CN104707538A - Pneumatic organic silicon synthesis device - Google Patents
Pneumatic organic silicon synthesis device Download PDFInfo
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- CN104707538A CN104707538A CN201510080288.2A CN201510080288A CN104707538A CN 104707538 A CN104707538 A CN 104707538A CN 201510080288 A CN201510080288 A CN 201510080288A CN 104707538 A CN104707538 A CN 104707538A
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Abstract
The invention discloses a pneumatic organic silicon synthesis device which comprises a working table, a support rack as well as a cylinder body, a piston cylinder, a feeder, a flow control tube, an air cylinder, a piston, a discharge tube, a storage tank and a hot oil pump. Compared with the prior art, the pneumatic organic silicon synthesis device works in a mode that the piston is pushed to move leftwards to completely expel out air inside the piston cylinder, the piston cylinder is subsequently sealed, hot oil is pumped into the main cylinder body through the hot oil pump, then the temperature in the piston cylinder can reach the organic silicon synthesis temperature, the piston moves rightwards, the sealed space formed by the piston and the main cylinder body is in a vacuum state, under the action of air pressure, methane chloride can be sucked in from the flow control tube, silicon powder can be fed into the piston cylinder through the feeder, the piston moves leftwards when the amount of the silicon powder reaches a certain degree, the flow control tube and the feeder are automatically closed, then the sealed space is formed, the air pressure of the sealed space can be increased when the piston moves leftwards, and then organic silicon can be synthesized from silicon powder and methane chloride, so that the utilization rate of materials can be increased, and the production cost can be lowered.
Description
Technical field
The present invention relates to a kind of synthesizer, particularly relate to a kind of pneumatic synthesizing organo-silicon device.
Background technology
Organosilicon is a large amount of a kind of organic material used in the various industry of life, and organosilicon is silicon and organic synthesis, current synthesizing organo-silicon synthesizes in high pressure and high temperature with silica flour and monochloro methane, and existing technology is making high-pressure space, after heating to high-pressure space, a certain proportion of monochloro methane of injection and silica flour are to high-pressure space again, but other gas or air must be added while being produced on high-pressure space again, monochloro methane can be caused like this to dilute, monochloro methane and silica flour is caused to synthesize not exclusively, waste material, increase processing cost, in view of above-mentioned defect, be necessary in fact to design a kind of pneumatic synthesizing organo-silicon device.
Summary of the invention
Technical problem to be solved by this invention is: provide a kind of pneumatic synthesizing organo-silicon device, solves existing technology synthetic reaction incomplete, causes the problem that cost increases.
For solving the problems of the technologies described above, technical scheme of the present invention is: a kind of pneumatic synthesizing organo-silicon device, comprise workbench, bracing frame, comprise cylinder body, piston cylinder, feed appliance, flow control tube, cylinder, piston, drainage conduit, material storing box, hot oil pump, described cylinder body is arranged in bench-top place, the two screw thread is connected, described piston cylinder is positioned at Master cylinder body center, the two is weldingly connected, described feed appliance is positioned at Master cylinder body top center left end, the two screw thread is connected, described flow control tube is positioned at cylinder body left end center, the two is weldingly connected, described cylinder is positioned at bracing frame top center place, the two screw thread is connected, described piston is positioned at piston cylinder inside center place, it is connected with cylinder screw thread, be connected with piston cylinder sliding joining, described drainage conduit is positioned at Master cylinder body bottom centre left end, the two is weldingly connected, described material storing box is positioned at Master cylinder body Left-side center place, it is connected with workbench screw thread, be connected with drainage conduit oil pipe, described hot oil pump is positioned at Master cylinder body Left-side center place, it is connected with Master cylinder body oil pipe, be connected with workbench screw thread.
Further, described cylinder bottom center is also provided with contiguous block, and it is connected with bracing frame, cylinder screw thread.
Further, described place of drainage conduit bottom centre also establishes manually-operated gate, and the two screw thread is connected.
Further, be also provided with induction coil in the middle of described heating oil pump, the two is weldingly connected.
Further, also hot flow path is provided with in the middle of described piston cylinder and Master cylinder body.
Further, be also provided with sliding sleeve in the middle of described piston and Master cylinder body, it was connected with piston sliding joining, and was connected with Master cylinder body screw thread.
