CN104666226B - A kind of floral water containing pummelo peel extract and preparation method thereof - Google Patents
A kind of floral water containing pummelo peel extract and preparation method thereof Download PDFInfo
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- CN104666226B CN104666226B CN201510123575.7A CN201510123575A CN104666226B CN 104666226 B CN104666226 B CN 104666226B CN 201510123575 A CN201510123575 A CN 201510123575A CN 104666226 B CN104666226 B CN 104666226B
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- 244000276331 Citrus maxima Species 0.000 title claims abstract description 109
- 235000001759 Citrus maxima Nutrition 0.000 title claims abstract description 105
- 239000000284 extract Substances 0.000 title claims abstract description 83
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 74
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 238000000605 extraction Methods 0.000 title abstract description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 102
- MGSRCZKZVOBKFT-UHFFFAOYSA-N thymol Chemical compound CC(C)C1=CC=C(C)C=C1O MGSRCZKZVOBKFT-UHFFFAOYSA-N 0.000 claims abstract description 28
- 206010004542 Bezoar Diseases 0.000 claims abstract description 16
- 239000008367 deionised water Substances 0.000 claims abstract description 16
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 16
- 238000000034 method Methods 0.000 claims abstract description 16
- 239000000049 pigment Substances 0.000 claims abstract description 16
- DTGKSKDOIYIVQL-WEDXCCLWSA-N (+)-borneol Chemical compound C1C[C@@]2(C)[C@@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-WEDXCCLWSA-N 0.000 claims abstract description 15
- REPVLJRCJUVQFA-UHFFFAOYSA-N (-)-isopinocampheol Natural products C1C(O)C(C)C2C(C)(C)C1C2 REPVLJRCJUVQFA-UHFFFAOYSA-N 0.000 claims abstract description 15
- 241000270295 Serpentes Species 0.000 claims abstract description 15
- 229940116229 borneol Drugs 0.000 claims abstract description 15
- CKDOCTFBFTVPSN-UHFFFAOYSA-N borneol Natural products C1CC2(C)C(C)CC1C2(C)C CKDOCTFBFTVPSN-UHFFFAOYSA-N 0.000 claims abstract description 15
- DTGKSKDOIYIVQL-UHFFFAOYSA-N dl-isoborneol Natural products C1CC2(C)C(O)CC1C2(C)C DTGKSKDOIYIVQL-UHFFFAOYSA-N 0.000 claims abstract description 15
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 claims abstract description 14
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000005844 Thymol Substances 0.000 claims abstract description 14
- 229940041616 menthol Drugs 0.000 claims abstract description 14
- 229960000790 thymol Drugs 0.000 claims abstract description 14
- 238000005238 degreasing Methods 0.000 claims abstract description 12
- 238000001914 filtration Methods 0.000 claims abstract description 12
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 12
- 238000007710 freezing Methods 0.000 claims description 9
- 230000008014 freezing Effects 0.000 claims description 9
- 239000003208 petroleum Substances 0.000 claims description 8
- 239000000084 colloidal system Substances 0.000 claims description 7
- 238000007599 discharging Methods 0.000 claims description 5
- 210000003934 vacuole Anatomy 0.000 claims description 5
- 238000005259 measurement Methods 0.000 claims description 4
- 239000000706 filtrate Substances 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 238000002525 ultrasonication Methods 0.000 claims description 2
- 238000002604 ultrasonography Methods 0.000 claims 2
- 239000000341 volatile oil Substances 0.000 abstract description 6
- 229930003944 flavone Natural products 0.000 abstract description 5
- 235000011949 flavones Nutrition 0.000 abstract description 5
- 240000000560 Citrus x paradisi Species 0.000 abstract description 4
- 230000000694 effects Effects 0.000 abstract description 4
- 241000255925 Diptera Species 0.000 abstract description 3
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 abstract description 3
- -1 flavone compounds Chemical class 0.000 abstract description 3
- 239000003205 fragrance Substances 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 abstract description 3
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 abstract description 3
- 241000238631 Hexapoda Species 0.000 abstract description 2
- 230000002265 prevention Effects 0.000 abstract description 2
- 230000001846 repelling effect Effects 0.000 abstract description 2
- 238000002137 ultrasound extraction Methods 0.000 abstract 1
- 238000007781 pre-processing Methods 0.000 description 9
- 238000004519 manufacturing process Methods 0.000 description 6
- HIXDQWDOVZUNNA-UHFFFAOYSA-N 2-(3,4-dimethoxyphenyl)-5-hydroxy-7-methoxychromen-4-one Chemical compound C=1C(OC)=CC(O)=C(C(C=2)=O)C=1OC=2C1=CC=C(OC)C(OC)=C1 HIXDQWDOVZUNNA-UHFFFAOYSA-N 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- 235000013399 edible fruits Nutrition 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000003921 oil Substances 0.000 description 4
