CN104739703A - Moisturizing facial cleanser and preparation method thereof - Google Patents

Moisturizing facial cleanser and preparation method thereof Download PDF

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Publication number
CN104739703A
CN104739703A CN201310735321.1A CN201310735321A CN104739703A CN 104739703 A CN104739703 A CN 104739703A CN 201310735321 A CN201310735321 A CN 201310735321A CN 104739703 A CN104739703 A CN 104739703A
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China
Prior art keywords
pot
oil
minutes
stearate
deionized water
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CN201310735321.1A
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Chinese (zh)
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陈冬英
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DALIAN MEILE BIOLOGICAL TECHNOLOGY DEVELOPMENT Co Ltd
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DALIAN MEILE BIOLOGICAL TECHNOLOGY DEVELOPMENT Co Ltd
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Priority to CN201310735321.1A priority Critical patent/CN104739703A/en
Publication of CN104739703A publication Critical patent/CN104739703A/en
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Abstract

A moisturizing facial cleanser comprises stearic acid, cetyl-stearyl mixed alcohol and methylisothiazolinone. A preparation method of the moisturizing facial cleanser comprises the following steps: 1, adding stearic acid, cetyl-stearyl mixed alcohol, monoglyceride, caprylic/capric triglyceride, 2,6-di-tert-butyl-methylphenol, jojoba oil, silicone oil 350, polyethylene glycol 100 stearate, glucoside stearate, polyoxyethylene ether glucoside stearate and avocado oil into an oil pot; 2, adding deionized water B into a water pot, and adding glycerin, betaine, 16-alkylglucoside, allantoin and a Sapindus mukurossi extract product into the water pot; 3, adding papain into deionized water A; 4, heating an emulsifying pot; 5, pumping the material in the oil pot into the emulsifying pot; 6, pumping the material in the water pot into the emulsifying pot; 7, cooling; 8, adding a mixture obtained in step 3 into the emulsifying pot, adding a Hamamelis mollis extract liquid, lavender oil, NaOH (a 10% solution) and methylisothiazolinone; 9, sampling; 10, discharging; and 11, packaging. The moisturizing facial cleanser can effectively clean face, guarantees maintenance of moisture of skins, enhances the oxidation and allergy resistance of skins, and can minimize pores.

