CN104673462A - Oil composition for total loss system produced by reclaimed oil - Google Patents
Oil composition for total loss system produced by reclaimed oil Download PDFInfo
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- CN104673462A CN104673462A CN201510041625.7A CN201510041625A CN104673462A CN 104673462 A CN104673462 A CN 104673462A CN 201510041625 A CN201510041625 A CN 201510041625A CN 104673462 A CN104673462 A CN 104673462A
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Abstract
The invention provides an oil composition for a total loss system produced by reclaimed oil. The lubricating oil is prepared from the following raw materials in parts by weight: 100.0 parts of reclaimed base oil, 0.01-10.0 part of a viscosity modifier, 0.01-10.0 parts of a clearing agent, 0.01-5.0 parts of a dispersing agent, 0.5-3.0 part of an oxidation and corrosion inhibitor, 0.01-10.0 parts of an extreme pressure agent, 0.5-3.0 parts of an antirust agent and 0.0001-0.01 part of an antifoaming agent. The oil composition for the total loss system produced by the reclaimed oil can meet the performance requirements of the oil for the total loss system, of which the viscosity grades are 5, 7, 10, 15, 22, 32, 46, 68, 100 and 150 in GB443-1989.
Description
Technical field
The present invention relates to total loss system oil composition, be particularly useful for, to the total loss oiling system of lubricating oil without particular requirement, not being suitable for circulation lubrication system.
Background technology
Total loss system oil is applicable to various textile manufacturing machine, various lathe, water pressure engine, small-sized pneumatic machinery, sewing machine, micro-machine, general instrument, woodworking machine, weight handling equipment, papermaking equipment, mining machinery etc.And be applicable to the general oiling systems such as wheel box, manually the oiling rotary part of the various light load machineries of working temperature below 60 DEG C.The whole world will consume a large amount of total loss system wet goods lubricating oil every year, produces again a large amount of waste lubricating oils.If waste lubricating oil is discarded in environment and goes, Metal Salts wherein, the organic compound such as sulfur-bearing, phosphorus, will cause severe contamination to environment, and waste lubricating oil is reclaimed in regeneration then can bring huge economic benefit.This technology in response national policy, is protection of the environment, makes rational use of resources just, and the technical scheme of actively probing into.The reclaimed lubricating base oil utilizing Xinjiang Fuke oil Co., Ltd to produce is to prepare total loss system oil, and this total loss system oil composition can meet the performance requriements that GB443-1989 total loss system oil viscosity grade is 5,7,10,15,22,32,46,68,100,150.
Searching document discloses: [1] patent CN103897790 [2] patent CN103740439 relates to patent of the present invention.
Current China total loss system oil is produced primarily of oil based on refined mineral oil, and selected antirust, anti-old, anti-bubble, the composite additive such as anti-oxidant, wear-resistant, form through scientific formula mediation.And the total loss system oil be in harmonious proportion by Reclaimed Base Oil rarely has report.As everyone knows, China's oil production accounts for 2 percent of petroleum products total amount, and quantity is every year more than ten million ton.If waste lubricating oil is discarded in environment and goes, severe contamination will be caused to environment.Therefore waste lubricant oil regeneration is reasonable energy utilization, the inexorable trend of recycling economy development.
The present invention just resource gradually with shortage, under country actively advocates the situation of refuse reclamation, the total loss system oil that Fu Ke oil product limited-liability company utilizes reclaimed lubricating base oil to prepare, this product is mainly used in, to the total loss oiling system of lubricating oil without particular requirement, not being suitable for circulation lubrication system.
Summary of the invention
The object of the invention is to: provide a kind of and utilize reclaimed lubricating base oil and the total loss system oil of producing, meet the total loss system oil performance requriements of each rank.
