CN104621714B - One kind improves brittle dripping pills of cigarette additive and preparation method thereof - Google Patents
One kind improves brittle dripping pills of cigarette additive and preparation method thereof Download PDFInfo
- Publication number
- CN104621714B CN104621714B CN201410729465.0A CN201410729465A CN104621714B CN 104621714 B CN104621714 B CN 104621714B CN 201410729465 A CN201410729465 A CN 201410729465A CN 104621714 B CN104621714 B CN 104621714B
- Authority
- CN
- China
- Prior art keywords
- cigarette additive
- dripping
- dripping pills
- cigarette
- pills
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000006187 pill Substances 0.000 title claims abstract description 79
- 239000000654 additive Substances 0.000 title claims abstract description 44
- 230000000996 additive effect Effects 0.000 title claims abstract description 44
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 44
- 238000002360 preparation method Methods 0.000 title claims abstract description 7
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 18
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 13
- 235000011187 glycerol Nutrition 0.000 claims abstract description 9
- 239000004202 carbamide Substances 0.000 claims abstract description 8
- 239000000463 material Substances 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims abstract description 6
- 235000010413 sodium alginate Nutrition 0.000 claims abstract description 6
- 229940005550 sodium alginate Drugs 0.000 claims abstract description 6
- 239000000661 sodium alginate Substances 0.000 claims abstract description 6
- 239000011229 interlayer Substances 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 3
- 239000000706 filtrate Substances 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 239000003292 glue Substances 0.000 description 15
- 239000000047 product Substances 0.000 description 7
- 230000035807 sensation Effects 0.000 description 6
- 239000002775 capsule Substances 0.000 description 5
- 235000013877 carbamide Nutrition 0.000 description 5
- 238000005336 cracking Methods 0.000 description 3
- 239000004014 plasticizer Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- UZGKAASZIMOAMU-UHFFFAOYSA-N 124177-85-1 Chemical compound NP(=O)=O UZGKAASZIMOAMU-UHFFFAOYSA-N 0.000 description 1
- -1 Carbonic acid Diamides Chemical class 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0216—Applying additives to filter materials the additive being in the form of capsules, beads or the like
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/04—Tobacco smoke filters characterised by their shape or structure
- A24D3/048—Tobacco smoke filters characterised by their shape or structure containing additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/05—Alcohols; Metal alcoholates
- C08K5/053—Polyhydroxylic alcohols
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/16—Nitrogen-containing compounds
- C08K5/21—Urea; Derivatives thereof, e.g. biuret
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
Abstract
The invention belongs to cigarette additive manufacturing technology field, and in particular to one kind improves brittle dripping pills of cigarette additive and preparation method thereof.It is formed by dripping pill lapping and cigarette additive parcel, and wherein dripping pill lapping is made up of following material component by weight mixing：Sodium alginate：Glycerine：Urea：The weight ratio of water is 1~8：0.5~3：1~5：85~100.The present invention can reduce the crushing strength of dripping pill to a certain extent, keep relatively stable water content, so that fragility feel when dripping pill possesses preferable extruding, the significant increase consumption experience of dripping pill product.
Description
Technical field
The invention belongs to cigarette additive manufacturing technology field, and in particular to one kind improves brittle dripping pills of cigarette additive
And preparation method thereof.
Background technology
In the prior art, granted patent " dripping pills of cigarette additive lapping and the dripping pill and dripping pill with its parcel
Using ", that is, a kind of lapping that cigarette additive can be wrapped up is provided, wrapping up additive with it is made dripping pill, then will
This dripping pill is applied in filter rod, and obtained one kind contains cigarette additive, can decide the filter rod of release in its sole discretion by consumer.Should
Lapping formula applied in patent is made up of the raw material of following component and parts by weight：Sodium alginate：Glycerine：Water for (1~
8)：(0.5~5)：(85~100).The crushing strength of dripping pills of cigarette additive is 0.3kPa -2.0kPa, dripping pills of cigarette additive
Rubber thickness be 20 microns -200 microns, a diameter of 2mm -5mm of dripping pills of cigarette additive, the moisture of dripping pills of cigarette additive
For 5% -30%.Because glycerine generally uses as plasticizer, the plasticity and toughness of material can be improved.But cigarette has with dripping pill
Some plasticity and toughness are excessive, can cause consumer in use, and dripping pill could be crushed compared with great strength by feeling to need to use,
Discharge the additive components such as essence therein.This can cause the bad sensation of product usage experience, influence product reputation
Lifting.
Urea, also known as phosphoamide (carbamide), it is a kind of white crystal.One of simplest organic compound.Carbonic acid
Diamides, molecular formula H2NCONH2(CO(NH2)2).Urea is also a kind of widely used plasticizer, but because it
Molecular structure in without hydroxyl, unlike glycerine is so easily combined with water, therefore be added in material, toughness to material and
Moisture absorption sexually revises less.Therefore the fragility of material can be properly increased if replacing glycerine to a certain extent.
