CN104629423A - Formula and production method of dark cyan wheat straw dye - Google Patents

Formula and production method of dark cyan wheat straw dye Download PDF

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Publication number
CN104629423A
CN104629423A CN201310546346.7A CN201310546346A CN104629423A CN 104629423 A CN104629423 A CN 104629423A CN 201310546346 A CN201310546346 A CN 201310546346A CN 104629423 A CN104629423 A CN 104629423A
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CN
China
Prior art keywords
wheat straw
darkcyan
raw material
solution
dye
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Pending
Application number
CN201310546346.7A
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Chinese (zh)
Inventor
马文侠
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Harbin Arts and Crafts Co Ltd
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Harbin Arts and Crafts Co Ltd
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Filing date
Publication date
Application filed by Harbin Arts and Crafts Co Ltd filed Critical Harbin Arts and Crafts Co Ltd
Priority to CN201310546346.7A priority Critical patent/CN104629423A/en
Publication of CN104629423A publication Critical patent/CN104629423A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K9/00Chemical or physical treatment of reed, straw, or similar material
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B61/00Dyes of natural origin prepared from natural sources, e.g. vegetable sources

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Forests & Forestry (AREA)
  • Noodles (AREA)

Abstract

The invention discloses a formula and a production method of a dark cyan wheat straw dye. According to the formula, dried broom, cornflower, Chinese tallow-tree leaf, alumen, iron ion compound solution, and mineral water are taken as main raw materials. The production method comprises following steps: material choosing, material cutting, drying, immersing, heat boiling, mixing, precipitating, dyeing, and finished product obtaining. The dark cyan wheat straw dye is pure natural, and is green and friendly to the environment; no pollution is caused; no toxic or side effect on human body is caused; and the dark cyan wheat straw dye is prepared from pure natural plant materials.

Description

A kind of formula and production method preparing darkcyan wheat straw dye
technical field:
the present invention relates to a kind of vegetable dye, particularly relates to a kind of formula and the production method of preparing darkcyan wheat straw dye
background technology:
in prior art, the method that the main raw material Wheat Straw making straw patchwork dyes darkcyan is had a variety of, but most dyestuff is chemical dye, the darkcyan dyed is impure, easily fade, not only not environmentally, some dyes even can produce toxic gas in the process of dye system, threatens the health of human body.
thus, make field at straw patchwork and lack a kind of vegetable dye Wheat Straw being dyed different colours, particularly Wheat Straw is dyed the natural plant dyestuff of darkcyan, not only color is pure for the darkcyan Wheat Straw that it dyes, and the straw patchwork made with its material is bright and new beautiful, not easily fades, and environmental protection, works give out plant fragrance for a long time, have the physical and mental health of easy people, and what degree was different solves other poisonous and harmful chemical dye in dye process processed to the prestige evil that people's health causes.
summary of the invention:
the object of the present invention is to provide a kind of pure natural, pollution-free, environmental protection, a kind of formula and the production method preparing darkcyan wheat straw dye be mixed with natural plant that the person is had no side effect
the object of the present invention is achieved like this.It is that the raw material of being joined by following weight is made, and Broome does 10-30 part, Minor centaury 10-30 part, black prostheca 5-15 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
the formula optimization weight proportion scope preparing darkcyan wheat straw dye of the present invention is, wherein the weight proportion of various raw material is that Broome does 10-25 part, Minor centaury 10-25 part, black prostheca 5-10 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
the optimum weight ratio range preparing darkcyan wheat straw dye of the present invention is that wherein the weight proportion of various raw material is: dry 15 parts of Broome, Minor centaury 15 parts, black prostheca 8 parts, alum 8 parts, ferric ion compounds solution 8 parts, mineral water 65 parts.
above-mentioned each component is made the production method of darkcyan wheat straw dye of the present invention, technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select that the Broome meeting national health and quality standard is dry, Minor centaury, black prostheca, alum, ferric ion compounds solution, mineral water be for subsequent use; B, blank, by the raw material selected except alum, ferric ion compounds solution, mineral water are cut into bulk respectively; C, oven dry, the shape raw material that will be cut into small pieces are placed in stoving oven mummification respectively, and temperature controls at 100-120 DEG C, 30 minutes time, make raw materials evaporate moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure darkcyan cellulose solution; H, dyeing, the temperature of 100 liters of pure darkcyan cellulose solutions is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb darkcyan cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to darkcyan Wheat Straw finished product at room temperature.
production method advantage of the present invention is: 1, select raw material, scientific formulation, color is pure; 2, do not add sanitas in product, industrial chemicals, pure natural, to human body without any injury, the straw patchwork works made with its raw material not only distribute Scent, and anticorrosive; 3 raw material sources are extensive, add process line short, the easy processing and manufacturing of product.
Embodiment
below in conjunction with specific embodiment, the present invention is further illustrated:
embodiment 1:
the formulation weight ratio range preparing darkcyan wheat straw dye of the present invention is: Broome does 10-30 part, Minor centaury 10-30 part, black prostheca 5-15 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
embodiment 2:
the formula optimization weight proportion scope preparing darkcyan wheat straw dye of the present invention is: Broome does 10-25 part, Minor centaury 10-25 part, black prostheca 5-10 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
embodiment 3:
the formula optimum weight ratio range preparing darkcyan wheat straw dye of the present invention is: wherein the weight proportion of various raw material is, dry 15 parts of Broome, Minor centaury 15 parts, black prostheca 8 parts, alum 8 parts, ferric ion compounds solution 8 parts, mineral water 65 parts.
above-mentioned each component is made the production method of darkcyan wheat straw dye of the present invention, technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select that the Broome meeting national health and quality standard is dry, Minor centaury, black prostheca, alum, ferric ion compounds solution, mineral water be for subsequent use; B, blank, by the raw material selected except alum, ferric ion compounds solution, mineral water are cut into bulk respectively; C, oven dry, the shape raw material that will be cut into small pieces are placed in stoving oven mummification respectively, and temperature controls at 100-120 DEG C, 30 minutes time, make raw materials evaporate moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure darkcyan cellulose solution; H, dyeing, the temperature of 100 liters of pure darkcyan cellulose solutions is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb darkcyan cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to darkcyan Wheat Straw finished product at room temperature.