- 235000010987 pectin Nutrition 0.000 description 4
- 239000001814 pectin Substances 0.000 description 4
- 229920001277 pectin Polymers 0.000 description 4
- 239000004744 fabric Substances 0.000 description 3
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 150000002213 flavones Chemical class 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 150000002576 ketones Chemical class 0.000 description 2
- 238000011031 large-scale manufacturing process Methods 0.000 description 2
- 235000000882 Citrus x paradisi Nutrition 0.000 description 1
- 241000167847 Koelreuteria paniculata Species 0.000 description 1
- 240000002853 Nelumbo nucifera Species 0.000 description 1
- 235000006508 Nelumbo nucifera Nutrition 0.000 description 1
- 235000006510 Nelumbo pentapetala Nutrition 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 240000002657 Thymus vulgaris Species 0.000 description 1
- 235000007303 Thymus vulgaris Nutrition 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000003266 anti-allergic effect Effects 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 235000013325 dietary fiber Nutrition 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 239000000077 insect repellent Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 210000003739 neck Anatomy 0.000 description 1
- 235000008935 nutritious Nutrition 0.000 description 1
- 230000001151 other effect Effects 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 230000005070 ripening Effects 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000001585 thymus vulgaris Substances 0.000 description 1
- 238000001291 vacuum drying Methods 0.000 description 1
- 238000013022 venting Methods 0.000 description 1
- 238000003809 water extraction Methods 0.000 description 1
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- Cosmetics (AREA)
- Medicinal Preparation (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses a kind of floral water containing pummelo peel extract and preparation method thereof; the component of the floral water includes ethanol, pummelo peel extract, essence, snake gall extract solution, cow-bezoar, menthol, thymol, borneol, pigment and deionized water; wherein it is using fresh grapefruit skin as raw material, by degreasing, ultrasonic extraction, filtering extraction shaddock ped active component.Through the above way, floral water containing pummelo peel extract of the present invention and preparation method thereof, contain a large amount of flavone compounds and Essential Oil From Citrus Grandis Peel in floral water containing pummelo peel extract, so that corresponding floral water has preferably fragrance and insect prevention mosquito effect, the natural fragrance and repelling effect of essential oil in natural origin raw material pomelo peel can be made full use of, prepare that the method process of floral water and pummelo peel extract is simple, and equipment requirement is low, can popularization and application.
Description
Technical field
The present invention relates to field, more particularly to a kind of floral water containing pummelo peel extract and preparation method thereof.
Background technology
Shaddock（Scientific name：Citrus maxima）It is the ripening fruits of Citrus paradisi Macfadyen, also known as pomelo, fragrant goldenrain tree, grapefruit
Deng originating in the southern areas such as China Fujian, Jiangxi, Guangdong, Guangxi, Sichuan.Its fruit sour-sweet Liang Run, it is nutritious, make us praising
Do not stop talking；Its pericarp, pomelo flower can all be used as medicine, and have the laudatory title of " natural fruit can ".Shaddock ped is rich in various active polysaccharide, Huang
The active component of the multiple beneficials such as ketone, pectin, natural pigment, essential oil health, and higher than the content in shaddock fruit.In addition, shaddock
Skin also has dispelling odor, mosquito proof and other effects, based on this feature, the natural extract can be added in mosquito-repellent perfume and sent out
Wave effect.
As a kind of important industrial crops, shaddock has large area plantation in southern region of China, and annual yield is up to
Million tons.After people eat and produce and process, the shaddock ped for still having fresh weight 20~30% can not be used shaddock.These shaddock peds
If directly thrown away as discarded object, serious pollution is not only caused to ecological environment, but also is wasted significantly rich in shaddock ped
Rich resource（Flavonoids, dietary fiber, pectin etc.）.
