CN104621714A - Tobacco additive dropping pill with improved brittleness and preparation method thereof - Google Patents
Tobacco additive dropping pill with improved brittleness and preparation method thereof Download PDFInfo
- Publication number
- CN104621714A CN104621714A CN201410729465.0A CN201410729465A CN104621714A CN 104621714 A CN104621714 A CN 104621714A CN 201410729465 A CN201410729465 A CN 201410729465A CN 104621714 A CN104621714 A CN 104621714A
- Authority
- CN
- China
- Prior art keywords
- cigarette additive
- dripping
- dripping pills
- dropping pill
- pills
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000006187 pill Substances 0.000 title claims abstract description 90
- 239000000654 additive Substances 0.000 title claims abstract description 52
- 230000000996 additive effect Effects 0.000 title claims abstract description 50
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 235000002637 Nicotiana tabacum Nutrition 0.000 title abstract 8
- 244000061176 Nicotiana tabacum Species 0.000 title 1
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 23
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 15
- 235000011187 glycerol Nutrition 0.000 claims abstract description 11
- 239000004202 carbamide Substances 0.000 claims abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000000463 material Substances 0.000 claims abstract description 9
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims abstract description 8
- 235000010413 sodium alginate Nutrition 0.000 claims abstract description 8
- 239000000661 sodium alginate Substances 0.000 claims abstract description 8
- 229940005550 sodium alginate Drugs 0.000 claims abstract description 8
- 235000019504 cigarettes Nutrition 0.000 claims description 44
- 238000010438 heat treatment Methods 0.000 claims description 4
- 239000011229 interlayer Substances 0.000 claims description 4
- 239000000706 filtrate Substances 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 238000003756 stirring Methods 0.000 claims description 2
- 238000005516 engineering process Methods 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 abstract description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 241000208125 Nicotiana Species 0.000 abstract 7
- 239000003292 glue Substances 0.000 description 15
- 239000000047 product Substances 0.000 description 7
- 239000002775 capsule Substances 0.000 description 5
- 235000013877 carbamide Nutrition 0.000 description 5
- 230000035807 sensation Effects 0.000 description 5
- 238000005336 cracking Methods 0.000 description 3
- 239000004014 plasticizer Substances 0.000 description 2
- UZGKAASZIMOAMU-UHFFFAOYSA-N 124177-85-1 Chemical compound NP(=O)=O UZGKAASZIMOAMU-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 150000001470 diamides Chemical class 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0216—Applying additives to filter materials the additive being in the form of capsules, beads or the like
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/04—Tobacco smoke filters characterised by their shape or structure
- A24D3/048—Tobacco smoke filters characterised by their shape or structure containing additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/05—Alcohols; Metal alcoholates
- C08K5/053—Polyhydroxylic alcohols
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/16—Nitrogen-containing compounds
- C08K5/21—Urea; Derivatives thereof, e.g. biuret
Abstract
The invention belongs to the field of manufacturing technologies of tobacco additives and particularly relates to a tobacco additive dropping pill with improved brittleness and a preparation method of the tobacco additive dropping pill. The tobacco additive dropping pill is formed by wrapping dropping pill wrapping materials and tobacco additives. The dropping pill wrapping materials are formed by mixing raw materials of sodium alginate tech grade, glycerol, urea and water based on the weight ratio being 1-8:0.5-3:1-5:85-100. The tobacco additive dropping pill with improved brittleness and the preparation method of the tobacco additive dropping pill can reduce crushing strength of the dropping pill to a certain extent and maintain stable water content, so the dropping pill can have good brittleness hand feeling when crushed, and consumption experience of dropping pill products is greatly promoted.
Description
Technical field
The invention belongs to cigarette additive manufacturing technology field, be specifically related to a kind of dripping pills of cigarette additive improving fragility and preparation method thereof.
