CN104629412A - Formula and production method of black wheat straw dye - Google Patents
Formula and production method of black wheat straw dye Download PDFInfo
- Publication number
- CN104629412A CN104629412A CN201310545741.3A CN201310545741A CN104629412A CN 104629412 A CN104629412 A CN 104629412A CN 201310545741 A CN201310545741 A CN 201310545741A CN 104629412 A CN104629412 A CN 104629412A
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- China
- Prior art keywords
- wheat straw
- black
- raw material
- solution
- alum
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K9/00—Chemical or physical treatment of reed, straw, or similar material
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Forests & Forestry (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a formula and a production method of a black wheat straw dye. According to the formula, black flower, copperas, alumen, iron ion compound solution, and mineral water are taken as main raw materials. The production method comprises following steps: material choosing, material cutting, drying, immersing, heat boiling, mixing, precipitating, dyeing, and finished product obtaining. The black wheat straw dye is pure natural, and is green and friendly to the environment; no pollution is caused; no toxic or side effect on human body is caused; and the black wheat straw dye is prepared from pure natural plant materials.
Description
technical field:
the present invention relates to a kind of vegetable dye, particularly relates to a kind of formula and the production method of preparing black wheat straw dye
background technology:
in prior art, the method that the main raw material Wheat Straw making straw patchwork dyes black is had a variety of, but most dyestuff is chemical dye, the black dyed is impure, easily fades, not only not environmentally, some dyes even can produce toxic gas in the process of dye system, threatens the health of human body
thus, make field at straw patchwork and lack a kind of vegetable dye Wheat Straw being dyed different colours, particularly Wheat Straw is dyed the natural plant dyestuff of black, not only color is pure for the black Wheat Straw that it dyes, and the straw patchwork made with its material is bright and new beautiful, not easily fades, and environmental protection, works give out plant fragrance for a long time, have the physical and mental health of easy people, and what degree was different solves other poisonous and harmful chemical dye in dye process processed to the prestige evil that people's health causes.
summary of the invention:
the object of the present invention is to provide a kind of pure natural, pollution-free, environmental protection, a kind of formula and the production method preparing black wheat straw dye be mixed with natural plant that the person is had no side effect
the object of the present invention is achieved like this.It is that the raw material of being joined by following weight is made, black colored 20-40 part, green vitriol 5-15 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
the formula optimization weight proportion scope preparing black wheat straw dye of the present invention is that wherein the weight proportion of various raw material is, black colored 20-35 part, green vitriol 5-10 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
the optimum weight ratio range preparing black wheat straw dye of the present invention is that wherein the weight proportion of various raw material is: black spend 30 parts, green vitriol 8 parts, alum 8 parts, ferric ion compounds solution 8 parts, mineral water 60 parts.
above-mentioned each component is made the production method of black wheat straw dye of the present invention, technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select the black flower, green vitriol, alum, ferric ion compounds solution, the mineral water that meet national health and quality standard for subsequent use; B, blank, by the raw material selected except green vitriol, alum, ferric ion compounds solution, mineral water are cut into bulk respectively; C, oven dry, will be cut into block stock and be placed in stoving oven mummification respectively, temperature controls at 100-120 DEG C, 30 minutes time, makes evaporation raw material moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure melanochrome solution; H, dyeing, the temperature of 100 liters of pure melanochrome solution is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb melanochrome solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to black Wheat Straw finished product at room temperature.
production method advantage of the present invention is: 1, select raw material, scientific formulation, color is pure; 2, do not add sanitas in product, industrial chemicals, pure natural, to human body without any injury, the straw patchwork works made with its raw material not only distribute Scent, and anticorrosive; 3 raw material sources are extensive, add process line short, the easy processing and manufacturing of product.
Embodiment
below in conjunction with specific embodiment, the present invention is further illustrated:
embodiment 1:
the formulation weight ratio range preparing black wheat straw dye of the present invention is: black colored 20-40 part, green vitriol 5-15 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
embodiment 2:
the formula optimization weight proportion scope preparing black wheat straw dye of the present invention is: black colored 20-35 part, green vitriol 5-10 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
embodiment 3:
the formula optimum weight ratio range preparing black wheat straw dye of the present invention is: black spend 30 parts, green vitriol 8 parts, alum 8 parts, ferric ion compounds solution 8 parts, mineral water 60 parts.
above-mentioned each component is made the production method of black wheat straw dye of the present invention, technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select the black flower, green vitriol, alum, ferric ion compounds solution, the mineral water that meet national health and quality standard for subsequent use; B, blank, by the raw material selected except green vitriol, alum, ferric ion compounds solution, mineral water are cut into bulk respectively; C, oven dry, will be cut into block stock and be placed in stoving oven mummification respectively, temperature controls at 100-120 DEG C, 30 minutes time, makes evaporation raw material moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure melanochrome solution; H, dyeing, the temperature of 100 liters of pure melanochrome solution is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb melanochrome solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to black Wheat Straw finished product at room temperature.
Claims (4)
1. prepare a formula for black wheat straw dye, it is characterized in that: it is made up of the raw material of following weight proportioning, black colored 20-40 part, green vitriol 5-15 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
2. prepare a formula for black wheat straw dye, it is characterized in that: wherein the weight proportion of various raw material is,
Black colored 20-35 part, green vitriol 5-10 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
3. prepare a formula for black wheat straw dye, it is characterized in that: wherein the weight proportion of various raw material is,
Black spend 30 parts, green vitriol 8 parts, alum 8 parts, ferric ion compounds solution 8 parts, mineral water 60 parts.
4. a kind of production method preparing black wheat straw dye formula according to claim 1-3, it is characterized in that: technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select the black flower, green vitriol, alum, ferric ion compounds solution, the mineral water that meet national health and quality standard for subsequent use; B, blank, by the raw material selected except green vitriol, alum, ferric ion compounds solution, mineral water are cut into bulk respectively; C, oven dry, will be cut into block stock and be placed in stoving oven mummification respectively, temperature controls at 100-120 DEG C, 30 minutes time, makes evaporation raw material moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure melanochrome solution; H, dyeing, the temperature of 100 liters of pure melanochrome solution is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb melanochrome solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to black Wheat Straw finished product at room temperature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310545741.3A CN104629412A (en) | 2013-11-07 | 2013-11-07 | Formula and production method of black wheat straw dye |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310545741.3A CN104629412A (en) | 2013-11-07 | 2013-11-07 | Formula and production method of black wheat straw dye |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104629412A true CN104629412A (en) | 2015-05-20 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310545741.3A Pending CN104629412A (en) | 2013-11-07 | 2013-11-07 | Formula and production method of black wheat straw dye |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104629412A (en) |
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2013
- 2013-11-07 CN CN201310545741.3A patent/CN104629412A/en active Pending
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| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20150520 |
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| WD01 | Invention patent application deemed withdrawn after publication |