Chinese invention patent publication number CN1356327A discloses a kind of method that flavones is extracted from shaddock ped, is using heat
After water extraction concentration, the impurity such as pectin are removed with ethanol, then by the use of aqueous phase as medium, impurity elimination is further removed using alkali hydrolysis method
Matter, acid precipitate to obtain crude product, then are dissolved with ethanol, cold water recrystallization, and last 80 DEG C of vacuum drying obtain flavones.This method extracts work
Skill step is more, improves large-scale production cost.Chinese invention patent publication number CN102703219A discloses a kind of ice
Brilliant broken wall Essential Oil From Citrus Grandis Peel extracting method, it is that slow freezing under shaddock ped oil vacuole layer low temperature is formed into ice slag, with being solved after crusher in crushing
Freeze, then squeezed with pressafiner；Pressed liquor saltout and is evaporated under reduced pressure after layering, shaddock ped essence is obtained after last profit layering
Oil.The technological operation of this method is more complicated, and production equipment input is larger.By patent retrieval, it yet there are no and extract shaddock ped
Thing is applied to the correlative study report of floral water production.
The content of the invention
The present invention solves the technical problem of providing a kind of floral water containing pummelo peel extract and preparation method thereof,
The shaddock ped extractive technique technique is simple, cost is cheap, workable, and is applied in floral water formula.
In order to solve the above technical problems, one aspect of the present invention is：One kind is provided and contains pummelo peel extract
Floral water, it is characterised in that in terms of parts by weight, the component of the floral water is：Ethanol 55~70%, pummelo peel extract
10~30%, essence 0.1~1.0%, snake gall extract solution 0.01~0.2%, cow-bezoar 0.01~0.2%, menthol 0.1~
0.25%th, thymol 0.1~0.25%, borneol 0.01~0.2%, pigment 0.00001~0.0001%, more than deionized water
Amount.
In a preferred embodiment of the present invention, in terms of parts by weight, the component of the floral water is：Ethanol 55~
65%th, pummelo peel extract 5~25%, essence 0.5~0.9%, snake gall extract solution 0.01~0.1%, cow-bezoar 0.01~0.1%, thin
Lotus alcohol 0.13~0.20%, thymol 0.14~0.20%, borneol 0.05~0.1%, pigment 0.00001~0.0001%,
Deionized water surplus.
In a preferred embodiment of the present invention, in terms of parts by weight, the component of the floral water is：Ethanol 57%, shaddock
Bark extract 15%, essence 0.8%, snake gall extract solution 0.02%, cow-bezoar 0.02%, menthol 0.15%, thymol
0.15%th, borneol 0.06%, pigment 0.00002%, deionized water surplus.
In a preferred embodiment of the present invention, the preparation process of the pummelo peel extract is：Take the shaddock ped oil vacuole of shaddock
Layer is simultaneously soaked in petroleum ether and carries out degreasing, dries to obtain the shaddock ped filter residue after degreasing after filtering petroleum ether；After the degreasing
Shaddock ped filter residue be placed in ethanol solution, be ultrasonically treated and be filtrated to get pummelo peel extract.
In a preferred embodiment of the present invention, in the preparation process of the pummelo peel extract, the matter of the ethanol solution
It is 95% to measure fraction, and the ratio of the shaddock ped filter residue and the ethanol solution is 1g：3ml, ultrasonication be 200~
15~30min is ultrasonically treated under 300W, the filtrate after filtering is the ethanol solution of pummelo peel extract, can be directly used in floral water
Production.
A kind of preparation method of the floral water containing pummelo peel extract is provided, including step is：Carried by described containing shaddock ped
Take the component of the floral water of thing to weigh, cow-bezoar is mixed to obtain to the first solution with ethanol；By menthol, thymol, borneol and snake
Courage extract solution is mixed to get the second solution with ethanol；Essence and ethanol are mixed to get the 3rd solution；Pigment is mixed with water
To the 4th solution；First solution, the second solution, the 3rd solution, the 4th solution, pummelo peel extract and surplus second alcohol and water are mixed
Stirring obtains colloid, and the pH value of the colloid is 5.0~7.0, obtains the floral water containing pummelo peel extract.
