CN104631155A - Dyeing method of flame retardant blended fabric - Google Patents
Dyeing method of flame retardant blended fabric Download PDFInfo
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- CN104631155A CN104631155A CN201510067885.1A CN201510067885A CN104631155A CN 104631155 A CN104631155 A CN 104631155A CN 201510067885 A CN201510067885 A CN 201510067885A CN 104631155 A CN104631155 A CN 104631155A
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Abstract
The invention relates to a dyeing method of a flame retardant blended fabric. The method comprises the following steps: (1) carrying out pretreatment, namely, boiling the flame retardant blended fabric in a pretreatment agent for 30-50 minutes at the temperature of 70-95 DEG C; (2) dyeing in a first bath, namely, transferring the flame retardant blended fabric obtained in the step (1) into a first dye vat; and (3) dyeing in a second bath, namely, transferring the flame retardant blended fabric obtained in the step (2) into a second dye vat. The flame retardant blended fabric comprises the following components in parts by weight: 40-60 parts of meta-position aramid fiber and 40-60 parts of flame retardant viscose fiber. According to the dyeing and finishing method, in the process of dyeing in the first bath, the meta-position aramid fiber is dyed, and in the process of dyeing in the second bath, the flame retardant viscose fiber is dyed, so that different dyeing and finishing processes are carried out on the two fibers with different functions; the dyeing method has the advantages of being uniform in dyeing, stable, washable, good in flame retardant property and the like.
Description
Technical field
The present invention relates to a kind of colouring method of fabric, be specifically related to a kind of colouring method of flame-retardant blended fabric.
Background technology
Carry out the technical process based on chemical treatment to textile material (fiber, yarn and fabric), the modern times are also commonly referred to as printing and dyeing.Dyeing and finishing with spinning, woven or knitting production together, forms the overall process that textiles is produced.Dyeing and finishing comprises preliminary treatment, dyeing, stamp and arrangement.The use value of quality on textiles of dyeing and finishing quality has important impact.Preliminary treatment is also known as scouringing and bleaching, and its main purpose is to remove the impurity on textile material, makes follow-up dyeing, stamp, arrangement process smooth, obtains the processing effect of expection.Dyeing is combination by dyestuff and fiber generation physics or chemistry and makes textile material have certain color.Stamp on textiles, obtains chromatic pattern pattern with mill base.Arrangement is by physical action or uses chemical agent to improve the outward appearance such as gloss, form of fabric; Improve the wearability of fabric or fabric had refuse water, refuse wet goods characteristic.
For blended yarn woven fabric, especially flame-retardant blended fabric, because two kinds of fibre property difference are comparatively large, therefore Colour Difference difficulty is large, easily occurs the phenomenon of uneven dyeing in dyeing course, and the quality of production is unstable.When carrying out dyeing and finishing technology, need to take into account the role and influence of process conditions to different fiber.Because each procedure all likely has influence on fire resistance, dyefastness, the dye level of fabric, this is those skilled in the art's technical problems urgently to be resolved hurrily.
Summary of the invention
For above shortcomings in prior art, one of technical problem to be solved by this invention is to provide a kind of colouring method of flame-retardant blended fabric.
A colouring method for flame-retardant blended fabric, comprises the steps:
(1) pre-treatment: practiced in pretreating reagent by flame-retardant blended fabric and boil 30-50min, it is 70-95 DEG C that white silk boils temperature, and described pretreating reagent comprises following component: refining agent 1-3g/l, caustic soda 1-3g/l, hydrogen peroxide 1-3g/l, whitening agent 2-6g/l;
(2) first bath dyeing: the flame-retardant blended fabric that step (1) obtains is moved into the first dye vat, it contains 1-3g/L acetic acid, add the yellow X-10GFF of cationic fluorescent of flame-retardant blended fabric weight 1-5%, after being heated to 60-80 DEG C, 100 DEG C are heated to the programming rate of 1-3 DEG C/min, insulation 40-60min, washing;
(3) two-bath dyeings: the flame-retardant blended fabric that step (2) obtains is moved into the second dye vat, add the Remazol fluorescein FL of flame-retardant blended fabric weight 1-5%, 30-50 DEG C adds 15-25g/L glauber salt, after being warming up to 55-65 DEG C, add 15-25g/L glauber salt, insulation 10-20min, adds 20-30g/L soda ash, insulation 40-60min;
Described flame-retardant blended fabric is made up of by weight following component: meta-aramid fibers 40-60 part and Fire resistant viscose fiber 40-60 part;
Described refining agent is selected from one in polyoxyethylene nonylphenol ether, cetanol polyoxyethylene ether, turkey red oil or its mixture;
Described whitening agent is selected from sodium chlorite or clorox.