The content of the invention
For the above-mentioned deficiency of prior art, improve brittle cigarette the technical problem to be solved in the present invention is to provide one kind and use
Additive dripping pill and preparation method thereof, can be on the basis of it can possess preferable crushing strength, meet Product processing demand, again
Can possess preferable fragility, make dripping pill be more easy to crumb in use, so as to improve cigarette dripping pill product quality.
The technical scheme is that：It is made up of the raw material of following component and parts by weight：
Sodium alginate：Glycerine：Urea：The weight ratio of water is 1~8：0.5~3：1~5：85~100；
The present invention preparation method be：According to the above ratio, above material is well mixed and is placed in that there is heating interlayer
Stirred in retort, interlayer is heated to 70 DEG C with steam, dissolves mixture, is incubated 1~2 hour, stands, and treats that foam floats
Afterwards, filtered under the conditions of being incubated 70 DEG C, gained filtrate is dripping pills of cigarette additive lapping.The viscosity of described sodium alginate
For 0.01~2Pa.s；Glycerine and urea are food grade products.
Described dripping pills of cigarette additive weight is 10mg -40mg, and the crushing strength of dripping pills of cigarette additive is
0.5kPa -5kPa, the rubber thickness of dripping pills of cigarette additive is 20 microns -200 microns, and dripping pills of cigarette additive is a diameter of
2mm -5mm, the moisture of dripping pills of cigarette additive is 1% -15%.
Advantages of the present invention：The present invention is ensureing that dripping pill is isobaric toward friction, the extruding for needing to reach during addition in filter stick
Power, intensity, weight, size requirements that product needs to reach are maintained, the crushing strength of dripping pill can be reduced to a certain extent,
Relatively stable water content is kept, so that fragility feel when dripping pill possesses preferable extruding, significant increase dripping pill product
Consumption experience.
Embodiment
The embodiment of the present invention is described in further detail with reference to embodiment.Following examples are
Laboratory data.
Embodiment 1：
By listed proportioning configuration glue 500ml in table 1, dripping pills of cigarette additive capsule is made using dropping-pill machine.This hair
Dripping machine used in bright is that prior art is existing, and the present invention borrows it and completes the task of the present invention.
The glue of table 1 matches
The glue dripping of configuration is smooth, and dripping pill crushing strength is 3.6kPa, and rubber thickness is 100 microns, dripping pill diameter
3.5mm, dripping pill moisture 10%, dripping pill firmly pinch flexible sensation, and rupture opening is linearly, and sound is not loud and clear enough.
Embodiment 2：
By listed proportioning configuration glue 500ml in table 2, dripping pills of cigarette additive capsule is made using dropping-pill machine.This hair
Dripping machine used in bright is that prior art is existing, and the present invention borrows it and completes the task of the present invention.
The glue of table 2 matches
The glue dripping of configuration is smooth, and dripping pill crushing strength is 2.5kPa, and rubber thickness is 100 microns, dripping pill diameter
3.5mm, dripping pill moisture 5%, dripping pill have firmly pinched fragility sensation, and rupture opening is in emitting shape, and cracking sound has loud and clear.
Embodiment 3：
By listed proportioning configuration glue 500ml in table 3, dripping pills of cigarette additive capsule is made using dropping-pill machine.This hair
Dripping machine used in bright is that prior art is existing, and the present invention borrows it and completes the task of the present invention.
The glue of table 3 matches
The glue dripping of configuration is smooth, and dripping pill crushing strength is 1.2kPa, and rubber thickness is 100 microns, dripping pill diameter
3.5mm, dripping pill moisture 2.3%, dripping pill is easily crumbed, and has fragility sensation, and rupture opening is in emitting shape, and cracking sound has loud and clear.
Embodiment 4：
By listed proportioning configuration glue 500ml in table 4, dripping pills of cigarette additive capsule is made using dropping-pill machine.This hair
Dripping machine used in bright is that prior art is existing, and the present invention borrows it and completes the task of the present invention.
The glue of table 4 matches
The glue dripping of configuration is smooth, and dripping pill crushing strength is 3.6kPa, and rubber thickness is 100 microns, dripping pill diameter
3.5mm, dripping pill moisture 10%, dripping pill firmly pinch flexible sensation, and rupture opening is linearly, and sound is not loud and clear enough.
Embodiment：5
By listed proportioning configuration glue 500ml in table 5, dripping pills of cigarette additive capsule is made using dropping-pill machine.This hair
Dripping machine used in bright is that prior art is existing, and the present invention borrows it and completes the task of the present invention.
The glue of table 5 matches
The glue dripping of configuration is smooth, and dripping pill crushing strength is 1.2kPa, and rubber thickness is 100 microns, dripping pill diameter
3.5mm, dripping pill moisture 2.3%, dripping pill is easily crumbed, and has fragility sensation, and rupture opening is in emitting shape, and cracking sound has loud and clear.