In a preferred embodiment of the present invention, the ratio of the cow-bezoar and the ethanol is 1：200~300, described
For one solution using preceding being filtered, it is 10%~20% to prepare the ethanol weight ratio being put into the second solution, prepares the 3rd solution
In the ethanol weight ratio that is put into be 1~10%, it is described obtain the floral water containing pummelo peel extract process be：It is first molten by first
In liquid, the second solution, the 3rd solution, the 4th solution, pummelo peel extract and surplus ethanol suction refrigerating pot, add excess water and open
Freezing agitating device stirring is opened, 2~10min is first stirred, freezes 20~40min after pH value is qualified at 0 DEG C again, treat density, turbid
Filtering and discharging after degree detection is qualified.
The beneficial effects of the invention are as follows：Floral water containing pummelo peel extract of the present invention and preparation method thereof, contains shaddock
Contain a large amount of flavone compounds and Essential Oil From Citrus Grandis Peel in the floral water of bark extract so that corresponding floral water has preferably virtue
Fragrant and insect prevention mosquito effect, the natural fragrance and repelling effect of essential oil in natural origin raw material pomelo peel, system can be made full use of
The method process of standby floral water and pummelo peel extract is simple, and equipment requirement is low, can popularization and application.
Embodiment
The technical scheme in the embodiment of the present invention will be clearly and completely described below, it is clear that described implementation
Example is only the part of the embodiment of the present invention, rather than whole embodiments.It is common based on the embodiment in the present invention, this area
All other embodiment that technical staff is obtained under the premise of creative work is not made, belong to the model that the present invention protects
Enclose.
Embodiment one：
A kind of floral water containing pummelo peel extract is provided, in terms of parts by weight, the component of the floral water is：Ethanol
57%th, pummelo peel extract 15%, essence 0.8%, snake gall extract solution 0.02%, cow-bezoar 0.02%, menthol 0.15%, thyme
Phenol 0.15%, borneol 0.06%, pigment 0.00002%, deionized water surplus.
The preparation process of wherein described pummelo peel extract is：Fresh grapefruit is chosen, the shaddock ped oil vacuole layer of outer layer is stripped, discards
Pulp, shaddock ped is immersed in petroleum ether and carries out degreasing, filter naturally dry at petroleum ether rear venting；Then the shaddock after extracting degreasing
Skin filter residue, which is placed in 95% ethanol solution, to be soaked, and the ratio of shaddock ped filter residue and ethanol solution is 1g：3ml, in 200~300W bars
It is ultrasonically treated 15~30min under part to be filtered, gained filtrate is the ethanol solution of pummelo peel extract.
To obtaining the detection and analysis of the pummelo peel extract：Carry out hydrochloric acid, magnesium powder reaction：Take pummelo peel extract solution 1ml
In test tube, a small amount of magnesium powder vibration is added, 1~5 drop concentrated hydrochloric acid is added, is heated 2 minutes in water-bath, it was observed that solution colour
Laking.It is consistent to be repeated twice result.It is possible thereby to illustrate to contain active flavone compound in shaddock ped extract solution.
A kind of preparation method of the floral water containing pummelo peel extract, including step is：
（1）Cow-bezoar is accurately weighed by formula ratio in pre-processing in pot, adds 200 times of amount ethanol, turn on agitator stirring is raw
It is antenatal to use filter-cloth filtering；
（2）Menthol, thymol, borneol and snake gall extract solution are accurately weighed by formula ratio in pre-processing in pot, is added
The ethanol of 15% parts by weight, turn on agitator stirring, make its dissolving complete；
（3）Essence is accurately weighed by formula ratio in preprocessing barrel, adds the ethanol of 4% parts by weight, is sufficiently mixed
It is even；
（4）Pigment is accurately weighed by formula ratio, is dissolved with appropriate amount of deionized water, it is standby；
（5）By remaining ethanol, above-mentioned（1）~（4）Pretreated material, pummelo peel extract are drawn into refrigerating pot, are added
Balance deionized water simultaneously opens freezing agitating device, stirs 5min；
（6）Take colloid to detect pH value, need to control in the range of 5.0~7.0；
（7）Continue 0 DEG C of freezing 30min, filtering and discharging after density, Turbidity measurement are qualified.
Embodiment two：
A kind of floral water containing pummelo peel extract is provided, in terms of parts by weight, the component of the floral water is：Ethanol
62%th, pummelo peel extract 5%, essence 0.6%, snake gall extract solution 0.10%, cow-bezoar 0.02%, menthol 0.20%, thymol
0.15%th, borneol 0.06%, pigment 0.00002%, deionized water surplus.