Description

A kind of moisturizing cleansing milk and preparation method thereof
technical fieldthe present invention relates to technical field of skin care, particularly a kind of cleansing milk and preparation method thereof.
background technologythe wetting agent that existing cleansing milk is mainly synthesized by more single surfactant compound is in the market made, thus reaches the object of decontamination.Owing to employing a large amount of surfactants, easily cause the undue defat of epiderm skin, thus make skin drier, more serious meeting causes damaging the irreversibility of skin, and function singleness, the demand of user to the multiple efficacies of skin care cannot be met.Its weak point: skin is drier, does not have effect of moisturizing and convergence pore.
summary of the inventionthe object of this invention is to provide a kind of effectively clean face, ensure that skin keeps moistening and a kind of moisturizing cleansing milk can restraining pore and preparation method thereof.
Technical scheme of the present invention is: a kind of moisturizing cleansing milk, its composition mainly comprises acid of destearinizing, 16-18 mixed alcohol, monoglyceride, caprylic capric triglyceride, 2, 6-di-tert-butyl-4-methy phenol, Jojoba oil, silicone oil 350, Polyethylene Glycol 100 stearate, glucoside stearate, polyoxyethylene ether glucoside stearate, American Avocado Tree oil, glycerol, betanin, 16-alkyl polyglucoside, allantoin, Radix Hamamelidis Mollis extracting solution, soapberry extract, papain, deionized water A, Oleum lavandula angustifolia, NaOH(10% solution), deionized water B and Methylisothiazolinone.Wherein, be 1 ultimate unit with deionized water B, deionized water B and acid of destearinizing, 16-18 mixed alcohol, monoglyceride, caprylic capric triglyceride, 2,6-di-tert-butyl-4-methy phenol, Jojoba oil, silicone oil 350, Polyethylene Glycol 100 stearate, glucoside stearate, polyoxyethylene ether glucoside stearate, American Avocado Tree oil, glycerol, betanin, 16-alkyl polyglucoside, allantoin, Radix Hamamelidis Mollis extracting solution, soapberry extract, papain, deionized water A, Oleum lavandula angustifolia, NaOH(10% solution) and the mass ratio of Methylisothiazolinone be 1:0.06209 ~ 0.10922, 1:0.03504 ~ 0.04283,1:0.02803 ~ 0.03426,1:0.03504 ~ 0.04283,1:0.00070 ~ 0.00086,1:0.04884 ~ 0.09132,1:0.02102 ~ 0.02570,1:0.00701 ~ 0.00857,1:0.01402 ~ 0.01713,1:0.02102 ~ 0.02570,1:0.02803 ~ 0.03426,1:0.05508 ~ 0.10066,1:0.02102 ~ 0.02570,1:0.00701 ~ 0.00857,1:0.00420 ~ 0.00514,1:0.03504 ~ 0.04283,1:0.00140 ~ 0.00171,1:0.00070 ~ 0.00086,1:0.02803 ~ 0.03426,1:0.00028 ~ 0.00034,1:0.00098 ~ 0.00120,1:0.00280 ~ 0.00343.
The manufacture method of moisturizing cleansing milk realizes according to the following steps:
(1) to destearinize acid, 16-18 mixed alcohol, monoglyceride, caprylic capric triglyceride, 2,6-di-tert-butyl-4-methy phenol, Jojoba oil, silicone oil 350, Polyethylene Glycol 100 stearate, glucoside stearate, polyoxyethylene ether glucoside stearate, American Avocado Tree oil are put into oil cauldron and are mixed, heating-up temperature 80 DEG C ± 2 DEG C, constant temperature stirs 10 minutes;
(2) deionized water B enters in kettle, opens stirring, and glycerol, betanin, 16-alkyl polyglucoside, allantoin, soapberry extract put into aqueous phase pot, agitating heating, temperature 80 DEG C ± 2 DEG C, and constant temperature stirs 10 minutes;
(3) papain puts into deionized water A, and stirring and dissolving is even, for subsequent use;
(4) heating emulsification pot, about temperature 45 C, evacuation, vacuum remains on 0.05Mpa;
(5) will meet the requirements of in oil cauldron material suction emulsifying pot, open stirring, mixing speed 300rpm, temperature 80 DEG C ± 1 DEG C;
(6) rapidly by kettle material suction emulsifying pot, mixing speed brings up to 500rpm, opens homogenizer, homogenizing speed 1800rpm, treats that material all exhausts, and homogenizing speed brings up to 2000rpm, homogenizing time 6 minutes, and homogenizing terminates, and constant temperature stirs 10 minutes;
(7) lower the temperature, open the cooling water of emulsifying pot, cooling rate 3 DEG C/2 minutes, treats that temperature reduces to 70 DEG C, again opens homogenizer, homogenizing speed 1800rpm, homogenizing time 3 minutes;
(8) treat that temperature reduces to 60 DEG C, mixing speed reduces to 400rpm, and temperature reduces to 45 DEG C, is added by the mixed material of step 3 in emulsifying pot; stir 2 minutes, add Radix Hamamelidis Mollis extracting solution respectively, Oleum lavandula angustifolia; NaOH(10% solution), Methylisothiazolinone, continues to stir;
(9) sample, analyze, do discharging simultaneously and prepare, sterilization discharge tank, opens uviol lamp, irradiates 10 minutes;
(10) treat that temperature reduces to 40 DEG C, after sample analysis result is qualified, discharging;
(11) material taken the dish out of the pot pushes rest chamber, ageing fill afterwards in 12 hours, packaging.
The present invention compared with prior art has the following advantages: effectively clean face, guarantee skin keep moistening, strengthen skin non-oxidizability and antiallergic, and can restrain pore.
