CN104629425A - Formula for preparing dark green wheat straw dye and production method thereof - Google Patents

Formula for preparing dark green wheat straw dye and production method thereof Download PDF

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Publication number
CN104629425A
CN104629425A CN201310550419.XA CN201310550419A CN104629425A CN 104629425 A CN104629425 A CN 104629425A CN 201310550419 A CN201310550419 A CN 201310550419A CN 104629425 A CN104629425 A CN 104629425A
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CN
China
Prior art keywords
wheat straw
raw material
dye
blackish green
alum
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201310550419.XA
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Chinese (zh)
Inventor
马文侠
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Harbin Arts and Crafts Co Ltd
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Harbin Arts and Crafts Co Ltd
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Filing date
Publication date
Application filed by Harbin Arts and Crafts Co Ltd filed Critical Harbin Arts and Crafts Co Ltd
Priority to CN201310550419.XA priority Critical patent/CN104629425A/en
Publication of CN104629425A publication Critical patent/CN104629425A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/52Impregnating agents containing mixtures of inorganic and organic compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K5/00Treating of wood not provided for in groups B27K1/00, B27K3/00
    • B27K5/02Staining or dyeing wood; Bleaching wood
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K9/00Chemical or physical treatment of reed, straw, or similar material
    • B27K9/007Straw
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B61/00Dyes of natural origin prepared from natural sources, e.g. vegetable sources
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K2240/00Purpose of the treatment

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Forests & Forestry (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Paper (AREA)

Abstract

The invention discloses a formula for preparing dark green wheat straw dye and a production method thereof. The dye is mainly composed of locust tree seed, cornflower petal, Chinese tallowtree leaf, alum, an iron ion compound solution, and mineral water. The main procedure of dyed wheat straw production comprises the following steps: material choosing, material cutting, drying, soaking, boiling, mixing, precipitating, dyeing, and finishing. The dye is prepared from pure natural plants, is natural, pollution-free, green, and environment-friendly, and does not have any side or toxic effect to human body.

Description

A kind of formula and production method preparing blackish green wheat straw dye
technical field:
the present invention relates to a kind of vegetable dye, particularly relates to a kind of formula and the production method of preparing blackish green wheat straw dye
background technology:
in prior art, the main raw material Wheat Straw making straw patchwork is dyed cyan method to be had a variety of, but most dyestuff is chemical dye, what dye is blackish green impure, easily fade, not only not environmentally, some dyes even can produce toxic gas in the process of dye system, threaten the health of human body
thus, make field at straw patchwork and lack a kind of vegetable dye Wheat Straw being dyed different colours, particularly Wheat Straw is dyed cyan natural plant dyestuff, not only color is pure for the blackish green Wheat Straw that it dyes, and the straw patchwork made with its material is bright and new beautiful, not easily fades, and environmental protection, works give out plant fragrance for a long time, have the physical and mental health of easy people, and what degree was different solves other poisonous and harmful chemical dye in dye process processed to the prestige evil that people's health causes.
summary of the invention:
the object of the present invention is to provide a kind of pure natural, pollution-free, environmental protection, a kind of formula and the production method preparing blackish green wheat straw dye be mixed with natural plant that the person is had no side effect
the object of the present invention is achieved like this.It is that the raw material of being joined by following weight is made, Chinese scholartree seed 10-30 part, Minor centaury petal 10-30 part, black prostheca 5-15 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
the formula optimization weight proportion scope of the blackish green wheat straw dye of preparation the present invention is that wherein the weight proportion of various raw material is Chinese scholartree seed 10-25 part, Minor centaury petal 10-25 part, black prostheca 5-10 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
the optimum weight ratio range of the blackish green wheat straw dye of preparation the present invention is that wherein the weight proportion of various raw material is: Chinese scholartree seed 15 parts, 15 parts, Minor centaury petal, black prostheca 8 parts, alum 8 parts, ferric ion compounds solution 8 parts, mineral water 65 parts.
above-mentioned each component is made the production method of the blackish green wheat straw dye of the present invention, technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select the Chinese scholartree seed, Minor centaury petal, black prostheca, alum, ferric ion compounds solution, the mineral water that meet national health and quality standard for subsequent use; B, blank, by the raw material selected except alum, ferric ion compounds solution, mineral water are cut into bulk respectively; C, oven dry, the shape raw material that will be cut into small pieces are placed in stoving oven mummification respectively, and temperature controls at 100-120 DEG C, 30 minutes time, make raw materials evaporate moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure blackish green cellulose solution; H, dyeing, the temperature of 100 liters of pure blackish green cellulose solutions is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb blackish green cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to blackish green Wheat Straw finished product at room temperature.
production method advantage of the present invention is: 1, select raw material, scientific formulation, color is pure; 2, do not add sanitas in product, industrial chemicals, pure natural, to human body without any injury, the straw patchwork works made with its raw material not only distribute Scent, and anticorrosive; 3 raw material sources are extensive, add process line short, the easy processing and manufacturing of product.
Embodiment
below in conjunction with specific embodiment, the present invention is further illustrated:
embodiment 1:
the formulation weight ratio range of the blackish green wheat straw dye of preparation the present invention is: Chinese scholartree seed 10-30 part, Minor centaury petal 10-30 part, black prostheca 5-15 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
embodiment 2:
the formula optimization weight proportion scope of the blackish green wheat straw dye of preparation the present invention is: Chinese scholartree seed 10-25 part, Minor centaury petal 10-25 part, black prostheca 5-10 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
embodiment 3:
the formula optimum weight ratio range of the blackish green wheat straw dye of preparation the present invention is: wherein the weight proportion of various raw material is, Chinese scholartree seed 15 parts, 15 parts, Minor centaury petal, black prostheca 8 parts, alum 8 parts, ferric ion compounds solution 8 parts, mineral water 65 parts.
above-mentioned each component is made the production method of the blackish green wheat straw dye of the present invention, technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select the Chinese scholartree seed, Minor centaury petal, black prostheca, alum, ferric ion compounds solution, the mineral water that meet national health and quality standard for subsequent use; B, blank, by the raw material selected except alum, ferric ion compounds solution, mineral water are cut into bulk respectively; C, oven dry, the shape raw material that will be cut into small pieces are placed in stoving oven mummification respectively, and temperature controls at 100-120 DEG C, 30 minutes time, make raw materials evaporate moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure blackish green cellulose solution; H, dyeing, the temperature of 100 liters of pure blackish green cellulose solutions is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb blackish green cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to blackish green Wheat Straw finished product at room temperature.

