CN103289838B - Litchi transparent soap and preparation method thereof - Google Patents
Litchi transparent soap and preparation method thereof Download PDFInfo
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- CN103289838B CN103289838B CN201310258542.4A CN201310258542A CN103289838B CN 103289838 B CN103289838 B CN 103289838B CN 201310258542 A CN201310258542 A CN 201310258542A CN 103289838 B CN103289838 B CN 103289838B
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Abstract
The invention relates to a litchi transparent soap. The litchi transparent soap comprises the following steps in percentage by weight: 8%-12% of coconut oil, 4%-8% of palm oil, 5%-9% of castor oil, 12%-14% of sodium hydroxide solution with the mass concentration of 30%, 10%-15% of anhydrous ethanol, 10%-18% of glycerine, 6%-8% of propylene glycol, 2%-3% of dipropylene glycol, 11%-15% of sucrose, 1%-3% of crystallization refining agent, 1%-5% of litchi seed extraction solution and 9%-14% of water. The litchi transparent soap disclosed by the invention has the advantages of capability of turning waste litchi seeds into treasures, ordinary raw material, easiness in obtaining the raw material, low production cost, high product transparency and good skin-moistening and skin care effects.
Description
Technical field
The present invention relates to a kind of daily necessities and preparation method thereof, relate in particular to transparent soap with beauty treatment, moisturizing, senile-resistant efficacy of a kind of all-transparent and preparation method thereof.
Background technology
At present, domestic in development, produce aspect all-transparent beauty soap and starting late, and early have production and selling all-transparent beauty soap in the market of the countries and regions such as Japan, the U.S., Singapore, Hong Kong, Taiwan, wash industry abroad and become trend to superior, functionalization development.Current domestic adding type transparent soap is mainly to take import as main, or is formed by import neat soap processing and fabricating, and product price is relatively costly, and ordinary consumer is also difficult to accept.
The main chemical compositions of Semen Litchi is saponin(e, phenols, lipid acid, polymerization cyanidin(e), amino acid and volatile component (steroid class, terpene etc.).Pharmacy and clinical study show, Semen Litchi have resistance of oxidation, antiviral, suppress many physiologically actives such as tumour, reducing blood-fat, enhancing immunity.Litchi nucleus extract fluid contains a large amount of biologically active substances, uses it in transparent soap, has sterilizing and anti-virus, resistance of oxidation effect, with after can salubrious skin, also very helpful to treatment comedo and acne, life-time service, can reach beauty treatment, skin care, senile-resistant efficacy.
Also there is no in the market to occur to take the transparent soap that Semen Litchi is raw material.
Summary of the invention
The technical problem to be solved in the present invention is: overcome the defect that also there is no the transparent soap of Semen Litchi raw material at present, provide a kind of proportioning raw materials precise and appropriate, transparency is high, has the all-transparent lichee soap of sterilization, skin care, beauty treatment.
In order to solve the problems of the technologies described above, the present invention proposes following technical scheme: a kind of lichee transparent soap, its component by following mass percent forms: the sodium hydroxide solution 12%-14% that Oleum Cocois 8%-12%, plam oil 4%-8%, Viscotrol C 5%-9%, mass concentration are 30%, dehydrated alcohol 10%-15%, glycerine 10%-18%, propylene glycol 6%-8%, dipropylene glycol 2%-3%, sucrose 11%-15%, crystallization fining agent 1%-3%, litchi nucleus extract fluid 1%-5%, water 9%-14%.
The further restriction of technique scheme is: above-mentioned crystallization fining agent is polyphosphoric acid salt or fatty alcohol ethers material.
The further restriction of technique scheme is: above-mentioned litchi nucleus extract fluid is with supercritical extraction method, to extract the crude extract of Semen Litchi gained.
