CN104645884A - Thermal synthesis device of organic silicon - Google Patents
Thermal synthesis device of organic silicon Download PDFInfo
- Publication number
- CN104645884A CN104645884A CN201510080289.7A CN201510080289A CN104645884A CN 104645884 A CN104645884 A CN 104645884A CN 201510080289 A CN201510080289 A CN 201510080289A CN 104645884 A CN104645884 A CN 104645884A
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- piston
- cylinder body
- master cylinder
- screw thread
- synthesis device
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
- B01J3/04—Pressure vessels, e.g. autoclaves
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic System
- C07F7/02—Silicon compounds
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- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Reciprocating Pumps (AREA)
Abstract
The invention discloses a thermal synthesis device of organic silicon. The thermal synthesis device of organic silicon comprises a work bench, a support frame, a main cylinder body, a piston cylinder, a one-way feeder, an exhaust tube, a motor, a cam, a piston, a spring, a discharge pipe, a storage tank and a hot oil pump. Compared with the prior art, all air in the piston cylinder is completely discharged by pushing the piston to move towards the left; the piston cylinder is sealed; the hot oil is pumped into the main cylinder body by the hot oil pump, so that the temperature in the piston cylinder reaches the synthesis temperature of the organic silicon; the piston moves towards the right; a blocked space composed of the piston and the main cylinder body is in a vacuum state; methane chloride is absorbed from the exhaust pipe under the action of air pressure; silicon powder is fed to the piston cylinder from an automatic feeder; the piston moves towards the left when a certain amount is reached; the exhaust pipe and the one-way feeder are automatically closed, so as to form the blocked space; the piston moves towards the left; and the air pressure in the blocked space is increased, so that the silicon powder and the methane chloride are completely synthesized into the organic silicon; the utilization rate of materials is increased; and the production cost is reduced.
Description
Technical field
The present invention relates to a kind of synthesizer, particularly relate to a kind of organosilicon thermal synthesis device.
Background technology
Organosilicon is a large amount of a kind of organic material used in the various industry of life, and organosilicon is silicon and organic synthesis, current synthesizing organo-silicon synthesizes in high pressure and high temperature with silica flour and monochloro methane, and existing technology is making high-pressure space, after heating to high-pressure space, a certain proportion of monochloro methane of injection and silica flour are to high-pressure space again, but other gas or air must be added while being produced on high-pressure space again, monochloro methane can be caused like this to dilute, monochloro methane and silica flour is caused to synthesize not exclusively, waste material, increase processing cost, in view of above-mentioned defect, be necessary to design a kind of organosilicon thermal synthesis device in fact.
Summary of the invention
Technical problem to be solved by this invention is: provide a kind of organosilicon thermal synthesis device, solves existing technology synthetic reaction incomplete, causes the problem that cost increases.
For solving the problems of the technologies described above, technical scheme of the present invention is: a kind of organosilicon thermal synthesis device, comprise workbench, bracing frame, comprise Master cylinder body, piston cylinder, unidirectional feed appliance, exhaust tube, motor, cam, piston, spring, drainage conduit, material storing box, hot oil pump, described Master cylinder body is arranged in bench-top place, the two screw thread is connected, described piston cylinder is positioned at Master cylinder body center, the two is weldingly connected, described unidirectional feed appliance is positioned at Master cylinder body top center left end, the two screw thread is connected, described exhaust tube is positioned at Master cylinder body left end center, the two is weldingly connected, described motor is positioned at bracing frame top center place, the two screw thread is connected, described cam is positioned at center, motor front end, the two screw thread is connected, described piston is positioned at piston cylinder inside center place, the two close-fitting is connected, described spring is positioned at piston left end center, it is connected with piston cylinder screw thread, described drainage conduit is positioned at Master cylinder body bottom centre left end, the two is weldingly connected, described material storing box is positioned at Master cylinder body Left-side center place, it is connected with workbench screw thread, be connected with drainage conduit oil pipe, described hot oil pump is positioned at Master cylinder body Left-side center place, it is connected with Master cylinder body oil pipe, be connected with workbench screw thread.
Further, also hot flow path is provided with in the middle of described piston cylinder and Master cylinder body.
Further, be also provided with sliding sleeve in the middle of described piston and Master cylinder body, it was connected with piston sliding joining, and was connected with Master cylinder body screw thread.
Further, described piston right-hand member center is also provided with roller, and the two screw thread is connected.
Further, described place of drainage conduit bottom centre also establishes manually-operated gate, and the two screw thread is connected.
Further, be also provided with induction coil in the middle of described heating oil pump, the two is weldingly connected.
Compared with prior art, air in piston cylinder is all discharged toward left movement by promoting piston, again piston cylinder is sealed, hot oil pump enters in Master cylinder body by hot oil pump, the temperature in piston cylinder is made to reach organosilicon synthesis temperature, piston moves right, the enclosure space that piston and Master cylinder body form is in vacuum state, under the influence of air pressure, monochloro methane sucks from exhaust tube, silica flour enters in piston cylinder from auto-feeder, when reaching a certain amount of, piston moves to left, exhaust tube and unidirectional feed appliance are closed automatically, thus form the space closed, piston makes the air pressure of enclosure space increase toward left movement, thus make silica flour and the complete synthesizing organo-silicon of monochloro methane, improve the utilization rate of material, reduce production cost.
