CN104645886A - Vulcanization bed for synthesizing organic silicon - Google Patents
Vulcanization bed for synthesizing organic silicon Download PDFInfo
- Publication number
- CN104645886A CN104645886A CN201510080335.3A CN201510080335A CN104645886A CN 104645886 A CN104645886 A CN 104645886A CN 201510080335 A CN201510080335 A CN 201510080335A CN 104645886 A CN104645886 A CN 104645886A
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- CN
- China
- Prior art keywords
- piston
- screw thread
- nut
- center
- silicon
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/24—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/008—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic System
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/12—Organo silicon halides
- C07F7/16—Preparation thereof from silicon and halogenated hydrocarbons direct synthesis
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00796—Details of the reactor or of the particulate material
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Heating, Cooling, Or Curing Plastics Or The Like In General (AREA)
Abstract
The invention discloses a vulcanization bed for synthesizing organic silicon. The vulcanization bed comprises a worktable, and comprises a main cylinder, a piston cylinder, a unidirectional material feeding box, a unidirectional air inlet pipe, an electromagnetic coil, a motor, a feeding nut, a screw rod and a piston, wherein the piston is pushed to move leftwards to exhaust all air in the piston cylinder; then the piston cylinder is sealed and the motor and the feeding nut rotate; under the connection effect of the screw rod, the piston moves rightwards, and a sealed space formed by the piston and the main cylinder is in a vacuum state; under the action of the air pressure, methane chloride is sucked from the unidirectional air inlet pipe and silicon powder enters the piston cylinder from the unidirectional material feeding box; the silicon powder is suspended in the piston cylinder; when the piston moves leftwards, the air inlet pipe and the unidirectional material feeding box are automatically closed so that the sealed space is formed; the piston moves leftwards and the air pressure of the sealed space is increased, so that the silicon powder and methane chloride can be completely synthesized into organic silicon; and the utilization rate of materials is improved, the production efficiency is improved, and the production cost is reduced.
Description
Technical field
The present invention relates to a kind of fluid bed, particularly relate to a kind of vulcanization bed of synthesizing organo-silicon.
Background technology
Organosilicon is a large amount of a kind of organic material used in the various industry of life, and organosilicon is silicon and organic synthesis, current synthesizing organo-silicon synthesizes in high pressure and high temperature with silica flour and monochloro methane, and existing technology is making high-pressure space, after heating to high-pressure space, a certain proportion of monochloro methane of injection and silica flour are to high-pressure space again, but other gas or air must be added while being produced on high-pressure space again, monochloro methane can be caused like this to dilute, monochloro methane and silica flour is caused to synthesize not exclusively, waste material, increase processing cost, in view of above-mentioned defect, be necessary the vulcanization bed designing a kind of synthesizing organo-silicon in fact.
Summary of the invention
Technical problem to be solved by this invention is: the vulcanization bed providing a kind of synthesizing organo-silicon, solves existing technology synthetic reaction incomplete, causes the problem that cost increases.
For solving the problems of the technologies described above, technical scheme of the present invention is: a kind of vulcanization bed of synthesizing organo-silicon, comprise workbench, comprise Master cylinder body, piston cylinder, unidirectional feed tank, unidirectional air inlet pipe, solenoid, motor, feed nut, screw rod, piston, described Master cylinder body is arranged in bench-top place, the two screw thread is connected, described piston cylinder is positioned at Master cylinder body inside center place, the two screw thread is connected, described unidirectional feed tank is positioned at Master cylinder body top center left end, the two screw thread is connected, described air inlet pipe is positioned at Master cylinder body left end center, the two is weldingly connected, described solenoid is positioned at center, piston cylinder outer end, it is connected with Master cylinder body screw thread.Described motor is positioned at bench-top central right, the two screw thread is connected, described feed nut is positioned at Master cylinder body right-hand member center, the two screw thread is connected, described screw rod is positioned at feed nut center, the two screw thread is connected, described piston is positioned at screw rod left end center, and the two screw thread is connected.
Further, described feed nut contains nut seat, bearing, nut, driven synchronizing wheel.
Further, described nut seat is positioned at Master cylinder body right-hand member center, and the two screw thread is connected.
Further, described bearing is positioned at nut seat inside center place, and the two close-fitting is connected.
Further, described nut is positioned at nut seat inside center place, and it is connected with bearing close-fitting.
Further, described driven synchronizing wheel is positioned at nut right-hand member center, and the two screw thread is connected.
Further, described motor left end center is also provided with synchronizing wheel, and it is connected with driven synchronizing wheel Timing Belt, is connected with motor screw thread.