In order to solve the problems of the technologies described above, the present invention proposes following technical scheme: a kind of preparation method who prepares described lichee transparent soap, it comprises the steps:
Step 1: according to mass percent, sodium hydroxide solution 12%-14%, dehydrated alcohol 10%-15%, glycerine 10%-18%, propylene glycol 6%-8%, dipropylene glycol 2%-3%, sucrose 11%-15%, crystallization fining agent 1%-3%, litchi nucleus extract fluid 1%-5%, water 9%-14% that to get Oleum Cocois 8%-12%, plam oil 4%-8%, Viscotrol C 5%-9%, mass concentration be 30%;
Step 2: Oleum Cocois, plam oil, Viscotrol C are mixed, be heated to 70-80 ℃, stir and make it fully mix thawing simultaneously with stirrer, adding successively mass concentration is 30% sodium hydroxide solution and dehydrated alcohol, continues to be stirred to thick, and saponification completes;
Step 3: become sucrose solution after the water dissolution by sucrose with 9%-14%, by glycerine, dipropylene glycol, propylene glycol, sucrose solution after 70-80 ℃ of heating dissolves, add in the mixture of step 2 gained and stir, add again crystallization fining agent to stir evenly, treat that temperature is down to 60 ℃ of left and right, add successively litchi nucleus extract fluid, stir 10 minutes, reverse mould, cooling curing moulding.
The further restriction of technique scheme is: above-mentioned crystallization fining agent is polyphosphoric acid salt or fatty alcohol ethers material.
The further restriction of technique scheme is: above-mentioned litchi nucleus extract fluid is with supercritical extraction method, to extract the crude extract of Semen Litchi gained.
Compared with prior art, the present invention has following beneficial effect: except small part Semen Litchi is as Chinese medicinal materials, most of Semen Litchi has all been discarded, Semen Litchi is turned waste into wealth in the present invention, and raw material is common to be easy to get, and production cost is low, product transparency is high, and moisturizing skin effect is good.
Embodiment
The present invention proposes a kind of lichee transparent soap, and its component by following mass percent forms: the sodium hydroxide solution 12%-14% that Oleum Cocois 8%-12%, plam oil 4%-8%, Viscotrol C 5%-9%, mass concentration are 30%, dehydrated alcohol 10%-15%, glycerine 10%-18%, propylene glycol 6%-8%, dipropylene glycol 2%-3%, sucrose 11%-15%, crystallization fining agent 1%-3%, litchi nucleus extract fluid 1%-5%, water 9%-14%.
Above-mentioned crystallization fining agent is divided into inorganic crystal fining agent and the large class of organic crystal fining agent two.Conventional inorganic crystal fining agent is polyphosphoric acid salt (sylvite, sodium salt), and conventional organic crystal fining agent is fatty alcohol ethers material.
Above-mentioned litchi nucleus extract fluid is with supercritical extraction method, to extract the crude extract of Semen Litchi gained.Supercritical extraction can effectively be protected the active skull cap components of Semen Litchi.
The preparation method of above-mentioned lichee transparent soap comprises the steps:
Step 1: according to mass percent, sodium hydroxide solution 12%-14%, dehydrated alcohol 10%-15%, glycerine 10%-18%, propylene glycol 6%-8%, dipropylene glycol 2%-3%, sucrose 11%-15%, crystallization fining agent 1%-3%, litchi nucleus extract fluid 1%-5%, water 9%-14% that to get Oleum Cocois 8%-12%, plam oil 4%-8%, Viscotrol C 5%-9%, mass concentration be 30%;
Step 2: Oleum Cocois, plam oil, Viscotrol C are mixed, be heated to 70-80 ℃, stir and make it fully mix thawing simultaneously with stirrer, adding successively mass concentration is 30% sodium hydroxide solution and dehydrated alcohol, continues to be stirred to thick, and saponification completes;
Step 3: become sucrose solution after the water dissolution by sucrose with 9%-14%, by glycerine, dipropylene glycol, propylene glycol, sucrose solution after 70-80 ℃ of heating dissolves, add in the mixture of step 2 gained and stir, add again crystallization fining agent to stir evenly, treat that temperature is down to 60 ℃ of left and right, add successively litchi nucleus extract fluid, stir 10 minutes, reverse mould, cooling curing moulding.
In above-mentioned preparation method, can be chosen in step 1 and take appropriate pigment and essence, in step 3, together add stirring with litchi nucleus extract fluid.
The transparent soap that said components and preparation method make contains litchi nucleus extract fluid, contain abundant activeconstituents saponin(e, plant polyphenol (being mainly flavonoid compound) etc., there is sterilizing and anti-virus, remove free radical, resistance of oxidation effect, the salubrious skin of energy after use, treatment comedo and acne are also benefited, and life-time service can reach beauty treatment, skin care, anti-aging effects.
Because grease easily reacts generation sodium soap hydrate macromole when the saponification with sodium hydroxide solution, and then affect the transparency of transparent soap, add crystallization fining agent can stop sodium soap in process of cooling, to form large xln, can obviously improve the transparency of lichee transparent soap, do not add the transparency of crystallization fining agent product to only have 70%, add crystallization fining agent after transparency can reach 92%.