The object of the present invention is achieved like this: a kind of total loss system oil composition utilizing recovered oil to produce, and this lubricating oil is become by following raw materials in parts by weight array: Reclaimed Base Oil: 100.0 parts, viscosity modifier: 0.01-10.0 part, purification agent: 0.01-10.0 part, dispersion agent: 0.01-5.0 part, oxidation and corrosion inhibitor 0.5-3.0 part, extreme pressure agent: 0.01-10.0 part, rust-preventive agent: 0.5-3.0 part, defoamer: 0.0001-0.01 part.
Know-why of the present invention and beneficial effect: regeneration is carried out to waste lubricating oil, not only protection of the environment, and economize on resources, the reclaimed lubricating base oil viscosity index utilizing Fu Ke oil product limited-liability company to produce is high, and outward appearance is well-illuminated transparent, modest viscosity; Viscosity modifier is selected to have good thickening and low-temperature performance; Purification agent is selected to have significant detergent power; Dispersion agent is selected to have excellent dispersiveness; Oxidation and corrosion inhibitor is selected to have good antioxidant-anticorrosive properties; Extreme pressure agent is selected to have good abrasion resistant extreme-pressure ability; Rust-preventive agent is selected to have significant corrosion resistance; Select defoamer to have defoaming, can adjust according to whipability in good time.
The lubricating oil environmental protection that the present invention produces, not only efficent use of resources, and bring huge economic benefit, the total loss system oil utilizing recovered oil to prepare, pour point is low, and flash-point is high, the excellent properties such as resistance to wear, meet every physical and chemical index of total loss system oil completely, for industry energy conservation consumption reduction serves exemplary role, show technical progress.
Embodiment
The present invention is described further in conjunction with the embodiments.
Embodiment 1
With parts by weight preparation, total loss system oil:
Formula 1:
Reclaimed Base Oil 100.0 parts, low alkali value calcium alkylbenzenesulfonate 3.0 parts, polyene-based succimide 1.5 parts, the two octyl group basic zinc salt 1.0 parts of sulphur phosphorus, N-phenyl-alpha-naphthylamine 1.0 parts, sulfide isobutene 1.5 parts, barium mahogany sulfonate 1.0 parts, methyl-silicone oil 0.0005 part.
Formula 2:
Reclaimed Base Oil 100.0 parts, middle calcium alkylbenzensulfonates 3.5 parts, diene base succimide 1.5 parts, the two octyl group basic zinc salt 1.0 parts of sulphur phosphorus, 2,6 ditertiary butyl p cresol 1.5 parts, positive 1.0 parts, the fourth fat of phosphorous acid two, sulfide isobutene 1.5 parts, neutral dinonyl naphthalene sulfonate barium 1.5 parts, methyl-silicone oil 0.0004 part.
Formula 3:
Reclaimed Base Oil 100.0 parts, ethylene-propylene copolymer 2.0 parts, sulfur phosphorization polyisobutylene titanate salt 3.0 parts, diene base succimide 2.0 parts, sulphur phosphorus secondary alcohol groups zinc salt 1.0 parts, N-phenyl-alpha-naphthylamine 1.0 parts, thiophosphoric acid phenyl ester 1.0 parts, sulfide isobutene 1.5 parts, petroleum sodium sulfonate zinc naphthenate 1.0 parts, methyl-silicone oil 0.0005 part.
Formula 4:
Reclaimed Base Oil 100.0 parts, the different monooctyl ester of polyacrylic acid 4.0 parts, low alkali value calcium alkylbenzenesulfonate 3.0 parts, polyene-based succimide 1.5 parts, sulphur phosphorus secondary alcohol groups zinc salt 1.0 parts, 2,6-ditertbutylparacresol 1.0 parts, sulphur phosphoric acid nitrogen containing derivative 1.0 parts, sulfide isobutene 1.5 parts, neutral dinonyl naphthalene sulfonate barium 1.0 parts, methyl-silicone oil 0.0005 part.
Formula 5:
Reclaimed Base Oil 100.0 parts, polymethacrylate 5.0 parts, middle calcium alkylbenzensulfonates 3.0 parts, diene base succimide 1.5 parts, the two octyl group basic zinc salt 1.5 parts of sulphur phosphorus, 1.0 parts, 124 Triazole derivative, tritolyl phosphate 1.0 parts, sulfide isobutene 1.5 parts, petroleum sodium sulfonate zinc naphthenate 1.0 parts, methyl-silicone oil 0.0004 part.