Compared with prior art, air in piston cylinder is all discharged toward left movement by promoting piston, again piston cylinder is sealed, motorized feed nut rotates, under the connection function of screw rod, piston is turned right motion, the enclosure space that piston and Master cylinder body form is in vacuum state, under the influence of air pressure, monochloro methane sucks from unidirectional air inlet pipe, silica flour enters in piston cylinder from unidirectional feed tank, and make silica flour be suspended in piston cylinder, when piston is toward left movement, air inlet pipe and unidirectional feed tank are closed automatically, thus form the space closed, piston makes the air pressure of enclosure space increase toward left movement, thus make silica flour and the complete synthesizing organo-silicon of monochloro methane, improve the utilization rate of material, with improve production efficiency, reduce production cost.
Accompanying drawing explanation
Fig. 1 is the sectional view of fluid bed
Fig. 2 is the partial view of fluid bed
Workbench 1 Master cylinder body 2
The unidirectional feed tank 4 of piston cylinder 3
One-way exhaust pipe 5 induction coil 6
Motor 7 feed nut 8
Screw rod 9 piston 10
Synchronous pulley 701 nut seat 801
Bearing 802 nut 803
Driven synchronizing wheel 804
Following detailed description of the invention will further illustrate in conjunction with above-mentioned accompanying drawing.
Detailed description of the invention
Hereinafter, set forth multiple specific detail, to provide the thorough understanding to the concept forming described embodiment basis.But to one skilled in the art, embodiment described obviously can be put into practice when not have in these specific detail some or all.In other cases, well-known treatment step is not specifically described.
As Fig. 1, shown in Fig. 2, comprise workbench 1, Master cylinder body 2, piston cylinder 3, unidirectional feed tank 4, unidirectional air inlet pipe 5, solenoid 6, motor 7, feed nut 8, screw rod 9, piston 10, described Master cylinder body 2 is positioned at workbench 1 top Zhong Chu, the two screw thread is connected, described piston cylinder 3 is positioned at Master cylinder body 2 inside center place, the two screw thread is connected, described unidirectional feed tank 4 is positioned at Master cylinder body 2 top center left end, the two screw thread is connected, described unidirectional air inlet pipe 5 is positioned at Master cylinder body 2 left end center, the two is weldingly connected, described solenoid 6 is positioned at center, piston cylinder 3 outer end, it is connected with Master cylinder body 2 screw thread.Described motor 7 is positioned on the right side of workbench 1 top center, the two screw thread is connected, described feed nut 8 is positioned at Master cylinder body 2 right-hand member center, the two screw thread is connected, described screw rod 9 is positioned at feed nut 8 center, the two screw thread is connected, described piston 10 is positioned at screw rod 9 left end center, the two screw thread is connected, described feed nut 8 contains nut seat 801, bearing 802, nut 803, driven synchronizing wheel 804, described nut seat 801 is positioned at Master cylinder body 2 right-hand member center, the two screw thread is connected, described bearing 802 is positioned at nut seat 801 inside center place, the two close-fitting is connected, described nut 803 is positioned at nut seat 801 inside center place, it is connected with bearing 802 close-fitting, described driven synchronizing wheel 804 is positioned at nut 803 right-hand member center, the two screw thread is connected, described motor 7 left end center is also provided with synchronizing wheel 701, it is connected with driven synchronizing wheel 804 Timing Belt, be connected with motor 7 screw thread, wherein unidirectional loader 4 is provided with check valve in its bottom, under the influence of air pressure, silica flour flows out from unidirectional feed tank, then automatically close when inverted, and seal, unidirectional air inlet pipe 5 principle is with unidirectional loader 4, piston cylinder 3 is joined with piston 10 is sliding, and form a closed space, motor 7 can drive synchronizing wheel 701 to rotate, synchronizing wheel 701 is connected with synchronous belt with driven synchronizing wheel 804, thus drive nut 804 to rotate, nut 803 engages with screw rod 9, screw rod 9 can be made to move left and right, thus promotion piston 10 acts on slip in piston cylinder 3, its middle (center) bearing 802 is more smooth and easy when nut 803 is rotated.This device is all discharged by the air in piston cylinder 3 toward left movement by promoting piston 10, again piston cylinder 3 is sealed, motor 7 drives feed nut 8 to rotate, under the connection function of screw rod 9, piston 10 is turned right motion, the enclosure space that piston 10 and piston cylinder form, and be in vacuum state, under the influence of air pressure, monochloro methane sucks from unidirectional air inlet pipe 5, silica flour enters in piston cylinder 3 from unidirectional feed tank 4, and make silica flour be suspended in piston cylinder 3, when piston 10 is toward left movement, unidirectional air inlet pipe 5 and unidirectional feed tank 4 are closed automatically, thus form the space closed, piston 10 makes the air pressure of enclosure space increase toward left movement, thus make silica flour and the complete synthesizing organo-silicon of monochloro methane, improve the utilization rate of material, with improve production efficiency, reduce production cost.