The physical and chemical index of the lichee transparent soap that the present invention makes is as shown in the table:
| Project | Index |
| Total working substance/% | ≥55 |
| Moisture and volatile matter/% | ≤30 |
| Free caustic alkali (in NaOH)/% | ≤0.2 |
| Total free caustic alkali (in NaOH)/% | ≤0.3 |
| Muriate (in NaCl)/% | ≤0.7 |
| Transparency [(6.50+0.15) the thick section of mm]/% | ≥90 |
| Roche Latherometer is surveyed foaming power (mm) | ≥50 |
Preparation Example one
According to weight percent, getting Oleum Cocois 12%, plam oil 4%, Viscotrol C 9%, mass concentration is 30% sodium hydroxide solution 14%, dehydrated alcohol 12%, glycerine 10%, propylene glycol 8%, dipropylene glycol 3%, sucrose 13%, crystallization fining agent 2%, litchi nucleus extract fluid 1%, water 12%;
Oleum Cocois, plam oil, Viscotrol C are mixed, be heated to 70-80 ℃, stir and make it fully mix thawing simultaneously with stirrer, adding successively mass concentration is 30% sodium hydroxide solution and dehydrated alcohol, continues to be stirred to thick, and saponification completes;
By sucrose with becoming sucrose solution after water dissolution, by glycerine, dipropylene glycol, propylene glycol, sucrose solution after 70-80 ℃ of heating dissolves, add in the mixture of previous step gained and stir, add again crystallization fining agent to stir evenly, treat that temperature is down to 60 ℃ of left and right, add successively litchi nucleus extract fluid, stir 10 minutes, reverse mould, cooling curing moulding, can obtain lichee transparent soap of the present invention.
| Project | Content |
| Total working substance/% | 67 |
| Moisture and volatile matter/% | 26 |
| Free caustic alkali (in NaOH)/% | 0.18 |
| Total free caustic alkali (in NaOH)/% | 0.21 |
| Muriate (in NaCl)/% | 0.2 |
| Transparency [(6.50+0.15) the thick section of mm]/% | 92 |
| Roche Latherometer is surveyed foaming power (mm) | 60 |
Preparation Example two
According to weight percent, getting Oleum Cocois 10%, plam oil 8%, Viscotrol C 8%, mass concentration is 30% sodium hydroxide solution 13%, dehydrated alcohol 10%, glycerine 10%, propylene glycol 6%, dipropylene glycol 2%, sucrose 15%, crystallization fining agent 1%, litchi nucleus extract fluid 5%, water 12%;
Oleum Cocois, plam oil, Viscotrol C are mixed, be heated to 70-80 ℃, stir and make it fully mix thawing simultaneously with stirrer, adding successively mass concentration is 30% sodium hydroxide solution and dehydrated alcohol, continues to be stirred to thick, and saponification completes;
By sucrose with becoming sucrose solution after water dissolution, by glycerine, dipropylene glycol, propylene glycol, sucrose solution after 70-80 ℃ of heating dissolves, add in the mixture of previous step gained and stir, add again crystallization fining agent to stir evenly, treat that temperature is down to 60 ℃ of left and right, add successively litchi nucleus extract fluid, stir 10 minutes, reverse mould, cooling curing moulding, can obtain lichee transparent soap of the present invention.
The transparency of the lichee transparent soap that the present embodiment makes is 93%.
| Project | Content |
| Total working substance/% | 70 |
| Moisture and volatile matter/% | 28 |
| Free caustic alkali (in NaOH)/% | 0.16 |
| Total free caustic alkali (in NaOH)/% | 0.24 |
| Muriate (in NaCl)/% | 0.3 |
| Transparency [(6.50+0.15) the thick section of mm]/% | 93 |
| Roche Latherometer is surveyed foaming power (mm) | 65 |
Preparation Example three
According to weight percent, getting Oleum Cocois 11%, plam oil 8%, Viscotrol C 5%, mass concentration is 30% sodium hydroxide solution 12%, dehydrated alcohol 15%, glycerine 14%, propylene glycol 7%, dipropylene glycol 2.5%, sucrose 11%, crystallization fining agent 3%, litchi nucleus extract fluid 1.5%, water 10%;
Oleum Cocois, plam oil, Viscotrol C are mixed, be heated to 70-80 ℃, stir and make it fully mix thawing simultaneously with stirrer, adding successively mass concentration is 30% sodium hydroxide solution and dehydrated alcohol, continues to be stirred to thick, and saponification completes;
By sucrose with becoming sucrose solution after water dissolution, by glycerine, dipropylene glycol, propylene glycol, sucrose solution after 70-80 ℃ of heating dissolves, add in the mixture of previous step gained and stir, add again crystallization fining agent to stir evenly, treat that temperature is down to 60 ℃ of left and right, add successively litchi nucleus extract fluid, stir 10 minutes, reverse mould, cooling curing moulding, can obtain lichee transparent soap of the present invention.
