CN104629411A - Formula and production method of pastel violet wheat straw dye - Google Patents
Formula and production method of pastel violet wheat straw dye Download PDFInfo
- Publication number
- CN104629411A CN104629411A CN201310545736.2A CN201310545736A CN104629411A CN 104629411 A CN104629411 A CN 104629411A CN 201310545736 A CN201310545736 A CN 201310545736A CN 104629411 A CN104629411 A CN 104629411A
- Authority
- CN
- China
- Prior art keywords
- wheat straw
- solution
- raw material
- purple powder
- dye
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/52—Impregnating agents containing mixtures of inorganic and organic compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
- B27K5/02—Staining or dyeing wood; Bleaching wood
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K9/00—Chemical or physical treatment of reed, straw, or similar material
- B27K9/007—Straw
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K2240/00—Purpose of the treatment
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Forests & Forestry (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Organic Chemistry (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a formula and a production method of a pastel violet wheat straw dye. According to the formula, exacum affine, antimony ion solution, alumen, iron ion compound solution, and mineral water are taken as main raw materials. The production method comprises following steps: material choosing, material cutting, drying, immersing, hot boiling, mixing, precipitating, dyeing, and finished product obtaining. The pastel violet wheat straw dye is pure natural, and is green and friendly to the environment; no pollution is caused; no toxic or side effect on human body is caused; and the pastel violet wheat straw dye is prepared from pure natural plant materials.
Description
technical field:
the present invention relates to a kind of vegetable dye, particularly relates to a kind of formula and the production method of preparing purple powder wheat straw dye
background technology:
in prior art, the method that the main raw material Wheat Straw making straw patchwork dyes purple powder is had a variety of, but most dyestuff is chemical dye, the purple powder dyed is impure, easily fade, not only not environmentally, some dyes even can produce toxic gas in the process of dye system, threatens the health of human body.
thus, make field at straw patchwork and lack a kind of vegetable dye Wheat Straw being dyed different colours, particularly Wheat Straw is dyed the natural plant dyestuff of purple powder, not only color is pure for the purple powder Wheat Straw that it dyes, and the straw patchwork made with its material is bright and new beautiful, not easily fades, and environmental protection, works give out plant fragrance for a long time, have the physical and mental health of easy people, and what degree was different solves other poisonous and harmful chemical dye in dye process processed to the prestige evil that people's health causes.
summary of the invention:
the object of the present invention is to provide a kind of pure natural, pollution-free, environmental protection, a kind of formula and the production method preparing purple powder wheat straw dye be mixed with natural plant that the person is had no side effect
the object of the present invention is achieved like this.It is that the raw material of being joined by following weight is made, Persian violet 10-30 part, antimony ion solution 10-30 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
the formula optimization weight proportion scope preparing purple powder wheat straw dye of the present invention is, wherein the weight proportion of various raw material is Persian violet 10-25 part, antimony ion solution 10-25 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
the optimum weight ratio range preparing purple powder wheat straw dye of the present invention is that wherein the weight proportion of various raw material is: Persian violet 15 parts, antimony ion solution 15 parts, alum 8 parts, ferric ion compounds solution 8 parts, mineral water 65 parts.
above-mentioned each component is made the production method of purple powder wheat straw dye of the present invention, it is characterized in that: technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select the Persian violet, antimony ion solution, alum, ferric ion compounds solution, the mineral water that meet national health and quality standard for subsequent use; B, blank, the raw material Persian violet selected is cut into bulk; C, oven dry, the Persian violet raw material of the shape that is cut into small pieces is placed in stoving oven mummification, temperature controls at 100-120 DEG C, 30 minutes time, makes raw materials evaporate moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, add antimony ion solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure purple powder cellulose solution; H, dyeing, the temperature of 100 liters of pure purple powder cellulose solutions is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb purple powder cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to purple powder Wheat Straw finished product at room temperature.
production method advantage of the present invention is: 1, select raw material, scientific formulation, color is pure; 2, do not add sanitas in product, industrial chemicals, pure natural, to human body without any injury, the straw patchwork works made with its raw material not only distribute Scent, and anticorrosive; 3 raw material sources are extensive, add process line short, the easy processing and manufacturing of product.
