CN104629453A - Formula for preparing dark blue wheat straw dye and production method thereof - Google Patents
Formula for preparing dark blue wheat straw dye and production method thereof Download PDFInfo
- Publication number
- CN104629453A CN104629453A CN201310551099.XA CN201310551099A CN104629453A CN 104629453 A CN104629453 A CN 104629453A CN 201310551099 A CN201310551099 A CN 201310551099A CN 104629453 A CN104629453 A CN 104629453A
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- Prior art keywords
- wheat straw
- mazarine
- raw material
- dye
- alum
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K9/00—Chemical or physical treatment of reed, straw, or similar material
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Forests & Forestry (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Paper (AREA)
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Abstract
The invention discloses a formula for preparing dark blue wheat straw dye and a production method thereof. The dye is mainly composed of leaves and stalks of indigo plant, cornflower, alum, an iron ion compound solution, and mineral water. The main procedure of dyed wheat straw production comprises the following steps: material choosing, material cutting, drying, soaking, boiling, mixing, precipitating, dyeing, and finishing. The dye is prepared from pure natural plants, is natural, pollution-free, green, and environment-friendly, and does not have any side or toxic effect to human body.
Description
technical field:
the present invention relates to a kind of vegetable dye, particularly relates to a kind of formula and the production method of preparing mazarine wheat straw dye.
background technology:
in prior art, the main raw material Wheat Straw making straw patchwork is dyed navy blue method to be had a variety of, but most dyestuff is chemical dye, the mazarine dyed is impure, easily fade, not only not environmentally, some dyes even can produce toxic gas in the process of dye system, threatens the health of human body.
thus, make field at straw patchwork and lack a kind of vegetable dye Wheat Straw being dyed different colours, particularly Wheat Straw is dyed navy blue natural plant dyestuff, not only color is pure for the mazarine Wheat Straw that it dyes, and the straw patchwork made with its material is bright and new beautiful, not easily fades, and environmental protection, works give out plant fragrance for a long time, have the physical and mental health of easy people, and what degree was different solves other poisonous and harmful chemical dye in dye process processed to the prestige evil that people's health causes.
summary of the invention:
the object of the present invention is to provide a kind of pure natural, pollution-free, environmental protection, a kind of formula and the production method preparing mazarine wheat straw dye be mixed with natural plant that the person is had no side effect.
the object of the present invention is achieved like this.It is that the raw material of being joined by following weight is made, indigo plant leaf stalk 10-30 part, Minor centaury 10-30 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
the formula optimization weight proportion scope preparing mazarine wheat straw dye of the present invention is, wherein the weight proportion of various raw material is indigo plant leaf stalk 10-25 part, Minor centaury 10-25 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
the optimum weight ratio range preparing mazarine wheat straw dye of the present invention is that wherein the weight proportion of various raw material is: indigo plant leaf stalk 15 parts, Minor centaury 15 parts, alum 8 parts, ferric ion compounds solution 8 parts, mineral water 65 parts.
above-mentioned each component is made the production method of mazarine wheat straw dye of the present invention, technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select the indigo plant leaf stalk, Minor centaury, alum, ferric ion compounds solution, the mineral water that meet national health and quality standard for subsequent use; B, blank, by the raw material selected except alum, ferric ion compounds solution, mineral water are cut into bulk respectively; C, oven dry, the shape raw material that will be cut into small pieces are placed in stoving oven mummification respectively, and temperature controls at 100-120 DEG C, 30 minutes time, make raw materials evaporate moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure mazarine cellulose solution; H, dyeing, the temperature of 100 liters of pure mazarine cellulose solutions is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb mazarine cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to mazarine Wheat Straw finished product at room temperature.
production method advantage of the present invention is: 1, select raw material, scientific formulation, color is pure; 2, do not add sanitas in product, industrial chemicals, pure natural, to human body without any injury, the straw patchwork works made with its raw material not only distribute Scent, and anticorrosive; 3 raw material sources are extensive, add process line short, the easy processing and manufacturing of product.