The transparency of the lichee transparent soap that the present embodiment makes is 94%.
| Project | Content |
| Total working substance/% | 68 |
| Moisture and volatile matter/% | 27 |
| Free caustic alkali (in NaOH)/% | 0.15 |
| Total free caustic alkali (in NaOH)/% | 0.18 |
| Muriate (in NaCl)/% | 0.1 |
| Transparency [(6.50+0.15) the thick section of mm]/% | 94 |
| Roche Latherometer is surveyed foaming power (mm) | 66 |
Preparation Example four
According to weight percent, getting Oleum Cocois 8%, plam oil 8%, Viscotrol C 5%, mass concentration is 30% sodium hydroxide solution 12%, dehydrated alcohol 10%, glycerine 10%, propylene glycol 6%, dipropylene glycol 3%, sucrose 15%, crystallization fining agent 3%, litchi nucleus extract fluid 5%, water 14%.
Oleum Cocois, plam oil, Viscotrol C are mixed, be heated to 70-80 ℃, stir and make it fully mix thawing simultaneously with stirrer, adding successively mass concentration is 30% sodium hydroxide solution and dehydrated alcohol, continues to be stirred to thick, and saponification completes;
By sucrose with becoming sucrose solution after water dissolution, by glycerine, dipropylene glycol, propylene glycol, sucrose solution after 70-80 ℃ of heating dissolves, add in the mixture of previous step gained and stir, add again crystallization fining agent to stir evenly, treat that temperature is down to 60 ℃ of left and right, add successively litchi nucleus extract fluid, stir 10 minutes, reverse mould, cooling curing moulding, can obtain lichee transparent soap of the present invention.
The transparency of the lichee transparent soap that the present embodiment makes is 92%.
| Project | Content |
| Total working substance/% | 66 |
| Moisture and volatile matter/% | 24 |
| Free caustic alkali (in NaOH)/% | 0.18 |
| Total free caustic alkali (in NaOH)/% | 0.20 |
| Muriate (in NaCl)/% | 0.2 |
| Transparency [(6.50+0.15) the thick section of mm]/% | 92 |
| Roche Latherometer is surveyed foaming power (mm) | 69 |
Preparation Example five
According to weight percent, Oleum Cocois 8%, plam oil 4%, Viscotrol C 9%, mass concentration are 30% sodium hydroxide solution 12%, dehydrated alcohol 12%, glycerine 18%, propylene glycol 7%, dipropylene glycol 2.5%, sucrose 14%, crystallization fining agent 1.5%, litchi nucleus extract fluid 3%, water 9%.
Oleum Cocois, plam oil, Viscotrol C are mixed, be heated to 70-80 ℃, stir and make it fully mix thawing simultaneously with stirrer, adding successively mass concentration is 30% sodium hydroxide solution and dehydrated alcohol, continues to be stirred to thick, and saponification completes;
By sucrose with becoming sucrose solution after water dissolution, by glycerine, dipropylene glycol, propylene glycol, sucrose solution after 70-80 ℃ of heating dissolves, add in the mixture of previous step gained and stir, add again crystallization fining agent to stir evenly, treat that temperature is down to 60 ℃ of left and right, add successively litchi nucleus extract fluid, stir 10 minutes, reverse mould, cooling curing moulding, can obtain lichee transparent soap of the present invention.