Compared with prior art, air in piston cylinder is all discharged toward left movement by promoting piston, again piston cylinder is sealed, hot oil pump enters in Master cylinder body by hot oil pump, the temperature in piston cylinder is made to reach organosilicon synthesis temperature, piston moves right, the enclosure space that piston and Master cylinder body form is in vacuum state, under the influence of air pressure, monochloro methane sucks from flow control tube, silica flour enters in piston cylinder from feed appliance, when reaching a certain amount of, piston moves to left, flow control tube and feed appliance are closed automatically, thus form the space closed, piston makes the air pressure of enclosure space increase toward left movement, thus make silica flour and the complete synthesizing organo-silicon of monochloro methane, improve the utilization rate of material, reduce production cost.
Accompanying drawing explanation
Fig. 1 is the sectional view of pneumatic synthesizing organo-silicon device
Workbench 1 bracing frame 2
Cylinder body 3 piston cylinder 4
Feed appliance 5 flow control tube 6
Tracheae 7 piston 8
Drainage conduit 9 material storing box 10
Hot oil pump 11 hot flow path 301
Sliding sleeve 302 connecting plate 701
Manually-operated gate 901 induction coil 1101
Following detailed description of the invention will further illustrate in conjunction with above-mentioned accompanying drawing.
Detailed description of the invention
Hereinafter, set forth multiple specific detail, to provide the thorough understanding to the concept forming described embodiment basis.But to one skilled in the art, embodiment described obviously can be put into practice when not have in these specific detail some or all.In other cases, well-known treatment step is not specifically described.
As shown in Figure 1, comprise workbench 1, bracing frame 2, cylinder body 3, piston cylinder 4, feed appliance 5, flow control tube 6, cylinder 7, piston 8, drainage conduit 9, material storing box 10, hot oil pump 11, described cylinder body 3 is positioned at workbench 1 top Zhong Chu, the two screw thread is connected, described piston cylinder 4 is positioned at Master cylinder body 2 center, the two is weldingly connected, described feed appliance 5 is positioned at cylinder body 3 top center left end, the two screw thread is connected, described flow control tube 6 is positioned at cylinder body 3 left end center, the two is weldingly connected, described cylinder 7 is positioned at bracing frame 2 top center place, the two screw thread is connected, described piston 8 is positioned at piston cylinder 4 inside center place, it is connected with cylinder 7 screw thread, be connected with piston cylinder 4 sliding joining, described drainage conduit 9 is positioned at cylinder body 3 bottom centre left end, the two is weldingly connected, described material storing box 10 is positioned at cylinder body 3 Left-side center place, it is connected with workbench 1 screw thread, be connected with drainage conduit 9 oil pipe, described hot oil pump 11 is positioned at cylinder body 3 Left-side center place, it is connected with cylinder body 3 oil pipe, be connected with workbench 1 screw thread, described place of cylinder 7 bottom centre is also provided with contiguous block 701, itself and bracing frame 2, cylinder 7 screw thread is connected, described place of drainage conduit 9 bottom centre also establishes manually-operated gate 901, the two screw thread is connected, induction coil 1101 is also provided with in the middle of described hot oil pump 11, the two is weldingly connected, hot flow path 301 is also provided with in the middle of described piston cylinder 4 and cylinder body 3, sliding sleeve 302 is also provided with in the middle of described piston 8 and cylinder body 3, it was connected with piston 8 sliding joining, be connected with cylinder body 3 screw thread, wherein workbench 1, bracing frame 2 is supporting constructions of this device, hot oil pump 11 is to the hot flow path 301 pump oil in cylinder body 3, and by induction coil 1101, oil is heated, thus ensure that the oil temperature pumped in hot flow path 301 can reach organosilicon synthesis temperature, thus heated to piston cylinder 4 by the oil in hot flow path 301, and can ensure that piston cylinder 4 is heated evenly, organosilicon can normally be synthesized, sliding sleeve 302 is the frictional force reducing piston 8 when piston 8 side-to-side movement, induction coil 1101 is oil supply heating, and ensure the temperature in organosilicon synthesis, this device promotes piston 8 by cylinder 7 all to be discharged by the air in piston cylinder 4 toward left movement, again piston cylinder 4 is sealed, deep fat pumps in cylinder body 3 by hot oil pump 11, the temperature in piston cylinder 4 is made to reach organosilicon synthesis temperature, cylinder 7 promotes piston 8 and moves right, the enclosure space that piston 8 and piston cylinder 4 form, and be in vacuum state, under the influence of air pressure, monochloro methane sucks from exhaust tube, silica flour enters piston cylinder 4 from feed appliance 5, when reaching a certain amount of, piston 8 moves to left, flow control tube 5 and feed appliance 6 are closed automatically, thus form the space closed, cylinder 7 promotes piston 8 and toward left movement, the air pressure of enclosure space is increased, thus make silica flour and the complete synthesizing organo-silicon of monochloro methane, the organosilicon of synthesis flows in drainage conduit 9, when drainage conduit 9 storage capacity reaches certain volume, opening manually-operated gate 901 enters in material storing box 10 by the organosilicon of synthesis, this device provides pressure voluntarily with monochloro methane, thus improve the density of monochloro methane, reduce blended space, reach complete synthesizing organo-silicon, improve the utilization rate of material, reduce production cost.Improve the utilization rate of material, reduce production cost.