Embodiment
below in conjunction with specific embodiment, the present invention is further illustrated:
embodiment 1:
the formulation weight ratio range preparing mazarine wheat straw dye of the present invention is: indigo plant leaf stalk 10-30 part, Minor centaury 10-30 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
embodiment 2:
the formula optimization weight proportion scope preparing mazarine wheat straw dye of the present invention is: indigo plant leaf stalk 10-25 part, Minor centaury 10-25 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
embodiment 3:
the formula optimum weight ratio range preparing mazarine wheat straw dye of the present invention is: wherein the weight proportion of various raw material is, indigo plant leaf stalk 15 parts, Minor centaury 15 parts, alum 8 parts, ferric ion compounds solution 8 parts, mineral water 65 parts.
above-mentioned each component is made the production method of mazarine wheat straw dye of the present invention, technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select the indigo plant leaf stalk, Minor centaury, alum, ferric ion compounds solution, the mineral water that meet national health and quality standard for subsequent use; B, blank, by the raw material selected except alum, ferric ion compounds solution, mineral water are cut into bulk respectively; C, oven dry, the shape raw material that will be cut into small pieces are placed in stoving oven mummification respectively, and temperature controls at 100-120 DEG C, 30 minutes time, make raw materials evaporate moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure mazarine cellulose solution; H, dyeing, the temperature of 100 liters of pure mazarine cellulose solutions is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb mazarine cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to mazarine Wheat Straw finished product at room temperature.
Claims (4)
1. prepare a formula for mazarine wheat straw dye, it is characterized in that: it is made up of the raw material of following weight proportioning, indigo plant leaf stalk 10-30 part, Minor centaury 10-30 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
2. prepare a formula for mazarine wheat straw dye, it is characterized in that: wherein the weight proportion of various raw material is, indigo plant leaf stalk 10-25 part, Minor centaury 10-25 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
3. prepare a formula for mazarine wheat straw dye, it is characterized in that: wherein the weight proportion of various raw material is, indigo plant leaf stalk 15 parts, Minor centaury 15 parts, alum 8 parts, ferric ion compounds solution 8 parts, mineral water 65 parts.
4. a kind of production method preparing mazarine wheat straw dye formula according to claim 1-3, it is characterized in that: technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select the indigo plant leaf stalk, Minor centaury, alum, ferric ion compounds solution, the mineral water that meet national health and quality standard for subsequent use; B, blank, by the raw material selected except alum, ferric ion compounds solution, mineral water are cut into bulk respectively; C, oven dry, the shape raw material that will be cut into small pieces are placed in stoving oven mummification respectively, and temperature controls at 100-120 DEG C, 30 minutes time, make raw materials evaporate moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure mazarine cellulose solution; H, dyeing, the temperature of 100 liters of pure mazarine cellulose solutions is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb mazarine cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to mazarine Wheat Straw finished product at room temperature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310551099.XA CN104629453A (en) | 2013-11-10 | 2013-11-10 | Formula for preparing dark blue wheat straw dye and production method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310551099.XA CN104629453A (en) | 2013-11-10 | 2013-11-10 | Formula for preparing dark blue wheat straw dye and production method thereof |
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| CN104629453A true CN104629453A (en) | 2015-05-20 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106398295A (en) * | 2015-08-11 | 2017-02-15 | 哈尔滨市工艺美术有限责任公司 | Deep-azure corn stalk dye and production method therefor |
-
2013
- 2013-11-10 CN CN201310551099.XA patent/CN104629453A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106398295A (en) * | 2015-08-11 | 2017-02-15 | 哈尔滨市工艺美术有限责任公司 | Deep-azure corn stalk dye and production method therefor |
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| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20150520 |
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| WD01 | Invention patent application deemed withdrawn after publication |