Claims (4)

1. prepare the formula of darkcyan wheat straw dye for one kind, it is characterized in that: it is made up of the raw material of following weight proportioning, Broome does 10-30 part, Minor centaury 10-30 part, black prostheca 5-15 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
2. prepare the formula of darkcyan wheat straw dye for one kind, it is characterized in that: wherein the weight proportion of various raw material is, Broome does 10-25 part, Minor centaury 10-25 part, black prostheca 5-10 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
3. prepare a formula for darkcyan wheat straw dye, it is characterized in that: wherein the weight proportion of various raw material is, dry 15 parts of Broome, Minor centaury 15 parts, black prostheca 8 parts, alum 8 parts, ferric ion compounds solution 8 parts, mineral water 65 parts.
4. a kind of production method preparing darkcyan wheat straw dye formula according to claim 1-3, it is characterized in that: technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select that the Broome meeting national health and quality standard is dry, Minor centaury, black prostheca, alum, ferric ion compounds solution, mineral water be for subsequent use; B, blank, by the raw material selected except alum, ferric ion compounds solution, mineral water are cut into bulk respectively; C, oven dry, the shape raw material that will be cut into small pieces are placed in stoving oven mummification respectively, and temperature controls at 100-120 DEG C, 30 minutes time, make raw materials evaporate moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure darkcyan cellulose solution; H, dyeing, the temperature of 100 liters of pure darkcyan cellulose solutions is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb darkcyan cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to darkcyan Wheat Straw finished product at room temperature.
CN201310546346.7A 2013-11-07 2013-11-07 Formula and production method of dark cyan wheat straw dye Pending CN104629423A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310546346.7A CN104629423A (en) 2013-11-07 2013-11-07 Formula and production method of dark cyan wheat straw dye

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201310546346.7A CN104629423A (en) 2013-11-07 2013-11-07 Formula and production method of dark cyan wheat straw dye

Publications (1)

Publication Number Publication Date
CN104629423A true CN104629423A (en) 2015-05-20

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CN201310546346.7A Pending CN104629423A (en) 2013-11-07 2013-11-07 Formula and production method of dark cyan wheat straw dye

Country Status (1)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106398292A (en) * 2015-08-11 2017-02-15 哈尔滨市工艺美术有限责任公司 Matcha-color corn stalk dye and production method therefor

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106398292A (en) * 2015-08-11 2017-02-15 哈尔滨市工艺美术有限责任公司 Matcha-color corn stalk dye and production method therefor

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Application publication date: 20150520