Preferably,
Described refining agent is made up of following weight parts component: polyoxyethylene nonylphenol ether 40-60 part, cetanol polyoxyethylene ether 40-60 part, turkey red oil 10-30 part.
Step (2) described washing comprises washing, soaps, washes three steps.
Meta-aramid fibers, also known as: aramid fiber 1313, Fanglun 1313; English name: polyisophthaloyl metaphenylene diamine fibre; Fanglun 1313.Meta-aramid fibers forms through solution-polymerized SBR by after m-phenylene diamine (MPD) and m-phthaloyl chloride polycondensation, and its feature gas permeability, poisture-penetrability are good, heat-resisting quantity, anti-flammability, resistance to most corrosion.
Fire resistant viscose fiber, can be prepared by blending method, dip coating etc. for viscose and fire retardant, also directly can buy acquisition.
Described glauber salt, i.e. Disodium sulfate decahydrate, have another name called saltcake.
Polyoxyethylene nonylphenol ether, No. CAS: 9016-45-9.
Cetanol polyoxyethylene ether, No. CAS: 9004-95-9.
Turkey red oil, No. CAS: 8002-33-3.
The techniques such as the toning in the present invention, soaps, fixation, washing are the common process of this area.
Use dyeing and finishing method of the present invention, first bath dyeing is dyeed to polyacrylic and polyester fiber, and two-bath dyeing dyes to cotton fiber, have been directed to the difference in functionality of two kinds of fibers, carry out different dyeing and finishing technologies, there is even dyeing, stablize, water-fastness, the advantages such as fire resistance is good.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described.
Take meta-aramid fibers 50 kilograms, Fire resistant viscose fiber 50 kilograms, mixes, and shredding preliminary treatment, carding machine is carded to the carded sliver; Also close on drawing frame again and make ripe bar; Speed frames carry out drawing-off and twisting, and finally further draw twisting on fine spining machine, make blended yarn, yarn linear density is 39tex.Adopted by blended yarn large circle machine knitting device making method to weave again, warp count is 200/10cm, warp count is 200/10cm, and the BLENDED FABRIC of final obtained meta-aramid and anti-flaming viscose, for following embodiment and comparative example.
The pearl power Fire resistant viscose fiber that the Fire resistant viscose fiber used in embodiment and comparative example is produced for Huzhou Zhu Li scientific & technical corporation, the article number on global textile web is SL128517810; Aramid fiber 1313: du pont company provides, trade name: Nomex, oxygen index (OI) LOI value 29.3%.Remazol fluorescein FL (RemazolluminousyellowFL) is that German De Sida (DyStar) company produces; The yellow X-10GFF of cationic fluorescent buys from Mei Le Chemical Co., Ltd. of Shangyu city.
Embodiment 1
(1) pre-treatment: add following component preparation pretreating reagent in water: refining agent 2g/l, caustic soda 2g/l, hydrogen peroxide 2g/l, clorox 4g/l, by flame-retardant blended fabric kiering 50min at 90 DEG C; Wherein, described refining agent is made up of following weight parts component: polyoxyethylene nonylphenol ether 50 parts, cetanol polyoxyethylene ether 50 parts, turkey red oil 20 parts;
(2) first bath dyeing: the flame-retardant blended fabric that step (1) obtains is moved into the first dye vat, it contains 2g/L acetic acid, add the yellow X-10GFF of cationic fluorescent of flame-retardant blended fabric weight 3%, after being heated to 70 DEG C, be heated to 100 DEG C with the programming rate of 1 DEG C/min, insulation 45min, washing, soap (neutral soap lotion 2g/L, 40 ± 2 DEG C, soap 30min), washing;
(3) two-bath dyeings: the flame-retardant blended fabric that step (2) obtains is moved into the second dye vat, add the Remazol fluorescein FL of flame-retardant blended fabric weight 3%, 40 DEG C add 25g/L glauber salt, after being warming up to 60 DEG C, add 25g/L glauber salt, insulation 10min, adds 25g/L soda ash, insulation 60min;
(4) wash, obtain the flame-retardant blended fabric after dyeing and finishing.
