CN104562386B - A kind of novel non-ironing textile and preparation method thereof - Google Patents
A kind of novel non-ironing textile and preparation method thereof Download PDFInfo
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- CN104562386B CN104562386B CN201510055998.XA CN201510055998A CN104562386B CN 104562386 B CN104562386 B CN 104562386B CN 201510055998 A CN201510055998 A CN 201510055998A CN 104562386 B CN104562386 B CN 104562386B
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- 239000004753 textile Substances 0.000 title claims abstract description 41
- 238000010409 ironing Methods 0.000 title claims abstract description 29
- 238000002360 preparation method Methods 0.000 title description 6
- 229920000742 Cotton Polymers 0.000 claims abstract description 39
- 239000000835 fiber Substances 0.000 claims abstract description 25
- 239000004744 fabric Substances 0.000 claims abstract description 17
- 239000004568 cement Substances 0.000 claims abstract description 11
- 239000002131 composite material Substances 0.000 claims abstract description 11
- 241000208202 Linaceae Species 0.000 claims abstract description 9
- 235000004431 Linum usitatissimum Nutrition 0.000 claims abstract description 9
- 238000000034 method Methods 0.000 claims description 54
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 36
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 24
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 20
- 239000007788 liquid Substances 0.000 claims description 19
- 239000003054 catalyst Substances 0.000 claims description 14
- 239000003431 cross linking reagent Substances 0.000 claims description 14
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 claims description 12
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 11
- 229920002472 Starch Polymers 0.000 claims description 11
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 11
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 11
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims description 11
- 239000008107 starch Substances 0.000 claims description 11
- 235000019698 starch Nutrition 0.000 claims description 11
- 239000008367 deionised water Substances 0.000 claims description 10
- 229910021641 deionized water Inorganic materials 0.000 claims description 10
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 10
- 238000004140 cleaning Methods 0.000 claims description 7
- 238000002386 leaching Methods 0.000 claims description 7
- 238000002156 mixing Methods 0.000 claims description 7
- 239000002608 ionic liquid Substances 0.000 claims description 6
- -1 alkyl imidazolium cation Chemical compound 0.000 claims description 5
- 150000001768 cations Chemical class 0.000 claims description 4
- 239000011973 solid acid Substances 0.000 claims description 3
- BPSIOYPQMFLKFR-UHFFFAOYSA-N trimethoxy-[3-(oxiran-2-ylmethoxy)propyl]silane Chemical group CO[Si](OC)(OC)CCCOCC1CO1 BPSIOYPQMFLKFR-UHFFFAOYSA-N 0.000 claims description 3
- 150000001450 anions Chemical class 0.000 claims description 2
- 150000003949 imides Chemical class 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 230000035699 permeability Effects 0.000 abstract description 3
- 230000000474 nursing effect Effects 0.000 abstract 1
- 238000009940 knitting Methods 0.000 description 5
- 238000009987 spinning Methods 0.000 description 5
- 238000003756 stirring Methods 0.000 description 5
- 238000005406 washing Methods 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- LEQAOMBKQFMDFZ-UHFFFAOYSA-N glyoxal Chemical compound O=CC=O LEQAOMBKQFMDFZ-UHFFFAOYSA-N 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 230000037303 wrinkles Effects 0.000 description 2
- 229920000858 Cyclodextrin Polymers 0.000 description 1
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000008065 acid anhydrides Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000001273 butane Substances 0.000 description 1
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 230000002153 concerted effect Effects 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 238000013016 damping Methods 0.000 description 1
- 238000005525 durable press finishing Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 229940015043 glyoxal Drugs 0.000 description 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 description 1
- OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- USHAGKDGDHPEEY-UHFFFAOYSA-L potassium persulfate Chemical group [K+].[K+].[O-]S(=O)(=O)OOS([O-])(=O)=O USHAGKDGDHPEEY-UHFFFAOYSA-L 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- HFHDHCJBZVLPGP-UHFFFAOYSA-N schardinger α-dextrin Chemical compound O1C(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(O)C2O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC2C(O)C(O)C1OC2CO HFHDHCJBZVLPGP-UHFFFAOYSA-N 0.000 description 1
- 239000012209 synthetic fiber Substances 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 239000011975 tartaric acid Substances 0.000 description 1
- 235000002906 tartaric acid Nutrition 0.000 description 1
- 238000009988 textile finishing Methods 0.000 description 1
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- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a kind of novel non-ironing textile, formed by warp thread and weft yarns, warp thread is cotton fiber, account for 80% of fabric weight, weft yarn is polyster fibre and flax fibre, and this textiles is first through Cement Composite Treated by Plasma, after through noniron finish, form novel non-ironing textile, this novel non-ironing textile sucting wet air permeability is good, soft comfortable, maintains the premium properties of natural fabric, has good ironing-free performance simultaneously, dimensionally stable, be easy to nursing, formaldehydeless release, harmless.