Above-mentioned preparation 1), 2), 3) ... select its 1, prepare total loss system oil.
Wherein Reclaimed Base Oil 40 DEG C of kinematic viscosity are 4.0-220mm
2﹒ s
-1, viscosity index>=80, acid number≤2, flash-point>=180 DEG C.
Wherein the purification agent of total loss system oil comprises at least one in low alkali value calcium alkylbenzenesulfonate and/or middle calcium alkylbenzensulfonates and/or high base number calcium alkylbenzenesulfonate and/or sulfur phosphorization polyisobutylene titanate salt and/or magnesium naphthenate.
Wherein the dispersion agent of total loss system oil is at least one in diene base succimide and/or polyene-based succimide and/or high molecular succimide.
Wherein the oxidation and corrosion inhibitor of total loss system oil is at least one in the two octyl group basic zinc salt of sulphur phosphorus or sulphur phosphorus brothers alcohol radical zinc salt or sulphur phosphorus secondary alcohol groups zinc salt and/or 2,6 ditertiary butyl p cresol and/or N-phenyl-alpha-naphthylamine and/or 124 Triazole derivative.
Wherein the extreme pressure agent of total loss system oil is at least one in the positive fourth fat of phosphorous acid two or sulphur phosphoric acid nitrogen containing derivative and/or tritolyl phosphate and/or thiophosphoric acid amine salt and/or thiophosphoric acid phenyl ester and/or sulfide isobutene and/or phosphorous acid diisobutyl ester.
Wherein the rust-preventive agent of total loss system oil is at least one in barium mahogany sulfonate and/or petroleum sodium sulfonate zinc naphthenate and/or neutral dinonyl naphthalene sulfonate barium and/or alkenyl succinic acid and/or alkenyl succinic acid ester.
Wherein the viscosity modifier of total loss system oil is at least one in polyvinyl n-butyl ether and/or ethylene-propylene copolymer and/or polymethacrylate and/or the different monooctyl ester of polyacrylic acid.
In example, every physicochemical property, sees attached list.
| Project | Preparation 1(7#) | Preparation 2(15#) | Preparation 3(32#) | Preparation 4(46#) | Preparation 5 (68#) | Method |
| 40 DEG C of kinematic viscosity/mm 2﹒s -1 | 7.15 | 15.62 | 33.74 | 48.98 | 71.95 | GB/T 265 |
| Ash content/% | 0.001 | 0.002 | 0.001 | 0.001 | 0.002 | GB/T 1995 |
| Flash-point (opening)/DEG C | 227 | 200 | 255 | 220 | 215 | GB/T 3536 |
| Pour point/DEG C | -27 | -21 | -18 | -15 | -15 | GB/T 3535 |
| Copper corrosion (100 DEG C, 3h)/level | Qualified | Qualified | Qualified | Qualified | Qualified | GB/T 5096 |
| Mechanical impurity/% (m/m) | Nothing | 0.002 | 0.003 | 0.001 | 0.0015 | GB/T 511 |
| Acid number/(mgKOH/g) | 0.04 | 0.02 | 0.03 | 0.03 | 0.04 | GB/T 264 |
| Moisture content/% | Nothing | Nothing | Nothing | Nothing | Nothing | GB/T 260 |
| Water soluble acid or alkali | Nothing | Nothing | Nothing | Nothing | Nothing | GB/T 259 |
As can be seen from the table, the total loss system oil pour point utilizing Reclaimed Base Oil to produce is low, and flash-point is high, meets the performance requriements that total loss system oil viscosity grade is 5,7,10,15,22,32,46,68,100,150 completely.
The national standard of product of the present invention is GB443-1989.
Reclaimed Base Oil is Fu Ke oil product limited-liability company commercially available prod.