Embodiment 2
According to method described in embodiment 1, described refining agent replaces with described refining agent and is made up of following weight parts component: polyoxyethylene nonylphenol ether 60 parts, cetanol polyoxyethylene ether 60 parts.
Embodiment 3
According to method described in embodiment 1, described refining agent replaces with described refining agent and is made up of following weight parts component: polyoxyethylene nonylphenol ether 100 parts, turkey red oil 20 parts.
Embodiment 4
According to method described in embodiment 1, described in described refining agent, refining agent is made up of following weight parts component: cetanol polyoxyethylene ether 100 parts, turkey red oil 20 parts.
Comparative example 1
(1) pre-treatment: add following component preparation pretreating reagent in water: refining agent 2g/l, caustic soda 2g/l, hydrogen peroxide 2g/l, clorox 4g/l, by flame-retardant blended fabric kiering 50min at 90 DEG C; Wherein, described refining agent is made up of following weight parts component: polyoxyethylene nonylphenol ether 50 parts, cetanol polyoxyethylene ether 50 parts, turkey red oil 20 parts;
(2) first bath dyeing: the flame-retardant blended fabric that step (1) obtains is moved into the first dye vat, it contains 2g/L acetic acid, add the yellow X-10GFF of cationic fluorescent of flame-retardant blended fabric weight 3%, after being heated to 100 DEG C, insulation 45min, washing, soap (neutral soap lotion 2g/L, 40 ± 2 DEG C, soap 30min), washing;
(3) two-bath dyeings: the flame-retardant blended fabric that step (2) obtains is moved into the second dye vat, add the Remazol fluorescein FL of flame-retardant blended fabric weight 3%, 60 DEG C, add 50g/L glauber salt, insulation 10min, adds 25g/L soda ash, insulation 60min;
(4) to sample toning, soap (neutral soap lotion 2g/L, 40 ± 2 DEG C, soap 30min), fixation, and washing, obtains the flame-retardant blended fabric after dyeing and finishing.
Comparative example 2
(1) pre-treatment: add following component preparation pretreating reagent in water: refining agent 2g/l, caustic soda 2g/l, hydrogen peroxide 2g/l, clorox 4g/l, by flame-retardant blended fabric kiering 50min at 90 DEG C; Wherein, described refining agent is made up of following weight parts component: polyoxyethylene nonylphenol ether 50 parts, cetanol polyoxyethylene ether 50 parts, turkey red oil 20 parts;
(2) first bath dyeing: the flame-retardant blended fabric that step (1) obtains is moved into the first dye vat, it contains 2g/L acetic acid, add the Remazol fluorescein FL of flame-retardant blended fabric weight 3%, after being heated to 70 DEG C, be heated to 100 DEG C with the programming rate of 1 DEG C/min, insulation 45min, washing, soap (neutral soap lotion 2g/L, 40 ± 2 DEG C, soap 30min), washing;
(3) two-bath dyeings: the flame-retardant blended fabric that step (2) obtains is moved into the second dye vat, add the Remazol fluorescein FL of flame-retardant blended fabric weight 3%, 40 DEG C add 25g/L glauber salt, after being warming up to 60 DEG C, add 25g/L glauber salt, insulation 10min, adds 25g/L soda ash, insulation 60min;
(4) to sample toning, soap (neutral soap lotion 2g/L, 40 ± 2 DEG C, soap 30min), fixation, and washing, obtains the flame-retardant blended fabric after dyeing and finishing.