Description
Technical field:
The present invention relates to textile finishing technical field, be specifically related to a kind of preparation method of novel non-ironing textile.
Background technology:
The natural fabrics such as cotton, hair, silk, fiber crops are the conventional textile fabrics of a class, have the performance of many excellences, as soft, comfortable and easy to wear, gloss is soft, antistatic property is better.But that is made up of these fibers takes textiles, the problems such as ubiquity creases easily in dress and washing process, easy-care properties is poor, need through follow-up noniron finish to improve its ironing-free performance.
After World War II, occur with synthetic fiber and blending thereof, clothes made by MIXED FABRIC, after washing machine washing, there is good planarization, the dark welcome by consumers in general particularly women, in order to improve the market competitiveness of COTTON FABRIC, doing to improve COTTON FABRIC, noniron finish for the purpose of wet wrinkle resistance receives extensive concern.Traditional wash and wear finisher is resinae (2D resin) mainly, and it arranges rear fabric can discharge a large amount of formaldehyde, harmful.Chinese patent (CN201010284544.7) discloses a kind of formaldehydeless fabric wash and wear finisher, by acrylamide, glyoxal, the polymerisation such as o-2 potassium acid acid anhydride, sulfuric acid and potassium peroxydisulfate forms, fabric ironing-free performance after arrangement is good, but its loss of mechanical properties is larger, and lose the distinctive performance of former natural fabric; It is that the formaldehydeless non-ironing method of fabric is carried out in catalyst concerted catalysis with ionic liquid that Chinese patent (CN201410073345.X) discloses a kind of, its formaldehydeless permanent press finishing agent adopted is 1,2,3, one or more compound in 4-tetrabasic carboxylic acid butane (BTCA), poly, citric acid, tartaric acid, shitosan, cyclodextrin, polyurethane, dissaving polymer, but BTCA is expensive.
Summary of the invention:
The object of this invention is to provide a kind of novel non-ironing textile, this textiles ironing-free performance is good, loss of mechanical properties is little, soft comfortable, remains the premium properties of natural fabric, and sucting wet air permeability is good, and the dressing liquid adopted in preparation process is real environmental protection material, formaldehydeless release, preparation technology is simple, and cost is low.
Another object of the present invention is to provide the preparation method of this textiles.
For achieving the above object, the present invention is by the following technical solutions:
A kind of novel non-ironing textile, formed by warp thread and weft yarns, warp thread is cotton fiber, accounts for 80% of fabric weight, and weft yarn is polyster fibre and flax fibre,
Wherein, cotton fiber first through Cement Composite Treated by Plasma, then through non-ironing process.
Preferred as technique scheme, the detailed process of described cotton fiber Cement Composite Treated by Plasma and non-ironing process is: cleaned by cotton fiber clear water, dry, be placed in plasma apparatus and process, be placed directly in noniron finish liquid after process, two leachings two are pricked, and pick-up is 60-80%, the water cleaning of the cotton fiber flowing after process 2-3 time, dries naturally.
Preferred as technique scheme, cotton fiber plasma process conditions is: the discharge frequency of plasma is 12000Hz, and the processing time is 20-30min.
Preferred as technique scheme, noniron finish liquid is made up of citric acid, acrylamide methviium starch, catalyst, carboxymethyl cellulose, sodium carbonate, crosslinking agent and deionized water.
