.90% ~ 99.99%
2, all the other components are the inert gas not participating in reaction.
The nucleus of described Chinese wolfberry health-care salt crystal is the functional component of matrimony vine, the hexahedron structure of crystal particle diameter 0.15 ~ 0.65mm; Described Chinese wolfberry health-care salt crystal, after every bag of 1000g ± 5g package encapsulation, stackedly put 30 days, its crystal particle diameter is between 0.12 ~ 0.75mm.
The preparation of embodiment 2, a kind of Chinese wolfberry health-care salt
A preparation method for Chinese wolfberry health-care salt, comprises the steps:
1) matrimony vine pretreatment: matrimony vine is dried 6hr at 60 DEG C, controlling water content is 10%, and stoning, is crushed to 100 orders, 100 DEG C of hot-water soak 3hr; Filter, washing, dry, obtain total sugar content and be less than 5%, the wolfberry fruit powder that water content is less than 5%;
2) supercritical CO
2extraction: by step 1) described in wolfberry fruit powder pass through supercritical CO
2extraction obtains the functional component of matrimony vine, comprises following extraction step:
A, pressure are 25MPa, temperature 25 DEG C, time 60min, remove residues of pesticides;
B, pressure are 35MPa, temperature 30 DEG C, time 6hr, obtain cAMP, colors;
C, pressure are 35MPa, temperature 30 DEG C, time 5hr, obtain vitamin and triterpenic acid;
D, pressure are 35MPa, temperature 35 DEG C, time 5hr, obtain protein;
3) be recrystallized: under normal temperature and pressure, by step 2) being dissolved in pure water solution of the matrimony vine function component of described B, C, D, then adding sodium chloride and dissolve until saturated, is then 1x10 at pressure
5pa, temperature is 30 DEG C, and namely reduction vaporization obtains Chinese wolfberry health-care salt crystal.
Claims (5)
1. a preparation method for Chinese wolfberry health-care salt, comprises the steps:
1) matrimony vine pretreatment: matrimony vine is dried 4 ~ 6hr at 60 ~ 100 DEG C, controlling water content is 5 ~ 10%, and stoning, is crushed to 60 ~ 100 orders, 75 ~ 100 DEG C of hot-water soak 30min ~ 3hr; Filter, washing, dry, obtain total sugar content and be less than 10%, the wolfberry fruit powder that water content is less than 10%;
2) supercritical CO
2extraction: by step 1) described in wolfberry fruit powder pass through supercritical CO
2extraction obtains the functional component of matrimony vine, comprises following extraction step:
A, pressure are 25 ~ 35MPa, temperature 25 ~ 40 DEG C, time 30 ~ 60min, remove residues of pesticides;
B, pressure are 25 ~ 35MPa, temperature 30 ~ 33 DEG C, time 30min ~ 6hr, obtain cAMP, colors;
C, pressure are 30 ~ 35MPa, temperature 30 ~ 37 DEG C, time 2 ~ 5hr, obtain vitamin and triterpenic acid;
D, pressure are 33 ~ 35MPa, temperature 35 ~ 45 DEG C, time 2 ~ 5hr, obtain protein;
3) be recrystallized: under normal temperature and pressure, by step 2) being dissolved in pure water solution of the matrimony vine function component of described B, C, D, then adding sodium chloride and dissolve until saturated, is then 0.5x10 at pressure
5pa ~ 1x10
5pa, temperature is 4 ~ 35 DEG C, and namely reduction vaporization obtains Chinese wolfberry health-care salt crystal.
2. the preparation method of Chinese wolfberry health-care salt as claimed in claim 1, is characterized in that: the purity of described sodium chloride is 98% ~ 99.94%, and particle diameter is 0.1 ~ 0.85mm, whiteness 55% ~ 95% microcrystal grain.
3. the preparation method of Chinese wolfberry health-care salt as claimed in claim 1, is characterized in that: described supercritical CO
2cO is used in extraction
2it is the high-purity CO of 99.90% ~ 99.99%
2, all the other components are the inert gas not participating in reaction.
4. the preparation method of Chinese wolfberry health-care salt as claimed in claim 1, is characterized in that: the nucleus of described Chinese wolfberry health-care salt crystal is the functional component of matrimony vine, the hexahedron structure of crystal particle diameter 0.15 ~ 0.65mm; Described Chinese wolfberry health-care salt crystal, after every bag of 1000g ± 5g package encapsulation, stackedly put 30 days, its crystal particle diameter is between 0.12 ~ 0.75mm.
5. a Chinese wolfberry health-care salt, the preparation method of the Chinese wolfberry health-care salt as described in as arbitrary in Claims 1 to 4 obtains.
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105639589A (en) * | 2016-03-29 | 2016-06-08 | 天津保元堂生物科技有限公司 | Fagopyrum tararicum low-sodium salt |
CN106666639A (en) * | 2016-12-29 | 2017-05-17 | 天津保元堂生物科技有限公司 | Chrysanthemum medicated food composition and preparation method thereof |
CN106805192A (en) * | 2017-01-16 | 2017-06-09 | 中盐新干盐化有限公司 | A kind of matrimony vine salt |
Citations (4)
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CN1233412A (en) * | 1998-04-28 | 1999-11-03 | 徐传祥 | Multi-function compound seasoning salt |
CN101331938A (en) * | 2008-07-23 | 2008-12-31 | 黄涛 | Natural green tea health edible salt |
CN102960706A (en) * | 2012-12-14 | 2013-03-13 | 四川久大品种盐有限责任公司 | Re-crystallization preparation method of bamboo salt |
CN103202455A (en) * | 2013-03-25 | 2013-07-17 | 河南省盐业总公司 | Jujube salt preparation method |
-
2014
- 2014-08-06 CN CN201410384503.3A patent/CN104770704A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1233412A (en) * | 1998-04-28 | 1999-11-03 | 徐传祥 | Multi-function compound seasoning salt |
CN101331938A (en) * | 2008-07-23 | 2008-12-31 | 黄涛 | Natural green tea health edible salt |
CN102960706A (en) * | 2012-12-14 | 2013-03-13 | 四川久大品种盐有限责任公司 | Re-crystallization preparation method of bamboo salt |
CN103202455A (en) * | 2013-03-25 | 2013-07-17 | 河南省盐业总公司 | Jujube salt preparation method |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105639589A (en) * | 2016-03-29 | 2016-06-08 | 天津保元堂生物科技有限公司 | Fagopyrum tararicum low-sodium salt |
CN106666639A (en) * | 2016-12-29 | 2017-05-17 | 天津保元堂生物科技有限公司 | Chrysanthemum medicated food composition and preparation method thereof |
CN106805192A (en) * | 2017-01-16 | 2017-06-09 | 中盐新干盐化有限公司 | A kind of matrimony vine salt |
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Application publication date: 20150715 |