Background technology
In prior art, granted patent " dripping pills of cigarette additive lapping and with dripping pill of its parcel and the application of dripping pill ", namely a kind of lapping that cigarette additive can be wrapped up is provided, dripping pill is made with its parcel additive, again this dripping pill is applied in filter rod, obtained a kind of containing cigarette additive, can be decided in its sole discretion the filter rod of release by consumer.The lapping formula applied in this patent is made up of the raw material of following component and weight portion: sodium alginate: glycerine: water is (1 ~ 8): (0.5 ~ 5): (85 ~ 100).The crushing strength of dripping pills of cigarette additive is 0.3kPa-2.0kPa, and the rubber thickness of dripping pills of cigarette additive is 20 microns-200 microns, and dripping pills of cigarette additive diameter is 2mm-5mm, and the moisture of dripping pills of cigarette additive is 5%-30%.Because glycerine generally uses as plasticizer, plasticity and the toughness of material can be improved.But the plasticity that cigarette dripping pill has and toughness excessive, consumer can be caused in use, sensation needs use comparatively great strength to crush dripping pill, discharge the additive components such as essence wherein.This sensation that product experience can be caused not good, affects the lifting of product reputation.
Urea, also known as phosphoamide (carbamide), is a kind of white crystal.One of the simplest organic compound.The diamides of carbonic acid, molecular formula is H
2nCONH
2(CO (NH
2)
2).Urea is also a kind of widely used plasticizer, but because without hydroxyl in its molecular structure, be so easily combined with water, be therefore added in material unlike glycerine, to the toughness of material and hygroscopicity change not quite.If therefore replace glycerine to a certain extent, the fragility of material suitably can be improved.
Summary of the invention
For the above-mentioned deficiency of prior art, the technical problem to be solved in the present invention is to provide a kind of dripping pills of cigarette additive improving fragility and preparation method thereof, can can possess better crushing strength, meet on the basis of Product processing demand, better fragility can be possessed again, dripping pill is in use more easily crumbed, thus improves cigarette dripping pill product quality.
Technical scheme of the present invention is: it is made up of the raw material of following component and weight portion:
Sodium alginate: glycerine: urea: the weight ratio of water is 1 ~ 8:0.5 ~ 3:1 ~ 5:85 ~ 100;
Preparation method of the present invention is: according to the above ratio, by above mixing of materials evenly and be placed in the retort with heating interlayer and stir, interlayer Steam Heating is to 70 DEG C, mixture is dissolved, be incubated 1 ~ 2 hour, leave standstill, after foam floats, filter under being incubated 70 DEG C of conditions, gained filtrate is dripping pills of cigarette additive lapping.The viscosity of described sodium alginate is 0.01 ~ 2Pa.s; Glycerine and urea are food grade products.
Described dripping pills of cigarette additive weight is 10mg-40mg, the crushing strength of dripping pills of cigarette additive is 0.5kPa-5kPa, the rubber thickness of dripping pills of cigarette additive is 20 microns-200 microns, dripping pills of cigarette additive diameter is 2mm-5mm, and the moisture of dripping pills of cigarette additive is 1%-15%.
Advantage of the present invention: the friction that the present invention needs when having ensured that dripping pill adds in filter stick to reach, extruding equal pressure, maintain intensity, weight, size requirements that product needed reaches, the crushing strength of dripping pill can be reduced to a certain extent, keep more stable water content, thus fragility feel when making dripping pill possess preferably extruding, the significant increase consumption experience of dripping pill product.
Detailed description of the invention
Below in conjunction with embodiment, the specific embodiment of the present invention is described in further detail.Following examples are laboratory data.
Embodiment 1:
By proportioning configuration glue 500ml listed in table 1, dropping-pill machine is used to make dripping pills of cigarette additive capsule.Dripping machine used in the present invention is that prior art is existing, and the present invention uses it and completes task of the present invention.
Table 1 glue proportioning
The glue dripping of configuration is smooth, and dripping pill crushing strength is 3.6kPa, and rubber thickness is 100 microns, dripping pill diameter 3.5mm, dripping pill moisture 10%, and dripping pill firmly pinches flexible sensation, and the opening that breaks is linearly, and sound is loud and clear not.
Embodiment 2:
By proportioning configuration glue 500ml listed in table 2, dropping-pill machine is used to make dripping pills of cigarette additive capsule.Dripping machine used in the present invention is that prior art is existing, and the present invention uses it and completes task of the present invention.
Table 2 glue proportioning
The glue dripping of configuration is smooth, and dripping pill crushing strength is 2.5kPa, and rubber thickness is 100 microns, dripping pill diameter 3.5mm, dripping pill moisture 5%, and dripping pill has firmly pinched fragility sensation, and the opening that breaks is emitting shape, and cracking sound has loud and clear.