detailed description of the invention
Embodiment 1
The manufacture method of moisturizing cleansing milk realizes according to the following steps:
(1) destearinize sour 0.06209kg, 16-18 mixed alcohol 0.03504 kg, monoglyceride 0.02803 kg, caprylic capric triglyceride 0.03504 kg, 2,6-di-tert-butyl-4-methy phenol 0.00070 kg, Jojoba oil 0.04884 kg, silicone oil 350 0.02102 kg, Polyethylene Glycol 100 stearate 0.00701 kg, glucoside stearate 0.01402 kg, polyoxyethylene ether glucoside stearate 0.02102 kg, American Avocado Tree oil 0.02803 kg put into oil cauldron and mix, heating-up temperature 80 DEG C ± 2 DEG C, constant temperature stirs 10 minutes;
(2) deionized water B1.1 kg enters in kettle, open stirring, glycerol 0.05508 kg, betanin 0.02102 kg, 16-alkyl polyglucoside 0.00701 kg, allantoin 0.00420 kg, soapberry extract 0.00140 kg put into aqueous phase pot, agitating heating, temperature 80 DEG C ± 2 DEG C, constant temperature stirs 10 minutes;
(3) papain 0.00070 kg puts into deionized water A0.02803 kg, and stirring and dissolving is even, for subsequent use;
(4) heating emulsification pot, about temperature 45 C, evacuation, vacuum remains on 0.05Mpa;
(5) will meet the requirements of in oil cauldron material suction emulsifying pot, open stirring, mixing speed 300rpm, temperature 80 DEG C ± 1 DEG C;
(6) rapidly by kettle material suction emulsifying pot, mixing speed brings up to 500rpm, opens homogenizer, homogenizing speed 1800rpm, treats that material all exhausts, and homogenizing speed brings up to 2000rpm, homogenizing time 6 minutes, and homogenizing terminates, and constant temperature stirs 10 minutes;
(7) lower the temperature, open the cooling water of emulsifying pot, cooling rate 3 DEG C/2 minutes, treats that temperature reduces to 70 DEG C, again opens homogenizer, homogenizing speed 1800rpm, homogenizing time 3 minutes;
(8) treat that temperature reduces to 60 DEG C; mixing speed reduces to 400rpm; temperature reduces to 45 DEG C; the mixed material of step 3 is added in emulsifying pot, stir 2 minutes, add Radix Hamamelidis Mollis extracting solution 0.03504 kg respectively; Oleum lavandula angustifolia 0.00028 kg; NaOH(10% solution) 0.00098 kg, Methylisothiazolinone 0.00280 kg, continue to stir;
(9) sample, analyze, do discharging simultaneously and prepare, sterilization discharge tank, opens uviol lamp, irradiates 10 minutes;
(10) treat that temperature reduces to 40 DEG C, after sample analysis result is qualified, discharging;
(11) material taken the dish out of the pot pushes rest chamber, ageing fill afterwards in 12 hours, packaging.
Embodiment 2
The manufacture method of moisturizing cleansing milk realizes according to the following steps:
(1) destearinize sour 0.10922 kg, 16-18 mixed alcohol 0.04283 kg, monoglyceride 0.03426 kg, caprylic capric triglyceride 0.04283 kg, 2,6-di-tert-butyl-4-methy phenol 0.00086 kg, Jojoba oil 0.09132 kg, silicone oil 350 0.02570 kg, Polyethylene Glycol 100 stearate 0.00857 kg, glucoside stearate 0.01713 kg, polyoxyethylene ether glucoside stearate 0.02570, American Avocado Tree oil 0.03426 kg put into oil cauldron and mix, heating-up temperature 80 DEG C ± 2 DEG C, constant temperature stirs 10 minutes;
(2) deionized water B0.9 kg enters in kettle, open stirring, glycerol 0.10066 kg, betanin 0.02570 kg, 16-alkyl polyglucoside 0.00857 kg, allantoin 0.00514 kg, soapberry extract 0.00171 kg put into aqueous phase pot, agitating heating, temperature 80 DEG C ± 2 DEG C, constant temperature stirs 10 minutes;
(3) papain 0.00086 kg puts into deionized water A0.03426 kg, and stirring and dissolving is even, for subsequent use;
(4) heating emulsification pot, about temperature 45 C, evacuation, vacuum remains on 0.05Mpa;
(5) will meet the requirements of in oil cauldron material suction emulsifying pot, open stirring, mixing speed 300rpm, temperature 80 DEG C ± 1 DEG C;
(6) rapidly by kettle material suction emulsifying pot, mixing speed brings up to 500rpm, opens homogenizer, homogenizing speed 1800rpm, treats that material all exhausts, and homogenizing speed brings up to 2000rpm, homogenizing time 6 minutes, and homogenizing terminates, and constant temperature stirs 10 minutes;
(7) lower the temperature, open the cooling water of emulsifying pot, cooling rate 3 DEG C/2 minutes, treats that temperature reduces to 70 DEG C, again opens homogenizer, homogenizing speed 1800rpm, homogenizing time 3 minutes;
(8) treat that temperature reduces to 60 DEG C; mixing speed reduces to 400rpm; temperature reduces to 45 DEG C; the mixed material of step 3 is added in emulsifying pot, stir 2 minutes, add Radix Hamamelidis Mollis extracting solution 0.04283 kg respectively; Oleum lavandula angustifolia 0.00034 kg; NaOH(10% solution) 0.00120 kg, Methylisothiazolinone 0.00343 kg, continue to stir;
(9) sample, analyze, do discharging simultaneously and prepare, sterilization discharge tank, opens uviol lamp, irradiates 10 minutes;
(10) treat that temperature reduces to 40 DEG C, after sample analysis result is qualified, discharging;
(11) material taken the dish out of the pot pushes rest chamber, ageing fill afterwards in 12 hours, packaging.

