CN104629422A - Formula and production method of dark gray wheat straw dye - Google Patents

Formula and production method of dark gray wheat straw dye Download PDF

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Publication number
CN104629422A
CN104629422A CN201310546324.0A CN201310546324A CN104629422A CN 104629422 A CN104629422 A CN 104629422A CN 201310546324 A CN201310546324 A CN 201310546324A CN 104629422 A CN104629422 A CN 104629422A
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CN
China
Prior art keywords
wheat straw
raw material
lead
solution
dye
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201310546324.0A
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Chinese (zh)
Inventor
马文侠
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Harbin Arts and Crafts Co Ltd
Original Assignee
Harbin Arts and Crafts Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Harbin Arts and Crafts Co Ltd filed Critical Harbin Arts and Crafts Co Ltd
Priority to CN201310546324.0A priority Critical patent/CN104629422A/en
Publication of CN104629422A publication Critical patent/CN104629422A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/52Impregnating agents containing mixtures of inorganic and organic compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K5/00Treating of wood not provided for in groups B27K1/00, B27K3/00
    • B27K5/02Staining or dyeing wood; Bleaching wood
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K9/00Chemical or physical treatment of reed, straw, or similar material
    • B27K9/007Straw
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B61/00Dyes of natural origin prepared from natural sources, e.g. vegetable sources
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K2240/00Purpose of the treatment

Abstract

The invention discloses a formula and a production method of a dark gray wheat straw dye. According to the formula, german oak husk, strawberry leaf, alumen, iron ion compound solution, and mineral water are taken as main raw materials. The production method comprises following steps: material choosing, material cutting, drying, immersing, heat boiling, mixing, precipitating, dyeing, and finished product obtaining. The dark gray wheat straw dye is pure natural, and is green and friendly to the environment; no pollution is caused; no toxic or side effect on human body is caused; and the dark gray wheat straw dye is prepared from pure natural plant materials.

Description

A kind of formula and production method preparing lead wheat straw dye
technical field:
the present invention relates to a kind of vegetable dye, particularly relates to a kind of formula and the production method of preparing lead wheat straw dye.
background technology:
in prior art, the main raw material Wheat Straw making straw patchwork is dyed dimmed method to be had a variety of, but most dyestuff is chemical dye, the lead dyed is impure, easily fade, not only not environmentally, some dyes even can produce toxic gas in the process of dye system, threatens the health of human body.
thus, make field at straw patchwork and lack a kind of vegetable dye Wheat Straw being dyed different colours, particularly Wheat Straw is dyed dimmed natural plant dyestuff, not only color is pure for the lead Wheat Straw that it dyes, and the straw patchwork made with its material is bright and new beautiful, not easily fades, and environmental protection, works give out plant fragrance for a long time, have the physical and mental health of easy people, and what degree was different solves other poisonous and harmful chemical dye in dye process processed to the prestige evil that people's health causes.
summary of the invention:
the object of the present invention is to provide a kind of pure natural, pollution-free, environmental protection, a kind of formula and the production method preparing lead wheat straw dye be mixed with natural plant that the person is had no side effect.
the object of the present invention is achieved like this.It is that the raw material of being joined by following weight is made, Quercus acutissima shell 20-40 part, strawberry leaves 10-30 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
the formula optimization weight proportion scope preparing lead wheat straw dye of the present invention is, wherein the weight proportion of various raw material is Quercus acutissima shell 20-35 part, strawberry leaves 10-25 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
the optimum weight ratio range preparing lead wheat straw dye of the present invention is that wherein the weight proportion of various raw material is: 30 parts, Quercus acutissima shell, strawberry leaves 15 parts, alum 8 parts, ferric ion compounds solution 8 parts, mineral water 65 parts.
above-mentioned each component is made the production method of lead wheat straw dye of the present invention, technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select the Quercus acutissima shell, strawberry leaves, alum, ferric ion compounds solution, the mineral water that meet national health and quality standard for subsequent use; B, blank, by the raw material selected except alum, ferric ion compounds solution, mineral water are cut into bulk respectively; C, oven dry, the shape raw material that will be cut into small pieces are placed in stoving oven mummification respectively, and temperature controls at 100-120 DEG C, 30 minutes time, make raw materials evaporate moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure lead cellulose solution; H, dyeing, the temperature of 100 liters of pure lead cellulose solutions is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb lead cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to lead Wheat Straw finished product at room temperature.
production method advantage of the present invention is: 1, select raw material, scientific formulation, color is pure; 2, do not add sanitas in product, industrial chemicals, pure natural, to human body without any injury, the straw patchwork works made with its raw material not only distribute Scent, and anticorrosive; 3 raw material sources are extensive, add process line short, the easy processing and manufacturing of product.
Embodiment
below in conjunction with specific embodiment, the present invention is further illustrated:
embodiment 1:
the formulation weight ratio range preparing lead wheat straw dye of the present invention is: Quercus acutissima shell 20-40 part, strawberry leaves 10-30 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
embodiment 2:
the formula optimization weight proportion scope preparing lead wheat straw dye of the present invention is: Quercus acutissima shell 20-35 part, strawberry leaves 10-25 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
embodiment 3:
the formula optimum weight ratio range preparing lead wheat straw dye of the present invention is: wherein the weight proportion of various raw material is, 30 parts, Quercus acutissima shell, strawberry leaves 15 parts, alum 8 parts, ferric ion compounds solution 8 parts, mineral water 65 parts.
above-mentioned each component is made the production method of lead wheat straw dye of the present invention, technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select the Quercus acutissima shell, strawberry leaves, alum, ferric ion compounds solution, the mineral water that meet national health and quality standard for subsequent use; B, blank, by the raw material selected except alum, ferric ion compounds solution, mineral water are cut into bulk respectively; C, oven dry, the shape raw material that will be cut into small pieces are placed in stoving oven mummification respectively, and temperature controls at 100-120 DEG C, 30 minutes time, make raw materials evaporate moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure lead cellulose solution; H, dyeing, the temperature of 100 liters of pure lead cellulose solutions is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb lead cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to lead Wheat Straw finished product at room temperature.