Preferred as technique scheme, in noniron finish liquid, the percentage by weight of each component is: citric acid 20-50%, acrylamide methviium starch 15-20%, catalyst 2-5%, carboxymethyl cellulose 15-20%, sodium carbonate 10-15%, crosslinking agent 2-6%, all the other are deionized water.
Preferred as technique scheme, in noniron finish liquid, the percentage by weight of each component is: citric acid 30%, acrylamide methviium starch 15%, catalyst 3%, carboxymethyl cellulose 15%, sodium carbonate 10%, crosslinking agent 2%, and all the other are deionized water.
Preferred as technique scheme, described catalyst is the mixture of ionic liquid and solid acid, and the two mass ratio is 3:1.
Preferred as technique scheme; the CATION of described ionic liquid is alkyl imidazolium cation or quaternaries cation, and anion is two (perfluoroalkyl sulfonyl) acid amides ion or two (perfluoroalkyl sulfonyl) imide ionic.
Preferred as technique scheme, described crosslinking agent is silane coupler KH560.
Compared with prior art, the present invention has following beneficial effect:
(1) novel non-ironing textile provided by the invention is by the cotton fiber through non-ironing process as warp thread, and polyster fibre or flax fibre, as weft yarn, are interwoven, both there is good ironing-free performance, remain again the distinctive premium properties of former natural fabric, soft comfortable, sucting wet air permeability is good;
(2) cotton fiber first uses Cement Composite Treated by Plasma before carrying out non-ironing process, fiber is expanded, and cotton fiber is in relaxed state, and the active group on fiber also more comes out, thus better and noniron finish liquid effect, the textiles ironing-free performance obtained is better;
(3) the adding of carboxymethyl cellulose, in noniron finish process can with fiber generation cross-linking reaction, textiles is transmitted faster and dispersive stress between yarn, between fiber when stressed, avoids stress to concentrate, cause the damage of textiles, thus provide the intensity of textiles, decrease the loss of textiles intensity in noniron finish, ionic liquid and solid acid are as catalyst, not volatile, there is good stability, belong to fully natural green environmental protection material;
(4) the present invention adopts citric acid, acrylamide methviium starch as wash and wear finisher, cheap, all belong to formaldehyde-free durable-press finishing, the formaldehydeless release of textiles after arrangement, to human body and environment all harmless, adopt silane coupler KH560 as crosslinking agent, it not only can as bridge crosslinked between wash and wear finisher and fiber, also can be cross-linked between crosslinking agent, thus form more stable three-dimensional net structure, the textiles washability after noniron finish is better.
Detailed description of the invention:
For a better understanding of the present invention, below by embodiment, the present invention is further described, and embodiment, only for explaining the present invention, can not form any restriction to the present invention.
Embodiment 1
(1) cleaned by cotton fiber clear water, dry, be placed in plasma apparatus and process, the discharge frequency of plasma is 8000Hz, takes out stand-by after process;
(2) by citric acid 2g, acrylamide methviium starch 1.5g, carboxymethyl cellulose 1.5g and deionized water mixing, ultrasonic 1h under 500W power, continues to add sodium carbonate 1g, crosslinking agent 0.2g, catalyst 0.2g, stirs 30min, obtains noniron finish liquid;
(3) dip in noniron finish liquid by the cotton fiber through Cement Composite Treated by Plasma, two leachings two are pricked, and pick-up is 60-80%, and the water cleaning of the cotton fiber flowing after process 2-3 time, dries naturally;
(4) cotton fiber of process and polyster fibre or flax fibre are adopted existing spinning method, and adopt knitting to make textiles, 80 DEG C of prebakes, bake 2min at 110 DEG C, obtain novel non-ironing textile.