A kind of preparation method of the floral water containing pummelo peel extract, including step is：
（1）Cow-bezoar is accurately weighed by formula ratio in pre-processing in pot, adds 200~300 times of ethanol, turn on agitator is stirred
Mix, filter-cloth filtering is used before production；
（2）Menthol, thymol, borneol and snake gall extract solution are accurately weighed by formula ratio in pre-processing in pot, is added
The ethanol of 10%~20% parts by weight, turn on agitator stirring, make its dissolving complete；
（3）Essence is accurately weighed by formula ratio in preprocessing barrel, the ethanol of 1~10% parts by weight is added, is sufficiently mixed
Uniformly；
（4）Pigment is accurately weighed by formula ratio, is dissolved with appropriate amount of deionized water, it is standby；
By remaining ethanol, above-mentioned（1）~（4）Pretreated material, pummelo peel extract are drawn into refrigerating pot, add surplus
Deionized water simultaneously opens freezing agitating device, stirs 2~10min；
Take colloid to detect pH value, need to control in the range of 5.0~7.0；
Continue 0 DEG C of 20~40min of freezing, filtering and discharging after density, Turbidity measurement are qualified.
Embodiment three：
A kind of floral water containing pummelo peel extract is provided, in terms of parts by weight, the component of the floral water is：With weight
Number meter, the component of the floral water are：Ethanol 55%, pummelo peel extract 25%, essence 0.8%, snake gall extract solution 0.02%,
Cow-bezoar 0.02%, menthol 0.14%, thymol 0.16%, borneol 0.06%, pigment 0.00002%, more than deionized water
Amount.
The preferred fabrication method of above example can be as follows：
（1）Cow-bezoar is accurately weighed by formula ratio in pre-processing in pot, adds 250 times of ethanol, turn on agitator stirring, production
It is preceding to use filter-cloth filtering；
（2）Menthol, thymol, borneol and snake gall extract solution are accurately weighed by formula ratio in pre-processing in pot, is added
The ethanol of 10% parts by weight, turn on agitator stirring, make its dissolving complete；
（3）Essence is accurately weighed by formula ratio in preprocessing barrel, adds the ethanol of 8% parts by weight, is sufficiently mixed
It is even；
（4）Pigment is accurately weighed by formula ratio, is dissolved with appropriate amount of deionized water, it is standby；
By remaining ethanol, above-mentioned（1）~（4）Pretreated material, pummelo peel extract are drawn into refrigerating pot, add surplus
Deionized water simultaneously opens freezing agitating device, stirs 10min；
Take colloid to detect pH value, need to control in the range of 5.0~7.0；
Continue 0 DEG C of freezing 30min, filtering and discharging after density, Turbidity measurement are qualified.
Pummelo peel extract process for making of the present invention is simple, and equipment requirement is low, can effectively extract effective in shaddock ped
Composition, and high-temperature operation is avoided to keep its chemism, suitable for large-scale production.Pummelo peel extract in the present invention can
Directly make the products such as floral water.
Contain pummelo peel extract in floral water of the invention containing pummelo peel extract, contain substantial amounts of Huang in pummelo peel extract
The materials such as ketone, pectin.Active component in shaddock ped not only increases dispelling odor and mosquito-proof after being matched with the formula of floral water
The effect of worm, and the multiple efficacies such as antiallergy, anti-inflammatory are also add, multifunctional cosmetics of the people to natural origin can be met
Demand.
Embodiments of the invention are the foregoing is only, are not intended to limit the scope of the invention, it is every to utilize this hair
The equivalent structure or equivalent flow conversion that bright description is made, or directly or indirectly it is used in other related technology necks
Domain, it is included within the scope of the present invention.
Claims (6)
1. a kind of floral water containing pummelo peel extract, it is characterised in that in terms of parts by weight, the component of the floral water is：
Ethanol 55~70%, pummelo peel extract 10~30%, essence 0.1~1.0%, snake gall extract solution 0.01~0.2%,
Cow-bezoar 0.01~0.2%, menthol 0.1~0.25%, thymol 0.1~0.25%, borneol 0.01~
0.2%th, pigment 0.00001~0.0001%, deionized water surplus；
The preparation process of the pummelo peel extract is：Take the shaddock ped oil vacuole layer of shaddock and be soaked in petroleum ether and carry out degreasing, filter
Dry to obtain the shaddock ped filter residue after degreasing after falling petroleum ether；Shaddock ped filter residue after the degreasing is placed in ethanol solution, ultrasound
Handle and be filtrated to get pummelo peel extract.