Comparative example 3
(1) pre-treatment: add following component preparation pretreating reagent in water: refining agent 2g/l, caustic soda 2g/l, hydrogen peroxide 2g/l, clorox 4g/l, by flame-retardant blended fabric kiering 50min at 90 DEG C; Wherein, described refining agent is made up of following weight parts component: polyoxyethylene nonylphenol ether 50 parts, cetanol polyoxyethylene ether 50 parts, turkey red oil 20 parts;
(2) first bath dyeing: the flame-retardant blended fabric that step (1) obtains is moved into the first dye vat, it contains 2g/L acetic acid, add the yellow X-10GFF of cationic fluorescent of flame-retardant blended fabric weight 3%, after being heated to 70 DEG C, be heated to 100 DEG C with the programming rate of 1 DEG C/min, insulation 45min, washing, soap (neutral soap lotion 2g/L, 40 ± 2 DEG C, soap 30min), washing;
(3) two-bath dyeings: the flame-retardant blended fabric that step (2) obtains is moved into the second dye vat, add the yellow X-10GFF of cationic fluorescent of flame-retardant blended fabric weight 3%, 40 DEG C add 25g/L glauber salt, after being warming up to 60 DEG C, add 25g/L glauber salt, insulation 10min, adds 25g/L soda ash, insulation 60min;
(4) to sample toning, soap (neutral soap lotion 2g/L, 40 ± 2 DEG C, soap 30min), fixation, and washing, obtains the flame-retardant blended fabric after dyeing and finishing.
Comparative example 4
(1) pre-treatment: add following component preparation pretreating reagent in water: refining agent 2g/l, caustic soda 2g/l, hydrogen peroxide 2g/l, clorox 4g/l, by flame-retardant blended fabric kiering 50min at 90 DEG C; Wherein, described refining agent is made up of following weight parts component: polyoxyethylene nonylphenol ether 50 parts, cetanol polyoxyethylene ether 50 parts, turkey red oil 20 parts;
(2) first bath dyeing: the flame-retardant blended fabric that step (1) obtains is moved into the first dye vat, it contains 2g/L acetic acid, add the Remazol fluorescein FL of flame-retardant blended fabric weight 3%, after being heated to 70 DEG C, be heated to 100 DEG C with the programming rate of 1 DEG C/min, insulation 45min, washing, soap (neutral soap lotion 2g/L, 40 ± 2 DEG C, soap 30min), washing;
(3) two-bath dyeings: the flame-retardant blended fabric that step (2) obtains is moved into the second dye vat, add the yellow X-10GFF of cationic fluorescent of flame-retardant blended fabric weight 3%, 40 DEG C add 25g/L glauber salt, after being warming up to 60 DEG C, add 25g/L glauber salt, insulation 10min, adds 25g/L soda ash, insulation 60min;
(4) to sample toning, soap (neutral soap lotion 2g/L, 40 ± 2 DEG C, soap 30min), fixation, and washing, obtains the flame-retardant blended fabric after dyeing and finishing.
Test case 1
Carry out fastness to soaping test to the flame-retardant blended fabric after embodiment 1-4 and comparative example 1-4 dyeing and finishing, every premium on currency contains 5g soap, soaping condition (1): 40 ± 2 DEG C, and soap 30min; Soaping condition (2): 60 ± 2 DEG C, soap 60min; Soaping condition (3): 95 ± 2 DEG C, soap 4h; Then use cold water clear twice, room temperature hang airing, the variable color of use variable color gray scale evaluation embodiment 1-6 and test result are in table 1.5 grades represent that variable color fastness is best, and 1 grade represents that variable color fastness is the poorest.