Embodiment 2
(1) cleaned by cotton fiber clear water, dry, be placed in plasma apparatus and process, the discharge frequency of plasma is 8000Hz, takes out stand-by after process;
(2) by citric acid 5g, acrylamide methviium starch 2g, carboxymethyl cellulose 2g and deionized water mixing, ultrasonic 2h under 500W power, continues to add sodium carbonate 1.5g, crosslinking agent 0.6g, catalyst 0.5g, stirs 60min, obtains noniron finish liquid;
(3) dip in noniron finish liquid by the cotton fiber through Cement Composite Treated by Plasma, two leachings two are pricked, and pick-up is 60-80%, and the water cleaning of the cotton fiber flowing after process 2-3 time, dries naturally;
(4) cotton fiber of process and polyster fibre or flax fibre are adopted existing spinning method, and adopt knitting to make textiles, 90 DEG C of prebakes, bake 5min at 119 DEG C, obtain novel non-ironing textile.
Embodiment 3
(1) cleaned by cotton fiber clear water, dry, be placed in plasma apparatus and process, the discharge frequency of plasma is 8000Hz, takes out stand-by after process;
(2) by citric acid 0.3g, acrylamide methviium starch 1.6g, carboxymethyl cellulose 1.6g and deionized water mixing, ultrasonic 70min under 500W power, continue to add sodium carbonate 1.1g, crosslinking agent 0.3g, catalyst 0.3g, stir 35min, obtain noniron finish liquid;
(3) dip in noniron finish liquid by the cotton fiber through Cement Composite Treated by Plasma, two leachings two are pricked, and pick-up is 60-80%, and the water cleaning of the cotton fiber flowing after process 2-3 time, dries naturally;
(4) cotton fiber of process and polyster fibre or flax fibre are adopted existing spinning method, and adopt knitting to make textiles, 82 DEG C of prebakes, bake 3min at 111 DEG C, obtain novel non-ironing textile.
Embodiment 4
(1) cleaned by cotton fiber clear water, dry, be placed in plasma apparatus and process, the discharge frequency of plasma is 8000Hz, takes out stand-by after process;
(2) by citric acid 4g, acrylamide methviium starch 1.7g, carboxymethyl cellulose 1.7g and deionized water mixing, ultrasonic 80min under 500W power, continue to add sodium carbonate 1.2g, crosslinking agent 0.4g, catalyst 0.4g, stir 40min, obtain noniron finish liquid;
(3) dip in noniron finish liquid by the cotton fiber through Cement Composite Treated by Plasma, two leachings two are pricked, and pick-up is 60-80%, and the water cleaning of the cotton fiber flowing after process 2-3 time, dries naturally;
(4) cotton fiber of process and polyster fibre or flax fibre are adopted existing spinning method, and adopt knitting to make textiles, 84 DEG C of prebakes, bake 4min at 113 DEG C, obtain novel non-ironing textile.
Embodiment 5
(1) cleaned by cotton fiber clear water, dry, be placed in plasma apparatus and process, the discharge frequency of plasma is 8000Hz, takes out stand-by after process;
(2) by citric acid 4.5g, acrylamide methviium starch 1.8g, carboxymethyl cellulose 1.8g and deionized water mixing, ultrasonic 100min under 500W power, continue to add sodium carbonate 1.4g, crosslinking agent 0.5g, catalyst 0.45g, stir 50min, obtain noniron finish liquid;
(3) dip in noniron finish liquid by the cotton fiber through Cement Composite Treated by Plasma, two leachings two are pricked, and pick-up is 60-80%, and the water cleaning of the cotton fiber flowing after process 2-3 time, dries naturally;
(4) cotton fiber of process and polyster fibre or flax fibre are adopted existing spinning method, and adopt knitting to make textiles, 86 DEG C of prebakes, bake 3min at 117 DEG C, obtain novel non-ironing textile.
The novel non-ironing textile prepared in embodiment is carried out mechanical performance and ironing-free performance test, tests as follows:
Get the sample of 20 × 20cm in the textiles prepared from embodiment respectively, as test sample, wherein, comparative example is untreated textiles.
(1) creasy recovery angle test
Carry out conditioning by before test sample test, adopt the test of YG541 type pincher elasticity instrument, it is 10N that sample bears load, and pressing time is 5min, and optical projector can be adopted after release to measure the creasy recovery angle of sample.
(2) surface smoothness test
Test sample is cut into zigzag in case off-clip, according to the every block sample of GB/T8629 regulated procedure process, each process 3 times, by sample according to GB/T6529 specified standard air damping 20h, two angles of clamping sample hang each sample, contrast carry out flatness grading to each sample through washing and smooth appearance degree standard sample.