Embodiment
below in conjunction with specific embodiment, the present invention is further illustrated:
embodiment 1:
the formulation weight ratio range preparing purple powder wheat straw dye of the present invention is: Persian violet 10-30 part, antimony ion solution 10-30 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
embodiment 2:
the formula optimization weight proportion scope preparing purple powder wheat straw dye of the present invention is: Persian violet 10-25 part, antimony ion solution 10-25 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
embodiment 3:
the formula optimum weight ratio range preparing purple powder wheat straw dye of the present invention is: wherein the weight proportion of various raw material is, Persian violet 15 parts, antimony ion solution 15 parts, alum 8 parts, ferric ion compounds solution 8 parts, mineral water 65 parts.
above-mentioned each component is made the production method of purple powder wheat straw dye of the present invention, technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select the Persian violet, antimony ion solution, alum, ferric ion compounds solution, the mineral water that meet national health and quality standard for subsequent use; B, blank, the raw material Persian violet selected is cut into bulk; C, oven dry, the Persian violet raw material of the shape that is cut into small pieces is placed in stoving oven mummification, temperature controls at 100-120 DEG C, 30 minutes time, makes raw materials evaporate moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, add antimony ion solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure purple powder cellulose solution; H, dyeing, the temperature of 100 liters of pure purple powder cellulose solutions is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb purple powder cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to purple powder Wheat Straw finished product at room temperature.
Claims (4)
1. prepare the formula of purple powder wheat straw dye for one kind, it is characterized in that: it is made up of the raw material of following weight proportioning, Persian violet 10-30 part, antimony ion solution 10-30 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
2. prepare a formula for purple powder wheat straw dye, it is characterized in that: wherein the weight proportion of various raw material is, Persian violet 10-25 part, antimony ion solution 10-25 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
3. prepare a formula for purple powder wheat straw dye, it is characterized in that: wherein the weight proportion of various raw material is, Persian violet 15 parts, antimony ion solution 15 parts, alum 8 parts, ferric ion compounds solution 8 parts, mineral water 65 parts.
4. a kind of production method preparing purple powder wheat straw dye formula according to claim 1-3, it is characterized in that: technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select the Persian violet, antimony ion solution, alum, ferric ion compounds solution, the mineral water that meet national health and quality standard for subsequent use; B, blank, the raw material Persian violet selected is cut into bulk; C, oven dry, the Persian violet raw material of the shape that is cut into small pieces is placed in stoving oven mummification, temperature controls at 100-120 DEG C, 30 minutes time, makes raw materials evaporate moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, add antimony ion solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure purple powder cellulose solution; H, dyeing, the temperature of 100 liters of pure purple powder cellulose solutions is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb purple powder cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to purple powder Wheat Straw finished product at room temperature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310545736.2A CN104629411A (en) | 2013-11-07 | 2013-11-07 | Formula and production method of pastel violet wheat straw dye |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310545736.2A CN104629411A (en) | 2013-11-07 | 2013-11-07 | Formula and production method of pastel violet wheat straw dye |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104629411A true CN104629411A (en) | 2015-05-20 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310545736.2A Pending CN104629411A (en) | 2013-11-07 | 2013-11-07 | Formula and production method of pastel violet wheat straw dye |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106700621A (en) * | 2015-08-11 | 2017-05-24 | 哈尔滨市工艺美术有限责任公司 | Red-purple corn straw dye and production method thereof |
-
2013
- 2013-11-07 CN CN201310545736.2A patent/CN104629411A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106700621A (en) * | 2015-08-11 | 2017-05-24 | 哈尔滨市工艺美术有限责任公司 | Red-purple corn straw dye and production method thereof |
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Application publication date: 20150520 |