The present invention is not limited to above-mentioned concrete embodiment, and those of ordinary skill in the art is from above-mentioned design, and without performing creative labour, all conversion made, all drop within protection scope of the present invention.
Claims (6)
1. a pneumatic synthesizing organo-silicon device, comprise workbench, bracing frame, it is characterized in that comprising cylinder body, piston cylinder, feed appliance, flow control tube, cylinder, piston, drainage conduit, material storing box, hot oil pump, described cylinder body is arranged in bench-top place, the two screw thread is connected, described piston cylinder is positioned at Master cylinder body center, the two is weldingly connected, described feed appliance is positioned at Master cylinder body top center left end, the two screw thread is connected, described flow control tube is positioned at cylinder body left end center, the two is weldingly connected, described cylinder is positioned at bracing frame top center place, the two screw thread is connected, described piston is positioned at piston cylinder inside center place, it is connected with cylinder screw thread, be connected with piston cylinder sliding joining, described drainage conduit is positioned at Master cylinder body bottom centre left end, the two is weldingly connected, described material storing box is positioned at Master cylinder body Left-side center place, it is connected with workbench screw thread, be connected with drainage conduit oil pipe, described hot oil pump is positioned at Master cylinder body Left-side center place, it is connected with Master cylinder body oil pipe, be connected with workbench screw thread.
2. a kind of pneumatic synthesizing organo-silicon device as claimed in claim 1, it is characterized in that described cylinder bottom center is also provided with contiguous block, it is connected with bracing frame, cylinder screw thread.
3. a kind of pneumatic synthesizing organo-silicon device as claimed in claim 2, it is characterized in that described place of drainage conduit bottom centre also establishes manually-operated gate, the two screw thread is connected.
4. a kind of pneumatic synthesizing organo-silicon device as claimed in claim 3, it is characterized in that also being provided with induction coil in the middle of described heating oil pump, the two is weldingly connected.
5. a kind of pneumatic synthesizing organo-silicon device as claimed in claim 4, is characterized in that also being provided with hot flow path in the middle of described piston cylinder and Master cylinder body.
6. a kind of pneumatic synthesizing organo-silicon device as claimed in claim 5, is characterized in that also being provided with sliding sleeve in the middle of described piston and Master cylinder body, and it was connected with piston sliding joining, and was connected with Master cylinder body screw thread.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510080288.2A CN104707538A (en) | 2015-02-12 | 2015-02-12 | Pneumatic organic silicon synthesis device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510080288.2A CN104707538A (en) | 2015-02-12 | 2015-02-12 | Pneumatic organic silicon synthesis device |
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| Publication Number | Publication Date |
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| CN104707538A true CN104707538A (en) | 2015-06-17 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201510080288.2A Pending CN104707538A (en) | 2015-02-12 | 2015-02-12 | Pneumatic organic silicon synthesis device |
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| CN (1) | CN104707538A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1343670A (en) * | 2001-10-19 | 2002-04-10 | 清华大学 | Process and system for synthesizing organosilicon monomer by direct method |
| CN1625437A (en) * | 2001-03-07 | 2005-06-08 | 洋马株式会社 | Reaction system of organic substance employing supercritical fluid or sub-critical fluid |
| CN202638402U (en) * | 2012-06-15 | 2013-01-02 | 江苏科圣化工机械有限公司 | Organosilicone fluidized bed reactor |
-
2015
- 2015-02-12 CN CN201510080288.2A patent/CN104707538A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1625437A (en) * | 2001-03-07 | 2005-06-08 | 洋马株式会社 | Reaction system of organic substance employing supercritical fluid or sub-critical fluid |
| CN1343670A (en) * | 2001-10-19 | 2002-04-10 | 清华大学 | Process and system for synthesizing organosilicon monomer by direct method |
| CN202638402U (en) * | 2012-06-15 | 2013-01-02 | 江苏科圣化工机械有限公司 | Organosilicone fluidized bed reactor |
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Application publication date: 20150617 |