(3) tensile strength test
L & W tensile strength tester is utilized to test.
Test result is as shown in table 1, and table 2 is fabric wrinkle grade.
Table 1
Table 2
Wherein, SA-5 level is equivalent to standard jig SA-5, and it represents that outward appearance degree is the most smooth, and original smooth appearance degree keeps best, and SA-1 level is equivalent to standard jig SA-1, and it represents that outward appearance degree is least smooth, and original smooth appearance degree keeps the poorest.
From table 1, table 2, novel non-ironing textile surface flatness provided by the invention is good, and ironing-free performance is good, and mechanical performance there is no loss.
Claims (6)
1. a novel non-ironing textile, is characterized in that, is formed by warp thread and weft yarns, and warp thread is cotton fiber, accounts for 80% of fabric weight, and weft yarn is polyster fibre and flax fibre mixing,
Wherein, cotton fiber first through Cement Composite Treated by Plasma, then through non-ironing process;
The detailed process of described cotton fiber Cement Composite Treated by Plasma and non-ironing process is: cleaned by cotton fiber clear water, dry, be placed in plasma apparatus and process, be placed directly in noniron finish liquid after process, two leachings two are pricked, pick-up is 60-80%, and the water cleaning of the cotton fiber flowing after process 2-3 time, dries naturally;
In noniron finish liquid, the percentage by weight of each component is: citric acid 20-50%, acrylamide methviium starch 15-20%, catalyst 2-5%, carboxymethyl cellulose 15-20%, sodium carbonate 10-15%, crosslinking agent 2-6%, and all the other are deionized water.
2. a kind of novel non-ironing textile as claimed in claim 1, it is characterized in that, cotton fiber plasma process conditions is: the discharge frequency of plasma is 12000Hz, and the processing time is 20-30min.
3. a kind of novel non-ironing textile as claimed in claim 1, it is characterized in that, in noniron finish liquid, the percentage by weight of each component is: citric acid 30%, acrylamide methviium starch 15%, catalyst 3%, carboxymethyl cellulose 15%, sodium carbonate 10%, crosslinking agent 2%, all the other are deionized water.
4. a kind of novel non-ironing textile as claimed in claim 1, is characterized in that, described catalyst is the mixture of ionic liquid and solid acid, and the two mass ratio is 3:1.
5. a kind of novel non-ironing textile as claimed in claim 4; it is characterized in that; the CATION of described ionic liquid is alkyl imidazolium cation or quaternaries cation, and anion is two (perfluoroalkyl sulfonyl) acid amides ion or two (perfluoroalkyl sulfonyl) imide ionic.
6. a kind of novel non-ironing textile as claimed in claim 1, is characterized in that, described crosslinking agent is silane coupler KH560.
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| CN105220485B (en) * | 2015-10-20 | 2018-08-10 | 惠州市酷尾巴科技有限公司 | A kind of infant's modified cotton fiber and preparation method thereof based on ionic liquid |
| CN106381598A (en) * | 2016-08-30 | 2017-02-08 | 辽东学院 | Preparing method for easy-care fabric |
| CN106192160A (en) * | 2016-08-31 | 2016-12-07 | 苏州市恒信针织印染有限责任公司 | A kind of wash-and-wear of shirt fabric |
| CN107780200A (en) * | 2017-09-28 | 2018-03-09 | 江苏新瑞贝科技股份有限公司 | A kind of wash and wear finisher and preparation method thereof |
| CN109056153A (en) * | 2018-09-18 | 2018-12-21 | 广东溢达纺织有限公司 | Tatting wash-and-wear fabrics and preparation method thereof |
| CN110904678B (en) * | 2019-12-06 | 2022-04-15 | 武汉纺织大学 | In-situ non-ironing method for cotton fabric by using silane coupling agent and hydroxyethyl methacrylate |
| CN112553897A (en) * | 2020-12-31 | 2021-03-26 | 苏州经贸职业技术学院 | Preparation method of durable super-soft crease-resistant functional agent |
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