Claims (2)

1. a moisturizing cleansing milk, is characterized in that: the raw material comprised destearinizes acid, 16-18 mixed alcohol, monoglyceride, caprylic capric triglyceride, 2,6-di-tert-butyl-4-methy phenol, Jojoba oil, silicone oil 350, Polyethylene Glycol 100 stearate, glucoside stearate, polyoxyethylene ether glucoside stearate, American Avocado Tree oil, glycerol, betanin, 16-alkyl polyglucoside, allantoin, Radix Hamamelidis Mollis extracting solution, soapberry extract, papain, deionized water A, Oleum lavandula angustifolia, NaOH(10% solution), deionized water B and Methylisothiazolinone are 1 ultimate unit with deionized water B, deionized water B and acid of destearinizing, 16-18 mixed alcohol, monoglyceride, caprylic capric triglyceride, 2,6-di-tert-butyl-4-methy phenol, Jojoba oil, silicone oil 350, Polyethylene Glycol 100 stearate, glucoside stearate, polyoxyethylene ether glucoside stearate, American Avocado Tree oil, glycerol, betanin, 16-alkyl polyglucoside, allantoin, Radix Hamamelidis Mollis extracting solution, soapberry extract, papain, deionized water A, Oleum lavandula angustifolia, NaOH(10% solution) and the mass ratio of Methylisothiazolinone be 1:0.06209 ~ 0.10922, 1:0.03504 ~ 0.04283,1:0.02803 ~ 0.03426,1:0.03504 ~ 0.04283,1:0.00070 ~ 0.00086,1:0.04884 ~ 0.09132,1:0.02102 ~ 0.02570,1:0.00701 ~ 0.00857,1:0.01402 ~ 0.01713,1:0.02102 ~ 0.02570,1:0.02803 ~ 0.03426,1:0.05508 ~ 0.10066,1:0.02102 ~ 0.02570,1:0.00701 ~ 0.00857,1:0.00420 ~ 0.00514,1:0.03504 ~ 0.04283,1:0.00140 ~ 0.00171,1:0.00070 ~ 0.00086,1:0.02803 ~ 0.03426,1:0.00028 ~ 0.00034,1:0.00098 ~ 0.00120,1:0.00280 ~ 0.00343.
2. a moisturizing cleansing milk, it is characterized in that: (1) destearinizes acid, 16-18 mixed alcohol, monoglyceride, caprylic capric triglyceride, 2,6-di-tert-butyl-4-methy phenol, Jojoba oil, silicone oil 350, Polyethylene Glycol 100 stearate, glucoside stearate, polyoxyethylene ether glucoside stearate, American Avocado Tree oil are put into oil cauldron and are mixed, heating-up temperature 80 DEG C ± 2 DEG C, constant temperature stirs 10 minutes;
(2) deionized water B enters in kettle, opens stirring, and glycerol, betanin, 16-alkyl polyglucoside, allantoin, soapberry extract put into aqueous phase pot, agitating heating, temperature 80 DEG C ± 2 DEG C, and constant temperature stirs 10 minutes;
(3) papain puts into deionized water A, and stirring and dissolving is even, for subsequent use;
(4) heating emulsification pot, about temperature 45 C, evacuation, vacuum remains on 0.05Mpa;
(5) will meet the requirements of in oil cauldron material suction emulsifying pot, open stirring, mixing speed 300rpm, temperature 80 DEG C ± 1 DEG C;
(6) rapidly by kettle material suction emulsifying pot, mixing speed brings up to 500rpm, opens homogenizer, homogenizing speed 1800rpm, treats that material all exhausts, and homogenizing speed brings up to 2000rpm, homogenizing time 6 minutes, and homogenizing terminates, and constant temperature stirs 10 minutes;
(7) lower the temperature, open the cooling water of emulsifying pot, cooling rate 3 DEG C/2 minutes, treats that temperature reduces to 70 DEG C, again opens homogenizer, homogenizing speed 1800rpm, homogenizing time 3 minutes;
(8) treat that temperature reduces to 60 DEG C, mixing speed reduces to 400rpm, and temperature reduces to 45 DEG C, is added by the mixed material of step 3 in emulsifying pot; stir 2 minutes, add Radix Hamamelidis Mollis extracting solution respectively, Oleum lavandula angustifolia; NaOH(10% solution), Methylisothiazolinone, continues to stir;
(9) sample, analyze, do discharging simultaneously and prepare, sterilization discharge tank, opens uviol lamp, irradiates 10 minutes;
(10) treat that temperature reduces to 40 DEG C, after sample analysis result is qualified, discharging;
(11) material taken the dish out of the pot pushes rest chamber, ageing fill afterwards in 12 hours, packaging.
CN201310735321.1A 2013-12-28 2013-12-28 Moisturizing facial cleanser and preparation method thereof Pending CN104739703A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107412075A (en) * 2017-09-04 2017-12-01 广州聚注通用技术研究院有限公司 A kind of deep layer cleaning mildy wash
CN108309843A (en) * 2018-02-05 2018-07-24 广州鹰远生物科技有限公司 It is a kind of to have effects that purify the composition and its preparation method and application of pore

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107412075A (en) * 2017-09-04 2017-12-01 广州聚注通用技术研究院有限公司 A kind of deep layer cleaning mildy wash
CN108309843A (en) * 2018-02-05 2018-07-24 广州鹰远生物科技有限公司 It is a kind of to have effects that purify the composition and its preparation method and application of pore

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