2. a kind of floral water containing pummelo peel extract, it is characterised in that in terms of parts by weight, the component of the floral water is：
Ethanol 55~65%, pummelo peel extract 5~25%, essence 0.5~0.9%, snake gall extract solution 0.01~0.1%, ox
Huang 0.01~0.1%, menthol 0.13~0.20%, thymol 0.14~0.20%, borneol 0.05~0.1%,
Pigment 0.00001~0.0001%, deionized water surplus；
The preparation process of the pummelo peel extract is：Take the shaddock ped oil vacuole layer of shaddock and be soaked in petroleum ether and carry out degreasing, filter
Dry to obtain the shaddock ped filter residue after degreasing after falling petroleum ether；Shaddock ped filter residue after the degreasing is placed in ethanol solution, ultrasound
Handle and be filtrated to get pummelo peel extract.
3. the floral water according to claim 2 containing pummelo peel extract, it is characterised in that described in terms of parts by weight
The component of floral water is：Ethanol 57%, pummelo peel extract 15%, essence 0.8%, snake gall extract solution 0.02%, cow-bezoar 0.02%,
Menthol 0.15%, thymol 0.15%, borneol 0.06%, pigment 0.00002%, deionized water surplus.
4. the floral water according to claim 1 containing pummelo peel extract, it is characterised in that the quality of the ethanol solution
Fraction is 95%, and the ratio of the shaddock ped filter residue and the ethanol solution is 1g：3ml, ultrasonication be 200~
15~30min is ultrasonically treated under 300W, the filtrate after filtering is the ethanol solution of pummelo peel extract, can be directly used in flower
Dew produces.
5. according to the preparation method of any described floral water containing pummelo peel extract of claim 1-3, it is characterised in that
It is including step：Weighed by the component of any floral water containing pummelo peel extract of claim 1-3, by cow-bezoar and second
Alcohol mixes to obtain the first solution；Menthol, thymol, borneol and snake gall extract solution and ethanol are mixed to get the second solution；Will
Essence is mixed to get the 3rd solution with ethanol；Pigment and water are mixed to get the 4th solution；By the first solution, the second solution,
Three solution, the 4th solution, pummelo peel extract and surplus second alcohol and water mix to obtain colloid, and the pH values of the colloid are 5.0
~7.0, obtain the floral water containing pummelo peel extract.
6. the preparation method of the floral water according to claim 5 containing pummelo peel extract, it is characterised in that the cow-bezoar
Ratio with the ethanol is 1：200~300, first solution is prepared and put in the second solution using preceding being filtered
The ethanol weight ratio entered is 10%~20%, and it is 1~10% to prepare the ethanol weight ratio being put into the 3rd solution, described to obtain
The process of floral water containing pummelo peel extract is：First the first solution, the second solution, the 3rd solution, the 4th solution, shaddock ped are carried
Take thing and surplus ethanol to suck in refrigerating pot, add excess water and open freezing agitating device stirring, first stir 2~10min,
Freeze 20~40min, the filtering and discharging after density, Turbidity measurement are qualified after pH value is qualified at 0 DEG C again.
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| CN105380857B (en) * | 2015-12-07 | 2018-06-22 | 青蛙王子(中国)日化有限公司 | A kind of long-acting children's mosquito-repellent paste and preparation method thereof |
| CN105851081A (en) * | 2016-05-06 | 2016-08-17 | 遵义医学院 | Mosquito-repelling essential oil |
| CN108096163A (en) * | 2017-12-20 | 2018-06-01 | 石永明 | A kind of facial mask with antipyretic and antidote functions |
| CN111012724A (en) * | 2019-12-31 | 2020-04-17 | 福建省梦娇兰日用化学品有限公司 | Children floral water prepared by plant active ingredient degreasing extraction technology |
| CN113304072B (en) * | 2021-05-26 | 2023-04-21 | 建昌帮药业有限公司 | Floral water |
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| CN103230351A (en) * | 2013-04-28 | 2013-08-07 | 马瑞 | All natural mosquito repel |
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| "柚皮总黄酮超声波辅助提取工艺的研究";仇燕，等;《河北科技大学学报》;20100831;第31卷(第4期);第330-333页 * |
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