CN104624120A - Organic silicon heating bath synthesis device - Google Patents
Organic silicon heating bath synthesis device Download PDFInfo
- Publication number
- CN104624120A CN104624120A CN201510076587.9A CN201510076587A CN104624120A CN 104624120 A CN104624120 A CN 104624120A CN 201510076587 A CN201510076587 A CN 201510076587A CN 104624120 A CN104624120 A CN 104624120A
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- piston
- heating
- cylinder body
- cylinder
- screw thread
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
- B01J3/04—Pressure vessels, e.g. autoclaves
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/008—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic System
- C07F7/02—Silicon compounds
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00796—Details of the reactor or of the particulate material
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)
Abstract
The invention discloses an organic silicon heating bath synthesis device which comprises a heating cylinder, wherein the heating cylinder comprises a main cylinder body, a piston cylinder body, a silicon powder tank, an air inlet pipe, a top plate, a hydraulic cylinder, a piston, an electric heater and heating oil; the piston is pushed by the hydraulic cylinder; air inside a piston cylinder is totally discharged, and then the main cylinder body is sealed; the electric heater is electrified to be heated to increase the temperature of the heating oil; and the piston cylinder body is heated, and the piston cylinder is uniformly heated. According to the organic silicon heating bath synthesis device, when certain temperature is reached, the hydraulic cylinder drives the piston to upwards pull, methane chloride is sucked from the air inlet pipe under the action of air pressure, silicon powder enters the piston cylinder from the silicon powder tank, the silicon powder is suspended in the piston cylinder, then the piston is pushed by the hydraulic cylinder to leftwards move, the air inlet pipe and the silicon powder tank are automatically closed so as to form a closed space, and the piston leftwards moves so as to increase the air pressure of the closed space, so that the silicon powder and the methane chloride are completely synthesized into organic silicon, the utilization rate of a material is enhanced, and the production cost is reduced.
Description
Technical field
The present invention relates to a kind of synthesizer, particularly relate to a kind of organosilicon heating bath synthesizer.
Background technology
Organosilicon is a large amount of a kind of organic material used in the various industry of life, and organosilicon is silicon and organic synthesis, current synthesizing organo-silicon synthesizes in high pressure and high temperature with silica flour and monochloro methane, and existing technology is making high-pressure space, after heating to high-pressure space, a certain proportion of monochloro methane of injection and silica flour are to high-pressure space again, but other gas or air must be added while being produced on high-pressure space again, monochloro methane can be caused like this to dilute, monochloro methane and silica flour is caused to synthesize not exclusively, waste material, increase processing cost, in view of above-mentioned defect, be necessary to design a kind of organosilicon heating bath synthesizer in fact.
Summary of the invention
Technical problem to be solved by this invention is: provide a kind of organosilicon heating bath synthesizer, solves existing technology synthetic reaction incomplete, causes the problem that cost increases.
For solving the problems of the technologies described above, technical scheme of the present invention is: a kind of organosilicon heating bath synthesizer, comprise heating cylinder, comprise Master cylinder body, piston/cylinder, silica flour case, air inlet pipe, top board, hydraulic cylinder, piston, electric heater, heating oil, described cylinder body is positioned at heating cylinder inside center place, the two screw thread is connected, described piston/cylinder is positioned at Master cylinder body inside center place, the two is weldingly connected, described silica flour case is positioned at Master cylinder body top center left end, the two screw thread is connected, described air inlet pipe is positioned at Master cylinder body left end center, the two is weldingly connected, described top board is positioned at heating cylinder top center place, the two screw thread is connected, described hydraulic cylinder is positioned at center, top board top, the two screw thread is connected.Described piston is positioned at end center, hydraulic cylinder bottom, the two screw thread is connected, described electric heater quantity is some, described electric heater is positioned at heating cylinder inwall place, it is evenly distributed on heating cylinder inwall, the two screw thread is connected, and described heating oil is positioned at heating cylinder inside, and its capacity depth will cover Master cylinder body.
Further, be also provided with sliding sleeve in the middle of described piston and Master cylinder body, itself and piston are slided and are joined, and are connected with Master cylinder body screw thread.
Further, be also provided with blast pipe on the left of described Master cylinder body bottom centre, itself and Master cylinder body are weldingly connected.
Further, described blast pipe bottom center place is also provided with plug, and the two screw thread is connected.
Further, described place of silica flour case bottom centre is also provided with check valve, and the two screw thread is connected.
Further, described air inlet pipe top is also provided with single-way switch, and it is connected with Master cylinder body screw thread.