The transparency of the lichee transparent soap that the present embodiment makes is 95%.
| Project | Content |
| Total working substance/% | 68 |
| Moisture and volatile matter/% | 25 |
| Free caustic alkali (in NaOH)/% | 0.19 |
| Total free caustic alkali (in NaOH)/% | 0.21 |
| Muriate (in NaCl)/% | 0.2 |
| Transparency [(6.50+0.15) the thick section of mm]/% | 95 |
| Roche Latherometer is surveyed foaming power (mm) | 68 |
Claims (6)
1. a lichee transparent soap, its component by following mass percent forms: the sodium hydroxide solution 12%-14% that Oleum Cocois 8%-12%, plam oil 4%-8%, Viscotrol C 5%-9%, mass concentration are 30%, dehydrated alcohol 10%-15%, glycerine 10%-18%, propylene glycol 6%-8%, dipropylene glycol 2%-3%, sucrose 11%-15%, crystallization fining agent 1%-3%, litchi nucleus extract fluid 1%-5%, water 9%-14%.
2. according to described lichee transparent soap claimed in claim 1, it is characterized in that: above-mentioned crystallization fining agent is polyphosphoric acid salt or fatty alcohol ethers material.
3. according to described lichee transparent soap claimed in claim 1, it is characterized in that: above-mentioned litchi nucleus extract fluid is with supercritical extraction method, to extract the crude extract of Semen Litchi gained.
4. a preparation method who prepares lichee transparent soap as claimed in claim 1, is characterized in that, it comprises the steps:
Step 1: according to mass percent, sodium hydroxide solution 12%-14%, dehydrated alcohol 10%-15%, glycerine 10%-18%, propylene glycol 6%-8%, dipropylene glycol 2%-3%, sucrose 11%-15%, crystallization fining agent 1%-3%, litchi nucleus extract fluid 1%-5%, water 9%-14% that to get Oleum Cocois 8%-12%, plam oil 4%-8%, Viscotrol C 5%-9%, mass concentration be 30%;
Step 2: Oleum Cocois, plam oil, Viscotrol C are mixed, be heated to 70-80 ℃, stir and make it fully mix thawing simultaneously with stirrer, adding successively mass concentration is 30% sodium hydroxide solution and dehydrated alcohol, continues to be stirred to thick, and saponification completes;
Step 3: become sucrose solution after the water dissolution by sucrose with 9%-14%, by glycerine, dipropylene glycol, propylene glycol, sucrose solution after 70-80 ℃ of heating dissolves, add in the mixture of step 2 gained and stir, add again crystallization fining agent to stir evenly, treat that temperature is down to 60 ℃ of left and right, add successively litchi nucleus extract fluid, stir 10 minutes, reverse mould, cooling curing moulding.
5. according to the preparation method of described lichee transparent soap claimed in claim 4, it is characterized in that: above-mentioned crystallization fining agent is polyphosphoric acid salt or fatty alcohol ethers material.
6. according to the preparation method of described lichee transparent soap claimed in claim 4, it is characterized in that: above-mentioned litchi nucleus extract fluid is with supercritical extraction method, to extract the crude extract of Semen Litchi gained.
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103834504B (en) * | 2013-12-27 | 2016-08-17 | 北华大学 | A kind of ginseng polypeptide Transparent handmade soap and preparation method thereof |
| CN105886164A (en) * | 2016-05-31 | 2016-08-24 | 李咏梅 | Gold pomelo seed oil soap and preparing method thereof |
| CN110144267B (en) * | 2019-06-18 | 2021-05-21 | 西藏自治区农牧科学院农产品开发与食品科学研究所 | Lanolin-containing handmade soap and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101427990A (en) * | 2008-12-12 | 2009-05-13 | 上海蔻漫生物科技有限公司 | Skin cleaning article |
| CN103013715A (en) * | 2012-12-20 | 2013-04-03 | 广东鹏锦实业有限公司 | Transparent soap |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101427990A (en) * | 2008-12-12 | 2009-05-13 | 上海蔻漫生物科技有限公司 | Skin cleaning article |
| CN103013715A (en) * | 2012-12-20 | 2013-04-03 | 广东鹏锦实业有限公司 | Transparent soap |
Non-Patent Citations (2)
| Title |
|---|
| 全透明美容皂的研制;张希琴等;《山 东 化 工》;20011231;第30卷(第4期);9-10，14 * |
| 张希琴等.全透明美容皂的研制.《山 东 化 工》.2001,第30卷(第4期),9-10，14. |
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Effective date of registration: 20180920 Address after: 518000 Floors 1-4 of Building 7, Shantangwei Fuan Industrial Zone, Pingdi Street Center, Longgang District, Shenzhen City, Guangdong Province Patentee after: Mei Fu source, Shenzhen daily necessities company limited Address before: 518055 Xili Lake, Nanshan District, Shenzhen, Guangdong Patentee before: Shenzhen Polytechnic |