The different monooctyl ester of viscosity modifier polyvinyl n-butyl ether, ethylene-propylene copolymer, polymethacrylate, polyacrylic acid is all purchased from Jinzhou Petrochemical Co.;
Purification agent low alkali value calcium alkylbenzenesulfonate, middle calcium alkylbenzensulfonates, high base number calcium alkylbenzenesulfonate are purchased from Shandong Zibo Hui Hua company limited, and sulfur phosphorization polyisobutylene titanate salt, magnesium naphthenate are purchased from Shandong Zibo Hui Hua company limited;
Dispersion agent diene base succimide, polyene-based succimide, high molecular succimide are all purchased from Shandong Zibo Hui Hua Chemical Co., Ltd.;
Oxidation and corrosion inhibitor is the two octyl group basic zinc salt of sulphur phosphorus, sulphur phosphorus brothers alcohol radical zinc salt, sulphur phosphorus secondary alcohol groups zinc salt, 2,6 ditertiary butyl p cresol, N-phenyl-alpha-naphthylamine, 124 Triazole derivative are all purchased from the emerging petroleum additive limited liability company in Jinzhou;
Extreme pressure agent phosphorous acid two positive fourth fat, sulphur phosphoric acid nitrogen containing derivative, tritolyl phosphate or thiophosphoric acid amine salt, thiophosphoric acid phenyl ester, sulfide isobutene, phosphorous acid diisobutyl ester are all purchased from Shandong Zibo Hui Hua Chemical Co., Ltd.;
Rust-preventive agent barium mahogany sulfonate, petroleum sodium sulfonate zinc naphthenate, neutral dinonyl naphthalene sulfonate barium, alkenyl succinic acid, alkenyl succinic acid ester are all purchased from the emerging petroleum additive limited liability company in Jinzhou;
Defoamer is all purchased from Shandong Zibo Hui Hua Chemical Co., Ltd..
Claims (2)
1. the total loss system oil composition utilizing recovered oil to produce, is characterized in that: this lubricating oil is become by following raw materials in parts by weight array: by Reclaimed Base Oil: 100.0 parts, viscosity modifier: 0.01-10.0 part, purification agent: 0.01-10.0 part, dispersion agent: 0.01-5.0 part, oxidation and corrosion inhibitor 0.5-3.0 part, extreme pressure agent: 0.01-10.0 part, rust-preventive agent: 0.5-3.0 part, defoamer: 0.0001-0.01 part.
2. total loss system oil according to claim 1, is characterized in that: Reclaimed Base Oil 40 DEG C of kinematic viscosity are 4.0-220mm
2﹒ s
-1, viscosity index>=80, acid number≤2, flash-point>=180 DEG C.
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1511931A (en) * | 2000-12-08 | 2004-07-14 | 申保安 | Full loss mechanical lubricating oil |
| CN101033433A (en) * | 2007-04-14 | 2007-09-12 | 中国石油化工集团公司 | Regeneration method for waste lubricating oil |
| CN103820201A (en) * | 2014-03-07 | 2014-05-28 | 淄博铁宇机车修理有限公司 | Technology and device for regenerating waste mechanical lubricant by four-stage short range distillation |
| CN103849455A (en) * | 2014-03-05 | 2014-06-11 | 重庆工商大学 | Method of reproducing lightly-degraded lubricating oil |
-
2015
- 2015-01-28 CN CN201510041625.7A patent/CN104673462B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1511931A (en) * | 2000-12-08 | 2004-07-14 | 申保安 | Full loss mechanical lubricating oil |
| CN101033433A (en) * | 2007-04-14 | 2007-09-12 | 中国石油化工集团公司 | Regeneration method for waste lubricating oil |
| CN103849455A (en) * | 2014-03-05 | 2014-06-11 | 重庆工商大学 | Method of reproducing lightly-degraded lubricating oil |
| CN103820201A (en) * | 2014-03-07 | 2014-05-28 | 淄博铁宇机车修理有限公司 | Technology and device for regenerating waste mechanical lubricant by four-stage short range distillation |
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