The application is application number is 201410002747.0, the applying date: on January 4th, 2014, invention and created name is: the preparation method of compound formulation of repairing willow bark wound of hanging down, the divisional application of patent of invention.
Summary of the invention
In order to solve the problem that vertical willow bark wound is not easily repaired, the present invention proposes a kind of restorative procedure, and this method effectively can repair wound, and reduces wound deterioration probability.
The technical scheme that technical solution problem of the present invention adopts is:
Repair the preparation method of the compound formulation of willow bark wound of hanging down, it is characterized in that:
The first step, the metasilicate pentahydrate sodium being 14.5 parts by weight be 100 water, parts by weight stirs,
Second step, inside the liquid of the first step, adds the boric acid that parts by weight are 3, and stirs 5 minutes to 10 minutes,
3rd step, adds the Iron dichloride tetrahydrate that parts by weight are 30 inside the liquid of second step, and stirs 5 minutes to 10 minutes.
Repair the compound formulation of willow bark wound of hanging down, it is characterized in that: this compound formulation is made up of following methods:
The first step, the metasilicate pentahydrate sodium being 14.5 parts by weight be 100 water, parts by weight stirs,
Second step, inside the liquid of the first step, adds the boric acid that parts by weight are 3, and stirs 5 minutes to 10 minutes,
3rd step, adds the Iron dichloride tetrahydrate that parts by weight are 30 inside the liquid of second step, and stirs 5 minutes to 10 minutes.
Hang down willow bark wound restorative procedure, it is characterized in that:
A: configuration compound formulation, method is:
The first step, the metasilicate pentahydrate sodium being 14.5 parts by weight be 100 water, parts by weight stirs,
Second step, inside the liquid of the first step, adds the boric acid that parts by weight are 3, and stirs 5 minutes to 10 minutes,
3rd step, adds the Iron dichloride tetrahydrate that parts by weight are 30 inside the liquid of second step, and stirs 5 minutes to 10 minutes.
B: the mixture obtained by step A is brushed the outer injury of vertical willow bark.
Embodiment
Repair the preparation method of the compound formulation of willow bark wound of hanging down, it is characterized in that:
The first step, the metasilicate pentahydrate sodium being 14.5 parts by weight be 100 water, parts by weight stirs, metasilicate pentahydrate sodium (Na
2si O
35H
2o): monocline pillar-shaped crystal, fusing point 72.2 DEG C, soluble in water and sig water.
Then, just second step is carried out.
Second step, inside the liquid of the first step, adds the boric acid that parts by weight are 3, and stirs 5 minutes to 10 minutes.Boric acid (molecular formula: H
3bO
3) be a kind of inorganic acid, it is white powder or clear crystals, water soluble.Mixing tool used is waddy.
Then, the 3rd step is just carried out.
3rd step, adds the Iron dichloride tetrahydrate (FeCl that parts by weight are 30 inside the liquid of second step
24H
2and stir 5 minutes to 10 minutes O).Mixing tool used is waddy.
The footmark (footnote) of chemical substance, when carrying out electronics submission, usually become non-footmark numeral, but it is footmarks that various equivalent modifications should know these numerals.
Test site and time: forest base, economic development zone, Lianyungang, start test the first tenday period of a month in May.
Test illustrates: 1, choose weeping willow tree trunk (also referred to as trunk) or the limb (limb is also referred to as branch) of more than diameter 10cm, about 10 centimeter length are cut out with cutter, about 5 centimetres of wide barks (comprise bast zone, form layer), until expose xylem, because the cross section of trunk or branch mostly is circular or oval, the size cutting out bark cannot be accomplished very accurate, so, about 10 centimetres, about 5 centimetres adopt " about " word to belong to various equivalent modifications knows.Also it should be noted that, " long 10 centimetres " described here refer to the length being parallel to marrow (trunk or branch), and " wide 5 centimetres " refers to the length perpendicular to marrow (trunk or branch).
2, manufacture 1 after wound and littlely in 2 hours, pick (being also written as: dip) compound formulation of the present invention with brush, be brushed to wound location.Wound hangs up label, marks the type of preparation of brushing, brushes the date first.
3, change the parts by weight of material used respectively, do comparative trial.
4, often organize experimental scheme wound 100.Every tree manufactures 2 wounds at the most, and two wound distance requirements are: be greater than 2 meters along stem.
5, every brushing in a 10 days same liquid.Together with brushing first, brushing 10 times altogether.Each brushing all newly configures identical brushing liquid.The liquid of each configuration, did not just re-use more than 24 hours.
6, brush in latter 4 hours as rainy in run into, then, in 24 hours that stop at rain, again brush same liquid, but such benefit brush number of times is not counted on brushes in number of times, and, be not considered to the zero date of brushing next time yet.
7, total Test result was investigated in mid-August, simultaneously statistical results.
8, result of the test is divided into three kinds: 1, healing.Healing refers to that bark forms knurl portion, closes or base closed wound, and withered phenomenon does not occur locally to fester.2, dry (referring to that healing ability is poor).Drying refers to that wound becomes dry, but bark does not form knurl portion; Though or form a small amount of knurl portion, knurl portion does not obviously close wound, and wound area accounts for more than 4/5 of former wound area.3, worsen.Worsen and refer to that wound obviously has juice to flow out, local is festered withered.
Below provide comparative test result.In form, water, metasilicate pentahydrate sodium, boric acid, Iron dichloride tetrahydrate all refer to parts by weight.
Below provide five groups of comparative test result again, wherein last group all substances content is all 0, means without specially treated, only result in its natural state.