Accompanying drawing content
Fig. 1 is the sectional view of device
Workbench 1 bracing frame 2
Master cylinder body 3 piston cylinder 4
Unidirectional feed appliance 5 exhaust tube 6
Motor 7 cam 8
Piston 9 spring 10
Drainage conduit 11 material storing box 12
Hot oil pump 13 hot flow path 301
Sliding sleeve 302 roller 901
Manually-operated gate 1101 induction coil 1301
Following detailed description of the invention will further illustrate in conjunction with above-mentioned accompanying drawing.
Detailed description of the invention
Hereinafter, set forth multiple specific detail, to provide the thorough understanding to the concept forming described embodiment basis.But to one skilled in the art, embodiment described obviously can be put into practice when not have in these specific detail some or all.In other cases, well-known treatment step is not specifically described.
As shown in Figure 1, workbench 1 is comprised, bracing frame 2, Master cylinder body 3, piston cylinder 4, unidirectional feed appliance 5, exhaust tube 6, motor 7, cam 8, piston 9, spring 10, drainage conduit 11, material storing box 12, hot oil pump 13, hot flow path 301, sliding sleeve 302, roller 901, manually-operated gate 1101, induction coil 1301, described Master cylinder body 3 is positioned at workbench 1 top Zhong Chu, the two screw thread is connected, described piston cylinder 4 is positioned at Master cylinder body 2 center, the two is weldingly connected, described unidirectional feed appliance 5 is positioned at Master cylinder body 3 top center left end, the two screw thread is connected, described exhaust tube 6 is positioned at Master cylinder body 3 left end center, the two is weldingly connected, described motor 7 is positioned at bracing frame 2 top center place, the two screw thread is connected, described cam 8 is positioned at center, motor 7 front end, the two screw thread is connected, described piston 9 is positioned at piston cylinder 4 inside center place, the two close-fitting is connected, described spring 10 is positioned at piston 9 left end center, it is connected with piston cylinder 4 screw thread, described drainage conduit 11 is positioned at Master cylinder body 3 bottom centre left end, the two is weldingly connected, described material storing box 12 is positioned at Master cylinder body 3 Left-side center place, it is connected with workbench 1 screw thread, be connected with drainage conduit 11 oil pipe, described hot oil pump 13 is positioned at Master cylinder body 3 Left-side center place, it is connected with Master cylinder body 3 oil pipe, be connected with workbench screw thread.Hot flow path 301 is also provided with in the middle of described piston cylinder 4 and Master cylinder body 3.Also be provided with sliding sleeve 302 in the middle of described piston 9 and Master cylinder body 3, it was connected with piston 9 sliding joining, and was connected with Master cylinder body 3 screw thread.Described piston 9 right-hand member center is also provided with roller 901, and the two screw thread is connected.Described place of drainage conduit 11 bottom centre also establishes manually-operated gate 1101, and the two screw thread is connected.Also be provided with induction coil 1301 in the middle of described hot oil pump 13, the two is weldingly connected.Wherein workbench 1, bracing frame 2 is supporting constructions of this device, heating oil pump 13 is to the hot flow path 301 pump oil in Master cylinder body 3, and by induction coil 1301, oil is heated, thus ensure that the oil temperature pumped in hot flow path can reach organosilicon synthesis temperature, thus heated to piston cylinder 4 by the oil in hot flow path 301, and can ensure that piston cylinder 4 is heated evenly, organosilicon can normally be synthesized, sliding sleeve 302 is the frictional force reducing piston 9 when piston 9 side-to-side movement, roller 901 is when cam 8 transports to peak, cam 8 and roller 901 Structure deformation, roller 901 and cam 8 belong to Structure deformation, it is stuck when cam 8 can be avoided to rotate.Induction coil 1301 is oil supply heating, and ensures the temperature in organosilicon synthesis.This device is all discharged by the air in piston cylinder 4 toward left movement by promoting piston 9, again piston cylinder 4 is sealed, hot oil pump enters in Master cylinder body by hot oil pump 13, the temperature in piston cylinder 4 is made to reach organosilicon synthesis temperature, piston 9 moves right, the enclosure space that piston 9 and piston cylinder 4 form, and be in vacuum state, under the influence of air pressure, monochloro methane sucks from exhaust tube, silica flour enters piston cylinder from auto-feeder, when reaching a certain amount of, piston 9 moves to left, exhaust tube 5 and unidirectional feed appliance 6 are closed automatically, thus form the space closed, piston 9 makes the air pressure of enclosure space increase toward left movement, thus make silica flour and the complete synthesizing organo-silicon of monochloro methane, the organosilicon of synthesis flows in drainage conduit 11, when drainage conduit 11 storage capacity reaches certain volume, opening manually-operated gate 1101 enters in material storing box 12 by the organosilicon of synthesis, this device provides pressure voluntarily with monochloro methane, thus improve the density of monochloro methane, reduce blended space, reach complete synthesizing organo-silicon, improve the utilization rate of material, reduce production cost.Improve the utilization rate of material, reduce production cost.