Claims (4)

1. prepare the formula of blackish green wheat straw dye for one kind, it is characterized in that: it is made up of the raw material of following weight proportioning, Chinese scholartree seed 10-30 part, Minor centaury petal 10-30 part, black prostheca 5-15 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
2. prepare the formula of blackish green wheat straw dye for one kind, it is characterized in that: wherein the weight proportion of various raw material is, Chinese scholartree seed 10-25 part, Minor centaury petal 10-25 part, black prostheca 5-10 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
3. prepare a formula for blackish green wheat straw dye, it is characterized in that: wherein the weight proportion of various raw material is, Chinese scholartree seed 15 parts, 15 parts, Minor centaury petal, black prostheca 8 parts, alum 8 parts, ferric ion compounds solution 8 parts, mineral water 65 parts.
4. a kind of production method preparing blackish green wheat straw dye formula according to claim 1-3, it is characterized in that: technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select the Chinese scholartree seed, Minor centaury petal, black prostheca, alum, ferric ion compounds solution, the mineral water that meet national health and quality standard for subsequent use; B, blank, by the raw material selected except alum, ferric ion compounds solution, mineral water are cut into bulk respectively; C, oven dry, the shape raw material that will be cut into small pieces are placed in stoving oven mummification respectively, and temperature controls at 100-120 DEG C, 30 minutes time, make raw materials evaporate moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure blackish green cellulose solution; H, dyeing, the temperature of 100 liters of pure blackish green cellulose solutions is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb blackish green cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to blackish green Wheat Straw finished product at room temperature.
CN201310550419.XA 2013-11-08 2013-11-08 Formula for preparing dark green wheat straw dye and production method thereof Pending CN104629425A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310550419.XA CN104629425A (en) 2013-11-08 2013-11-08 Formula for preparing dark green wheat straw dye and production method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201310550419.XA CN104629425A (en) 2013-11-08 2013-11-08 Formula for preparing dark green wheat straw dye and production method thereof

Publications (1)

Publication Number Publication Date
CN104629425A true CN104629425A (en) 2015-05-20

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Application Number Title Priority Date Filing Date
CN201310550419.XA Pending CN104629425A (en) 2013-11-08 2013-11-08 Formula for preparing dark green wheat straw dye and production method thereof

Country Status (1)

Country Link
CN (1) CN104629425A (en)

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WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20150520

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