The present invention is not limited to above-mentioned concrete embodiment, and those of ordinary skill in the art is from above-mentioned design, and without performing creative labour, all conversion made, all drop within protection scope of the present invention.
Claims (7)
1. the vulcanization bed of a synthesizing organo-silicon, comprise workbench, it is characterized in that comprising Master cylinder body, piston cylinder, unidirectional feed tank, unidirectional air inlet pipe, solenoid, motor, feed nut, screw rod, piston, described Master cylinder body is arranged in bench-top place, the two screw thread is connected, described piston cylinder is positioned at Master cylinder body inside center place, the two screw thread is connected, described unidirectional feed tank is positioned at Master cylinder body top center left end, the two screw thread is connected, described unidirectional air inlet pipe is positioned at Master cylinder body left end center, the two is weldingly connected, described solenoid is positioned at center, piston cylinder outer end, it is connected with Master cylinder body screw thread.Described motor is positioned at bench-top central right, the two screw thread is connected, described feed nut is positioned at Master cylinder body right-hand member center, the two screw thread is connected, described screw rod is positioned at feed nut center, the two screw thread is connected, described piston is positioned at screw rod left end center, and the two screw thread is connected.
2. the vulcanization bed of a kind of synthesizing organo-silicon as claimed in claim 1, is characterized in that described feed nut contains nut seat, bearing, nut, driven synchronizing wheel.
3. the vulcanization bed of a kind of synthesizing organo-silicon as claimed in claim 2, is characterized in that described nut seat is positioned at Master cylinder body right-hand member center, and the two screw thread is connected.
4. the vulcanization bed of a kind of synthesizing organo-silicon as claimed in claim 3, is characterized in that described bearing is positioned at nut seat inside center place, and the two close-fitting is connected.
5. the vulcanization bed of a kind of synthesizing organo-silicon as claimed in claim 4, it is characterized in that described nut is positioned at nut seat inside center place, it is connected with bearing close-fitting.
6. the vulcanization bed of a kind of synthesizing organo-silicon as claimed in claim 5, is characterized in that described driven synchronizing wheel is positioned at nut right-hand member center, and the two screw thread is connected.
7. the vulcanization bed of a kind of synthesizing organo-silicon as claimed in claim 6, it is characterized in that described motor left end center is also provided with synchronizing wheel, it is connected with driven synchronizing wheel Timing Belt, is connected with motor screw thread.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510080335.3A CN104645886A (en) | 2015-02-12 | 2015-02-12 | Vulcanization bed for synthesizing organic silicon |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510080335.3A CN104645886A (en) | 2015-02-12 | 2015-02-12 | Vulcanization bed for synthesizing organic silicon |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104645886A true CN104645886A (en) | 2015-05-27 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510080335.3A Withdrawn CN104645886A (en) | 2015-02-12 | 2015-02-12 | Vulcanization bed for synthesizing organic silicon |
Country Status (1)
| Country | Link |
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| CN (1) | CN104645886A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105890297A (en) * | 2016-04-10 | 2016-08-24 | 安徽众尚微波科技有限公司 | Continuous microwave vacuum drying/sterilizing processing equipment |
| CN109404533A (en) * | 2017-08-16 | 2019-03-01 | 平高集团有限公司 | Worm drive structure for the fine tuning of pressure vessel inner components |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1343670A (en) * | 2001-10-19 | 2002-04-10 | 清华大学 | Process and system for synthesizing organosilicon monomer by direct method |
| CN1625437A (en) * | 2001-03-07 | 2005-06-08 | 洋马株式会社 | Reaction system of organic substance employing supercritical fluid or sub-critical fluid |
| CN202638402U (en) * | 2012-06-15 | 2013-01-02 | 江苏科圣化工机械有限公司 | Organosilicone fluidized bed reactor |
-
2015
- 2015-02-12 CN CN201510080335.3A patent/CN104645886A/en not_active Withdrawn
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1625437A (en) * | 2001-03-07 | 2005-06-08 | 洋马株式会社 | Reaction system of organic substance employing supercritical fluid or sub-critical fluid |
| CN1343670A (en) * | 2001-10-19 | 2002-04-10 | 清华大学 | Process and system for synthesizing organosilicon monomer by direct method |
| CN202638402U (en) * | 2012-06-15 | 2013-01-02 | 江苏科圣化工机械有限公司 | Organosilicone fluidized bed reactor |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105890297A (en) * | 2016-04-10 | 2016-08-24 | 安徽众尚微波科技有限公司 | Continuous microwave vacuum drying/sterilizing processing equipment |
| CN109404533A (en) * | 2017-08-16 | 2019-03-01 | 平高集团有限公司 | Worm drive structure for the fine tuning of pressure vessel inner components |
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| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20150527 |