The present invention is not limited to above-mentioned concrete embodiment, and those of ordinary skill in the art is from above-mentioned design, and without performing creative labour, all conversion made, all drop within protection scope of the present invention.
Claims (6)
1. an organosilicon thermal synthesis device, comprise workbench, bracing frame, it is characterized in that comprising Master cylinder body, piston cylinder, unidirectional feed appliance, exhaust tube, motor, cam, piston, spring, drainage conduit, material storing box, hot oil pump, described Master cylinder body is arranged in bench-top place, the two screw thread is connected, described piston cylinder is positioned at Master cylinder body center, the two is weldingly connected, described unidirectional feed appliance is positioned at Master cylinder body top center left end, the two screw thread is connected, described exhaust tube is positioned at Master cylinder body left end center, the two is weldingly connected, described motor is positioned at bracing frame top center place, the two screw thread is connected, described cam is positioned at center, motor front end, the two screw thread is connected, described piston is positioned at piston cylinder inside center place, the two close-fitting is connected, described spring is positioned at piston left end center, it is connected with piston cylinder screw thread, described drainage conduit is positioned at Master cylinder body bottom centre left end, the two is weldingly connected, described material storing box is positioned at Master cylinder body Left-side center place, it is connected with workbench screw thread, be connected with drainage conduit oil pipe, described hot oil pump is positioned at Master cylinder body Left-side center place, it is connected with Master cylinder body oil pipe, be connected with workbench screw thread.
2. a kind of organosilicon thermal synthesis device as claimed in claim 1, is characterized in that also being provided with hot flow path in the middle of described piston cylinder and Master cylinder body.
3. a kind of organosilicon thermal synthesis device as claimed in claim 2, is characterized in that also being provided with sliding sleeve in the middle of described piston and Master cylinder body, and it was connected with piston sliding joining, and was connected with Master cylinder body screw thread.
4. a kind of organosilicon thermal synthesis device as claimed in claim 3, is characterized in that described piston right-hand member center is also provided with roller, and the two screw thread is connected.
5. a kind of organosilicon thermal synthesis device as claimed in claim 4, it is characterized in that described place of drainage conduit bottom centre also establishes manually-operated gate, the two screw thread is connected.
6. a kind of organosilicon thermal synthesis device as claimed in claim 5, it is characterized in that also being provided with induction coil in the middle of described heating oil pump, the two is weldingly connected.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510080289.7A CN104645884A (en) | 2015-02-12 | 2015-02-12 | Thermal synthesis device of organic silicon |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510080289.7A CN104645884A (en) | 2015-02-12 | 2015-02-12 | Thermal synthesis device of organic silicon |
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| Publication Number | Publication Date |
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| CN104645884A true CN104645884A (en) | 2015-05-27 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201510080289.7A Pending CN104645884A (en) | 2015-02-12 | 2015-02-12 | Thermal synthesis device of organic silicon |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108951007A (en) * | 2017-05-27 | 2018-12-07 | 无锡小天鹅股份有限公司 | The automatic release device of washing machine and washing machine with it |
| CN112254503A (en) * | 2020-10-16 | 2021-01-22 | 安徽沃园生物科技有限公司 | Rapid cooling device used after organic fertilizer granulation by breeding waste |
| CN113441988A (en) * | 2021-07-13 | 2021-09-28 | 马鞍山杰特瑞机械制造有限公司 | Extruder screw element processing piece discharge device |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1343670A (en) * | 2001-10-19 | 2002-04-10 | 清华大学 | Process and system for synthesizing organosilicon monomer by direct method |
| CN1625437A (en) * | 2001-03-07 | 2005-06-08 | 洋马株式会社 | Reaction system of organic substance employing supercritical fluid or sub-critical fluid |
| CN202638402U (en) * | 2012-06-15 | 2013-01-02 | 江苏科圣化工机械有限公司 | Organosilicone fluidized bed reactor |
-
2015
- 2015-02-12 CN CN201510080289.7A patent/CN104645884A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1625437A (en) * | 2001-03-07 | 2005-06-08 | 洋马株式会社 | Reaction system of organic substance employing supercritical fluid or sub-critical fluid |
| CN1343670A (en) * | 2001-10-19 | 2002-04-10 | 清华大学 | Process and system for synthesizing organosilicon monomer by direct method |
| CN202638402U (en) * | 2012-06-15 | 2013-01-02 | 江苏科圣化工机械有限公司 | Organosilicone fluidized bed reactor |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108951007A (en) * | 2017-05-27 | 2018-12-07 | 无锡小天鹅股份有限公司 | The automatic release device of washing machine and washing machine with it |
| CN112254503A (en) * | 2020-10-16 | 2021-01-22 | 安徽沃园生物科技有限公司 | Rapid cooling device used after organic fertilizer granulation by breeding waste |
| CN113441988A (en) * | 2021-07-13 | 2021-09-28 | 马鞍山杰特瑞机械制造有限公司 | Extruder screw element processing piece discharge device |
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Application publication date: 20150527 |