Claims (2)
1. one kind improves brittle dripping pills of cigarette additive, it is formed by dripping pill lapping and cigarette additive parcel, wherein
Dripping pill lapping is made up of following material component by weight mixing：Sodium alginate：Glycerine：Urea：The weight ratio of water be 2~
6：1~2.5：2~3：85~95；Described dripping pills of cigarette additive weight is 10mg -40mg, the pressure of dripping pills of cigarette additive
Broken intensity is 0.5kPa -5kPa, and the rubber thickness of dripping pills of cigarette additive is 20 microns -200 microns, dripping pills of cigarette additive
A diameter of 2mm -5mm, the moisture of dripping pills of cigarette additive is 1% -15%.
A kind of 2. preparation method for improving brittle dripping pills of cigarette additive, according to sodium alginate：Glycerine：Urea：The weight of water
Than for 2~6：1~2.5：2~3：85~95, it will be stirred in the well mixed retort for being placed in that there is heating interlayer of above material
Mix, interlayer is heated to 70 DEG C with steam, dissolves mixture, is incubated 1~2 hour, is filtered under the conditions of being then incubated 70 DEG C, gained
Filtrate is dripping pills of cigarette additive lapping, and dripping pill lapping mixes with cigarette additive produces cigarette additive drop
Ball；Described dripping pills of cigarette additive weight is 10mg -40mg, the crushing strength of dripping pills of cigarette additive for 0.5kPa -
5kPa, the rubber thickness of dripping pills of cigarette additive is 20 microns -200 microns, a diameter of 2mm -5mm of dripping pills of cigarette additive,
The moisture of dripping pills of cigarette additive is 1% -15%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410729465.0A CN104621714B (en) | 2014-12-04 | 2014-12-04 | One kind improves brittle dripping pills of cigarette additive and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410729465.0A CN104621714B (en) | 2014-12-04 | 2014-12-04 | One kind improves brittle dripping pills of cigarette additive and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104621714A CN104621714A (en) | 2015-05-20 |
| CN104621714B true CN104621714B (en) | 2018-01-05 |
Family
ID=53201359
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410729465.0A Active CN104621714B (en) | 2014-12-04 | 2014-12-04 | One kind improves brittle dripping pills of cigarette additive and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104621714B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105105334A (en) * | 2015-07-17 | 2015-12-02 | 云南中烟工业有限责任公司 | Spice slow-release filter tip additive with polymer covering film as well as preparation method and application thereof |
| CN106220905B (en) * | 2016-08-30 | 2018-05-25 | 湖北中烟工业有限责任公司 | A kind of raising cigarette dripping pill lapping of dripping pill stability and preparation method thereof |
| CN109021307A (en) * | 2018-07-05 | 2018-12-18 | 湖北中烟工业有限责任公司 | A kind of sodium alginate-modified cigarette quick-fried pearl composite membrane and preparation method thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1469738A (en) * | 2000-11-09 | 2004-01-21 | �����ʩ���عɷݹ�˾ | Soft capsules comprising a starch mixture having reduced branching degree |
| CA2488923A1 (en) * | 2002-07-16 | 2004-01-22 | Rita Mayur Parikh | Oral care capsules |
| CN1626076A (en) * | 2003-12-11 | 2005-06-15 | 天津天士力制药股份有限公司 | Andrographolide drop pills and preparation method |
| EP1586436A1 (en) * | 2004-04-16 | 2005-10-19 | Swiss Caps Rechte und Lizenzen AG | Process for manufacturing moulded plastomeric parts |
| EP1738751A2 (en) * | 2001-01-12 | 2007-01-03 | Sun Pharmaceutical Industries Limited | Spaced drug delivery system |
| CN102108136A (en) * | 2009-12-25 | 2011-06-29 | 湖北中烟工业有限责任公司 | Tobacco additive dropping pill wrapping material, dropping pill wrapped thereby and application of dropping pill |
-
2014
- 2014-12-04 CN CN201410729465.0A patent/CN104621714B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1469738A (en) * | 2000-11-09 | 2004-01-21 | �����ʩ���عɷݹ�˾ | Soft capsules comprising a starch mixture having reduced branching degree |
| EP1738751A2 (en) * | 2001-01-12 | 2007-01-03 | Sun Pharmaceutical Industries Limited | Spaced drug delivery system |
| CA2488923A1 (en) * | 2002-07-16 | 2004-01-22 | Rita Mayur Parikh | Oral care capsules |
| CN1626076A (en) * | 2003-12-11 | 2005-06-15 | 天津天士力制药股份有限公司 | Andrographolide drop pills and preparation method |
| EP1586436A1 (en) * | 2004-04-16 | 2005-10-19 | Swiss Caps Rechte und Lizenzen AG | Process for manufacturing moulded plastomeric parts |
| CN102108136A (en) * | 2009-12-25 | 2011-06-29 | 湖北中烟工业有限责任公司 | Tobacco additive dropping pill wrapping material, dropping pill wrapped thereby and application of dropping pill |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104621714A (en) | 2015-05-20 |
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| GR01 | Patent grant | ||
| GR01 | Patent grant |