Table 1 embodiment 1-4 and the test of comparative example 1-4 fastness to soaping
| Soaping condition (1) | Soaping condition (2) | Soaping condition (3) | |
| Embodiment 1 | 5 | 5 | 5 |
| Embodiment 2 | 5 | 4 | 3.5 |
| Embodiment 3 | 5 | 4.5 | 4 |
| Embodiment 4 | 5 | 4 | 4 |
| Comparative example 1 | 4 | 3 | 2.5 |
| Comparative example 2 | 4.5 | 3.5 | 3 |
| Comparative example 3 | 4 | 3.5 | 2.5 |
| Comparative example 4 | 4 | 3.5 | 3 |
Test case 2
Resistance to adjacent fabric staining test of soaping is carried out to the flame-retardant blended fabric after embodiment 1-4 and comparative example 1-4 dyeing and finishing, to fit on flame-retardant blended fabric two sides to be measured respectively the pure aramid fiber 1313 fabric of one deck and one deck anti-flaming viscose fabric, and sew up three layers of sample, sample size is 40mm × 100mm, soap according to the method for test case 1, then cold water is used clear twice, room temperature hang airing, the variable color of use staining gray scale evaluation embodiment 1-4 and comparative example 1-4 and test result are in table 2.5 grades indicate without staining, and 1 grade represents that staining is the most serious.
The resistance to adjacent fabric staining test of soaping of table 1 embodiment 1-4 and comparative example 1-4
| Soaping condition (1) | Soaping condition (2) | Soaping condition (3) | |
| Embodiment 1 | 5 | 5 | 5 |
| Embodiment 2 | 5 | 4.5 | 4 |
| Embodiment 3 | 4.5 | 4 | 3.5 |
| Embodiment 4 | 5 | 4 | 4 |
| Comparative example 1 | 4.5 | 3 | 2.5 |
| Comparative example 2 | 5 | 3.5 | 3 |
| Comparative example 3 | 4 | 3 | 2 |
| Comparative example 4 | 4 | 3 | 2.5 |
Use dyeing and finishing method of the present invention, first bath dyeing is dyeed to aramid fiber 1313, and two-bath dyeing dyes to Fire resistant viscose fiber, have been directed to the difference in functionality of two kinds of fibers, carry out different dyeing and finishing technologies, there is even dyeing, stablize, water-fastness, the advantages such as fire resistance is good.
Above-described embodiment is interpreted as only being not used in for illustration of the present invention limiting the scope of the invention.After the content of having read the present invention's record, those skilled in the art can make various changes or modifications the present invention, and these equivalence changes and modification fall into the scope of the claims in the present invention equally.
Claims (3)
1. a colouring method for flame-retardant blended fabric, is characterized in that, comprises the steps:
(1) pre-treatment: practiced in pretreating reagent by flame-retardant blended fabric and boil 30-50min, it is 70-95 DEG C that white silk boils temperature, and described pretreating reagent comprises following component: refining agent 1-3g/l, caustic soda 1-3g/l, hydrogen peroxide 1-3g/l, whitening agent 2-6g/l;
(2) first bath dyeing: the flame-retardant blended fabric that step (1) obtains is moved into the first dye vat, it contains 1-3g/L acetic acid, add the yellow X-10GFF of cationic fluorescent of flame-retardant blended fabric weight 1-5%, after being heated to 60-80 DEG C, 100 DEG C are heated to the programming rate of 1-3 DEG C/min, insulation 40-60min, washing;
(3) two-bath dyeings: the flame-retardant blended fabric that step (2) obtains is moved into the second dye vat, add the Remazol fluorescein FL of flame-retardant blended fabric weight 1-5%, 30-50 DEG C adds 15-25g/L glauber salt, after being warming up to 55-65 DEG C, add 15-25g/L glauber salt, insulation 10-20min, adds 20-30g/L soda ash, insulation 40-60min;
Described flame-retardant blended fabric is made up of by weight following component: meta-aramid fibers 40-60 part and Fire resistant viscose fiber 40-60 part;
Described refining agent is selected from one in polyoxyethylene nonylphenol ether, cetanol polyoxyethylene ether, turkey red oil or its mixture;
Described whitening agent is selected from sodium chlorite or clorox.
2. the colouring method of flame-retardant blended fabric as claimed in claim 1, is characterized in that: described refining agent is made up of following weight parts component: polyoxyethylene nonylphenol ether 40-60 part, cetanol polyoxyethylene ether 40-60 part, turkey red oil 10-30 part.
3. the colouring method of flame-retardant blended fabric as claimed in claim 1 or 2, is characterized in that: step (2) described washing comprises washing, soaps, washes three steps.
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| CN104631155B (en) | 2016-12-07 |
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