CN104725234A - 尼泊金甲酯钠的制备方法 - Google Patents

尼泊金甲酯钠的制备方法 Download PDF

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Publication number
CN104725234A
CN104725234A CN201310718398.8A CN201310718398A CN104725234A CN 104725234 A CN104725234 A CN 104725234A CN 201310718398 A CN201310718398 A CN 201310718398A CN 104725234 A CN104725234 A CN 104725234A
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China
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preparation
hydroxybenzoate
sodium methylparaben
methyl
reaction vessel
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CN201310718398.8A
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English (en)
Inventor
郝永明
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Qingdao Xiuxian Foods Co Ltd
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Qingdao Xiuxian Foods Co Ltd
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Priority to CN201310718398.8A priority Critical patent/CN104725234A/zh
Publication of CN104725234A publication Critical patent/CN104725234A/zh
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/30—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group
    • C07C67/31—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by introduction of functional groups containing oxygen only in singly bound form

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

本发明公开了一种尼泊金甲酯钠的制备方法，包括以下步骤：一、先将对羟基苯甲酸甲酯加入反应容器中，然后取1.05倍对羟基苯甲酸甲酯摩尔量的氢氧化钠，缓慢滴加到反应器中，室温下反应1h；二、反应完毕，静置结晶，离心过滤，真空干燥，即得成品尼泊金甲酯钠。本发明提供的尼泊金甲酯钠的制备方法，生产工艺简便易行，原料易得，降低了生产成本，生产过程无“三废”产生，绿色环保。

Description

尼泊金甲酯钠的制备方法
 
技术领域
本发明涉及一种防腐剂的制备方法，具体涉及一种尼泊金甲酯钠的制备方法。
 
背景技术
尼泊金甲酯钠作为尼泊金酯的改性产品，拥有尼泊金酯的抑菌性能和安全性能，同时克服了尼泊金酯水溶性低的缺陷。许多国家和地区把尼泊金甲酯钠作为食品防腐剂，已广泛应用于肉制品、脂肪制品、乳制品、水产品、调味品、糖果、果蔬制品、啤酒、果酒及果蔬保鲜等领域。尼泊金甲酯钠作为一种新型的光谱、高效防腐剂，同苯甲酸钠和山梨酸钾相比，具有以下优势：抑菌效果好、适用的pH范围广、毒副作用小、使用成本低、方便。
 
发明内容
本发明的目的在于，提供一种尼泊金甲酯钠的制备方法，生产工艺简便易行，原料易得，降低了生产成本，生产过程无“三废”产生，绿色环保。
所述尼泊金甲酯钠的制备方法，包括以下步骤：
一、先将对羟基苯甲酸甲酯加入反应容器中，然后取1.05倍对羟基苯甲酸甲酯摩尔量的氢氧化钠，缓慢滴加到反应器中，室温下反应1h；
二、反应完毕，静置结晶，离心过滤，真空干燥，即得成品尼泊金甲酯钠。
本发明提供的尼泊金甲酯钠的制备方法，其有益效果在于，生产工艺简便易行，原料易得，降低了生产成本，生产过程无“三废”产生，绿色环保。
 
具体实施方式
下面结合一个实施例，对本发明提供的尼泊金甲酯钠的制备方法进行详细的说明。
 
    实施例
一、先将1mol对羟基苯甲酸甲酯加入反应容器中，然后将1.05mol氢氧化钠缓慢滴加到反应器中，室温下反应1h；
二、反应完毕，静置结晶，离心过滤，真空干燥，即得成品尼泊金甲酯钠。

Claims (1)

1.一种尼泊金甲酯钠的制备方法，其特征在于：它包括以下步骤：
一、先将对羟基苯甲酸甲酯加入反应容器中，然后取1.05倍对羟基苯甲酸甲酯摩尔量的氢氧化钠，缓慢滴加到反应器中，室温下反应1h；
二、反应完毕，静置结晶，离心过滤，真空干燥，即得成品尼泊金甲酯钠。
CN201310718398.8A 2013-12-24 2013-12-24 尼泊金甲酯钠的制备方法 Pending CN104725234A (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310718398.8A CN104725234A (zh) 2013-12-24 2013-12-24 尼泊金甲酯钠的制备方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201310718398.8A CN104725234A (zh) 2013-12-24 2013-12-24 尼泊金甲酯钠的制备方法

Publications (1)

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CN104725234A true CN104725234A (zh) 2015-06-24

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CN201310718398.8A Pending CN104725234A (zh) 2013-12-24 2013-12-24 尼泊金甲酯钠的制备方法

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CN (1) CN104725234A (zh)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106496032A (zh) * 2016-08-30 2017-03-15 芜湖华海生物工程有限公司 一种对羟基苯甲酸甲酯钠的制备方法

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106496032A (zh) * 2016-08-30 2017-03-15 芜湖华海生物工程有限公司 一种对羟基苯甲酸甲酯钠的制备方法

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Application publication date: 20150624