Embodiment 3:
By proportioning configuration glue 500ml listed in table 3, dropping-pill machine is used to make dripping pills of cigarette additive capsule.Dripping machine used in the present invention is that prior art is existing, and the present invention uses it and completes task of the present invention.
Table 3 glue proportioning
The glue dripping of configuration is smooth, and dripping pill crushing strength is 1.2kPa, and rubber thickness is 100 microns, dripping pill diameter 3.5mm, dripping pill moisture 2.3%, and dripping pill is easily crumbed, and has fragility to feel, the opening that breaks is emitting shape, and cracking sound has loud and clear.
Embodiment 4:
By proportioning configuration glue 500ml listed in table 4, dropping-pill machine is used to make dripping pills of cigarette additive capsule.Dripping machine used in the present invention is that prior art is existing, and the present invention uses it and completes task of the present invention.
Table 4 glue proportioning
The glue dripping of configuration is smooth, and dripping pill crushing strength is 3.6kPa, and rubber thickness is 100 microns, dripping pill diameter 3.5mm, dripping pill moisture 10%, and dripping pill firmly pinches flexible sensation, and the opening that breaks is linearly, and sound is loud and clear not.
Embodiment: 5
By proportioning configuration glue 500ml listed in table 5, dropping-pill machine is used to make dripping pills of cigarette additive capsule.Dripping machine used in the present invention is that prior art is existing, and the present invention uses it and completes task of the present invention.
Table 5 glue proportioning
The glue dripping of configuration is smooth, and dripping pill crushing strength is 1.2kPa, and rubber thickness is 100 microns, dripping pill diameter 3.5mm, dripping pill moisture 2.3%, and dripping pill is easily crumbed, and has fragility to feel, the opening that breaks is emitting shape, and cracking sound has loud and clear.
Claims (6)
1. one kind is improved the dripping pills of cigarette additive of fragility, it is wrapped up by dripping pill lapping and cigarette additive and forming, and wherein dripping pill lapping is made up of by weight mixing following material component: sodium alginate: glycerine: urea: the weight ratio of water is 1 ~ 8:0.5 ~ 3:1 ~ 5:85 ~ 100.
2. a kind of dripping pills of cigarette additive improving fragility according to claim 1, is characterized in that: described dripping pill lapping pulp furnish is sodium alginate: glycerine: urea: the weight ratio of water is 2 ~ 6:1 ~ 2.5:2 ~ 3:85 ~ 95.
3. a kind of dripping pills of cigarette additive improving fragility according to claim 1, it is characterized in that: described dripping pills of cigarette additive weight is 10mg-40mg, the crushing strength of dripping pills of cigarette additive is 0.5kPa-5kPa, the rubber thickness of dripping pills of cigarette additive is 20 microns-200 microns, dripping pills of cigarette additive diameter is 2mm-5mm, and the moisture of dripping pills of cigarette additive is 1%-15%.
4. one kind is improved the preparation preparation method of the dripping pills of cigarette additive of fragility, according to sodium alginate: glycerine: urea: the weight ratio of water is 1 ~ 8:0.5 ~ 3:1 ~ 5:85 ~ 100, by above mixing of materials evenly and be placed in the retort with heating interlayer and stir, interlayer Steam Heating is to 70 DEG C, mixture is dissolved, be incubated 1 ~ 2 hour, then filter under being incubated 70 DEG C of conditions, gained filtrate is dripping pills of cigarette additive lapping, and dripping pill lapping mixes with cigarette additive and obtains dripping pills of cigarette additive.
5. a kind of preparation preparation method improving the dripping pills of cigarette additive of fragility according to claim 4, is characterized in that: described dripping pill lapping pulp furnish is sodium alginate: glycerine: urea: the weight ratio of water is 2 ~ 6:1 ~ 2.5:2 ~ 3:85 ~ 95.