Claims (4)

1. prepare a formula for lead wheat straw dye, it is characterized in that: it is made up of the raw material of following weight proportioning, Quercus acutissima shell 20-40 part, strawberry leaves 10-30 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
2. prepare a formula for lead wheat straw dye, it is characterized in that: wherein the weight proportion of various raw material is, Quercus acutissima shell 20-35 part, strawberry leaves 10-25 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
3. prepare a formula for lead wheat straw dye, it is characterized in that: wherein the weight proportion of various raw material is, 30 parts, Quercus acutissima shell, strawberry leaves 15 parts, alum 8 parts, ferric ion compounds solution 8 parts, mineral water 65 parts.
4. a kind of production method preparing lead wheat straw dye formula according to claim 1-3, it is characterized in that: technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select the Quercus acutissima shell, strawberry leaves, alum, ferric ion compounds solution, the mineral water that meet national health and quality standard for subsequent use; B, blank, by the raw material selected except alum, ferric ion compounds solution, mineral water are cut into bulk respectively; C, oven dry, the shape raw material that will be cut into small pieces are placed in stoving oven mummification respectively, and temperature controls at 100-120 DEG C, 30 minutes time, make raw materials evaporate moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure lead cellulose solution; H, dyeing, the temperature of 100 liters of pure lead cellulose solutions is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb lead cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to lead Wheat Straw finished product at room temperature.
CN201310546324.0A 2013-11-07 2013-11-07 Formula and production method of dark gray wheat straw dye Pending CN104629422A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310546324.0A CN104629422A (en) 2013-11-07 2013-11-07 Formula and production method of dark gray wheat straw dye

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201310546324.0A CN104629422A (en) 2013-11-07 2013-11-07 Formula and production method of dark gray wheat straw dye

Publications (1)

Publication Number Publication Date
CN104629422A true CN104629422A (en) 2015-05-20

Family

ID=53208683

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201310546324.0A Pending CN104629422A (en) 2013-11-07 2013-11-07 Formula and production method of dark gray wheat straw dye

Country Status (1)

Country Link
CN (1) CN104629422A (en)

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WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20150520

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