Compared with prior art, by Hydraulic Cylinder piston, air in piston/cylinder is all discharged, again Master cylinder body is sealed, electric heater electrified regulation, heating oil temperature is raised, piston/cylinder is heated, and piston/cylinder is heated evenly, when reaching uniform temperature, hydraulic cylinder drives piston toward pull-up, under the influence of air pressure, monochloro methane sucks from air inlet pipe, silica flour enters in piston/cylinder from silica flour case, and make silica flour be suspended in piston/cylinder, pass through Hydraulic Cylinder piston again toward left movement, air inlet pipe and silica flour case are closed automatically, thus form the space closed, piston makes the air pressure of enclosure space increase toward left movement, thus make silica flour and the complete synthesizing organo-silicon of monochloro methane, improve the utilization rate of material, reduce production cost.
Accompanying drawing explanation
Fig. 1 is the sectional view of device
Heating cylinder 1 Master cylinder body 2
Piston/cylinder 3 silica flour case 4
Blast pipe 5 top board 6
Hydraulic cylinder 7 piston 8
Electric heater 9 heating oil 10
Sliding sleeve 201 blast pipe 202
Plug 203 check valve 401
Single-way switch 501
Following detailed description of the invention will further illustrate in conjunction with above-mentioned accompanying drawing.
Detailed description of the invention
Hereinafter, set forth multiple specific detail, to provide the thorough understanding to the concept forming described embodiment basis.But to one skilled in the art, embodiment described obviously can be put into practice when not have in these specific detail some or all.In other cases, well-known treatment step is not specifically described.
As shown in Figure 1, comprise heating cylinder 1, Master cylinder body 2, piston/cylinder 3, silica flour case 4, air inlet pipe 5, top board 6, hydraulic cylinder 7, piston 8, electric heater 9, heating oil 10, described Master cylinder body 2 is positioned at heating cylinder 1 inside center place, the two screw thread is connected, described piston/cylinder 3 body is positioned at Master cylinder body 2 inside center place, the two is weldingly connected, described silica flour case 4 is positioned at Master cylinder body 2 top center left end, the two screw thread is connected, described air inlet pipe 5 is positioned at Master cylinder body 2 left end center, the two is weldingly connected, described top board 6 is positioned at heating cylinder 1 top center place, the two screw thread is connected, described hydraulic cylinder 7 is positioned at top board 6 top center place, the two screw thread is connected, described piston 8 is positioned at end center, hydraulic cylinder 7 bottom, the two screw thread is connected, described electric heater 9 quantity is some, described electric heater 9 is positioned at heating cylinder 1 inwall place, it is evenly distributed on heating cylinder 1 inwall, the two screw thread is connected, it is inner that described heating oil 10 is positioned at heating cylinder 1, its capacity depth will cover Master cylinder body 2, sliding sleeve 201 is also provided with in the middle of described piston 8 and Master cylinder body 2, itself and piston 8 are slided and are joined, be connected with Master cylinder body 2 screw thread, blast pipe 202 is also provided with on the upside of described Master cylinder body 2 left end center, itself and Master cylinder body 2 are weldingly connected, described blast pipe 202 left end center is also provided with plug 203, the two screw thread is connected, described place of silica flour case 4 bottom centre is also provided with check valve 401, the two screw thread is connected, described air inlet pipe 5 right-hand member is also provided with single-way switch 501, it is connected with Master cylinder body 2 screw thread, wherein heating cylinder 1 is that heating oil 10 is housed, at electric heater 9 electrified regulation, heating oil 10 temperature is raised, and pass to piston/cylinder 3, heated by heating oil 10 pairs of piston/cylinders 3, it is heated evenly, temperature stabilization, can better synthesizing organo-silicon, sliding sleeve 201 reduces its frictional force when piston 8 slides with Master cylinder body 2, blast pipe 202 is when this device first time uses, air in piston/cylinder 3 is all discharged to left movement by piston 8, with plug 203, blast pipe is being blocked, ensure that piston/cylinder 3 is in vacuum state, this device promotes piston 8 by hydraulic cylinder 7, air in piston/cylinder 3 is all discharged, again Master cylinder body 2 is sealed, electric heater 9 electrified regulation, heating oil 10 temperature is raised, piston/cylinder 3 body is heated, and piston/cylinder 3 is heated evenly, when reaching uniform temperature, hydraulic cylinder 7 drives piston 8 toward pull-up, under the influence of air pressure, monochloro methane sucks from air inlet pipe, silica flour enters in piston/cylinder 3 from silica flour case 4, and make silica flour be suspended in piston/cylinder 3, piston 8 is promoted toward left movement again by hydraulic cylinder 7, air inlet pipe 5 and silica flour are closed automatically, thus form the space closed, piston 8 makes the air pressure of enclosure space increase toward left movement, thus make silica flour and the complete synthesizing organo-silicon of monochloro methane, improve the utilization rate of material, reduce production cost.
The present invention is not limited to above-mentioned concrete embodiment, and those of ordinary skill in the art is from above-mentioned design, and without performing creative labour, all conversion made, all drop within protection scope of the present invention.