6. a kind of preparation preparation method improving the dripping pills of cigarette additive of fragility according to claim 4, it is characterized in that: described dripping pills of cigarette additive weight is 10mg-40mg, the crushing strength of dripping pills of cigarette additive is 0.5kPa-5kPa, the rubber thickness of dripping pills of cigarette additive is 20 microns-200 microns, dripping pills of cigarette additive diameter is 2mm-5mm, and the moisture of dripping pills of cigarette additive is 1%-15%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410729465.0A CN104621714B (en) | 2014-12-04 | 2014-12-04 | One kind improves brittle dripping pills of cigarette additive and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410729465.0A CN104621714B (en) | 2014-12-04 | 2014-12-04 | One kind improves brittle dripping pills of cigarette additive and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104621714A true CN104621714A (en) | 2015-05-20 |
| CN104621714B CN104621714B (en) | 2018-01-05 |
Family
ID=53201359
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410729465.0A Active CN104621714B (en) | 2014-12-04 | 2014-12-04 | One kind improves brittle dripping pills of cigarette additive and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104621714B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105105334A (en) * | 2015-07-17 | 2015-12-02 | 云南中烟工业有限责任公司 | Spice slow-release filter tip additive with polymer covering film as well as preparation method and application thereof |
| CN106220905A (en) * | 2016-08-30 | 2016-12-14 | 湖北中烟工业有限责任公司 | A kind of drop pill lapping improving cigarette drop pill stability and preparation method thereof |
| CN109021307A (en) * | 2018-07-05 | 2018-12-18 | 湖北中烟工业有限责任公司 | A kind of sodium alginate-modified cigarette quick-fried pearl composite membrane and preparation method thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1469738A (en) * | 2000-11-09 | 2004-01-21 | �����ʩ���عɷݹ�˾ | Soft capsules comprising a starch mixture having reduced branching degree |
| CA2488923A1 (en) * | 2002-07-16 | 2004-01-22 | Rita Mayur Parikh | Oral care capsules |
| CN1626076A (en) * | 2003-12-11 | 2005-06-15 | 天津天士力制药股份有限公司 | Andrographolide drop pills and preparation method |
| EP1586436A1 (en) * | 2004-04-16 | 2005-10-19 | Swiss Caps Rechte und Lizenzen AG | Process for manufacturing moulded plastomeric parts |
| EP1738751A2 (en) * | 2001-01-12 | 2007-01-03 | Sun Pharmaceutical Industries Limited | Spaced drug delivery system |
| CN102108136A (en) * | 2009-12-25 | 2011-06-29 | 湖北中烟工业有限责任公司 | Tobacco additive dropping pill wrapping material, dropping pill wrapped thereby and application of dropping pill |
-
2014
- 2014-12-04 CN CN201410729465.0A patent/CN104621714B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1469738A (en) * | 2000-11-09 | 2004-01-21 | �����ʩ���عɷݹ�˾ | Soft capsules comprising a starch mixture having reduced branching degree |
| EP1738751A2 (en) * | 2001-01-12 | 2007-01-03 | Sun Pharmaceutical Industries Limited | Spaced drug delivery system |
| CA2488923A1 (en) * | 2002-07-16 | 2004-01-22 | Rita Mayur Parikh | Oral care capsules |
| CN1626076A (en) * | 2003-12-11 | 2005-06-15 | 天津天士力制药股份有限公司 | Andrographolide drop pills and preparation method |
| EP1586436A1 (en) * | 2004-04-16 | 2005-10-19 | Swiss Caps Rechte und Lizenzen AG | Process for manufacturing moulded plastomeric parts |
| CN102108136A (en) * | 2009-12-25 | 2011-06-29 | 湖北中烟工业有限责任公司 | Tobacco additive dropping pill wrapping material, dropping pill wrapped thereby and application of dropping pill |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105105334A (en) * | 2015-07-17 | 2015-12-02 | 云南中烟工业有限责任公司 | Spice slow-release filter tip additive with polymer covering film as well as preparation method and application thereof |
| CN106220905A (en) * | 2016-08-30 | 2016-12-14 | 湖北中烟工业有限责任公司 | A kind of drop pill lapping improving cigarette drop pill stability and preparation method thereof |
| CN106220905B (en) * | 2016-08-30 | 2018-05-25 | 湖北中烟工业有限责任公司 | A kind of raising cigarette dripping pill lapping of dripping pill stability and preparation method thereof |
| CN109021307A (en) * | 2018-07-05 | 2018-12-18 | 湖北中烟工业有限责任公司 | A kind of sodium alginate-modified cigarette quick-fried pearl composite membrane and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104621714B (en) | 2018-01-05 |
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