Claims (6)
1. an organosilicon heating bath synthesizer, comprise heating cylinder, it is characterized in that comprising Master cylinder body, piston/cylinder, silica flour case, air inlet pipe, top board, hydraulic cylinder, piston, electric heater, heating oil, described cylinder body is positioned at heating cylinder inside center place, the two screw thread is connected, described piston/cylinder is positioned at Master cylinder body inside center place, the two is weldingly connected, described silica flour case is positioned at Master cylinder body top center left end, the two screw thread is connected, described air inlet pipe is positioned at Master cylinder body left end center, the two is weldingly connected, described top board is positioned at heating cylinder top center place, the two screw thread is connected, described hydraulic cylinder is positioned at center, top board top, the two screw thread is connected, described piston is positioned at end center, hydraulic cylinder bottom, the two screw thread is connected, described electric heater quantity is some, described electric heater is positioned at heating cylinder inwall place, it is evenly distributed on heating cylinder inwall, the two screw thread is connected, described heating oil is positioned at heating cylinder inside, its capacity depth will cover Master cylinder body.
2. a kind of organosilicon heating bath synthesizer as claimed in claim 1, it is characterized in that also being provided with sliding sleeve in the middle of described piston and Master cylinder body, itself and piston are slided and are joined, and are connected with Master cylinder body screw thread.
3. a kind of organosilicon heating bath synthesizer as claimed in claim 2, it is characterized in that also being provided with blast pipe on the left of described Master cylinder body bottom centre, itself and Master cylinder body are weldingly connected.
4. as a kind of organosilicon heating bath synthesizer that claim 3 is stated, it is characterized in that described blast pipe bottom center place is also provided with plug, the two screw thread is connected.
5. a kind of organosilicon heating bath synthesizer as claimed in claim 4, it is characterized in that described place of silica flour case bottom centre is also provided with check valve, the two screw thread is connected.
6. a kind of organosilicon heating bath synthesizer as claimed in claim 5, it is characterized in that described air inlet pipe top is also provided with single-way switch, it is connected with Master cylinder body screw thread.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510076587.9A CN104624120A (en) | 2015-02-12 | 2015-02-12 | Organic silicon heating bath synthesis device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510076587.9A CN104624120A (en) | 2015-02-12 | 2015-02-12 | Organic silicon heating bath synthesis device |
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| Publication Number | Publication Date |
|---|---|
| CN104624120A true CN104624120A (en) | 2015-05-20 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510076587.9A Pending CN104624120A (en) | 2015-02-12 | 2015-02-12 | Organic silicon heating bath synthesis device |
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| Country | Link |
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| CN (1) | CN104624120A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107447984A (en) * | 2017-08-02 | 2017-12-08 | 惠州鼎泰利科技有限公司 | A kind of plug for plastic building template |
| CN112657402A (en) * | 2021-01-08 | 2021-04-16 | 江门市兆晖电器科技有限公司 | Anti-oxidation vacuum mixer |
| CN113477183A (en) * | 2021-07-05 | 2021-10-08 | 安徽海顺化工有限公司 | Reaction kettle for p-chlorobenzyl chloride production and production process of p-chlorobenzyl chloride |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1343670A (en) * | 2001-10-19 | 2002-04-10 | 清华大学 | Process and system for synthesizing organosilicon monomer by direct method |
| CN1625437A (en) * | 2001-03-07 | 2005-06-08 | 洋马株式会社 | Reaction system of organic substance employing supercritical fluid or sub-critical fluid |
| CN202638402U (en) * | 2012-06-15 | 2013-01-02 | 江苏科圣化工机械有限公司 | Organosilicone fluidized bed reactor |
-
2015
- 2015-02-12 CN CN201510076587.9A patent/CN104624120A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1625437A (en) * | 2001-03-07 | 2005-06-08 | 洋马株式会社 | Reaction system of organic substance employing supercritical fluid or sub-critical fluid |
| CN1343670A (en) * | 2001-10-19 | 2002-04-10 | 清华大学 | Process and system for synthesizing organosilicon monomer by direct method |
| CN202638402U (en) * | 2012-06-15 | 2013-01-02 | 江苏科圣化工机械有限公司 | Organosilicone fluidized bed reactor |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107447984A (en) * | 2017-08-02 | 2017-12-08 | 惠州鼎泰利科技有限公司 | A kind of plug for plastic building template |
| CN112657402A (en) * | 2021-01-08 | 2021-04-16 | 江门市兆晖电器科技有限公司 | Anti-oxidation vacuum mixer |
| CN113477183A (en) * | 2021-07-05 | 2021-10-08 | 安徽海顺化工有限公司 | Reaction kettle for p-chlorobenzyl chloride production and production process of p-chlorobenzyl chloride |
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Application publication date: 20150520 |