CN107780200A - A kind of wash and wear finisher and preparation method thereof - Google Patents

A kind of wash and wear finisher and preparation method thereof Download PDF

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Publication number
CN107780200A
CN107780200A CN201710897076.2A CN201710897076A CN107780200A CN 107780200 A CN107780200 A CN 107780200A CN 201710897076 A CN201710897076 A CN 201710897076A CN 107780200 A CN107780200 A CN 107780200A
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parts
wash
wear finisher
ethanol
minutes
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Inventor
储平
徐有琦
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Jiangsu New Lucky Polytron Technologies Inc
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Jiangsu New Lucky Polytron Technologies Inc
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Priority to CN201710897076.2A priority Critical patent/CN107780200A/en
Publication of CN107780200A publication Critical patent/CN107780200A/en
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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/73Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
    • D06M11/76Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon oxides or carbonates
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/07Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof
    • D06M11/11Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof with halogen acids or salts thereof
    • D06M11/155Halides of elements of Groups 2 or 12 of the Periodic System
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/80Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides
    • D06M11/82Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides with boron oxides; with boric, meta- or perboric acids or their salts, e.g. with borax
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/207Substituted carboxylic acids, e.g. by hydroxy or keto groups; Anhydrides, halides or salts thereof
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/368Hydroxyalkylamines; Derivatives thereof, e.g. Kritchevsky bases
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03Polysaccharides or derivatives thereof
    • D06M15/05Cellulose or derivatives thereof
    • D06M15/09Cellulose ethers
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
    • D06M15/6436Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing amino groups
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/20Treatment influencing the crease behaviour, the wrinkle resistance, the crease recovery or the ironing ease
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/45Shrinking resistance, anti-felting properties

Abstract

The invention discloses a kind of wash and wear finisher and preparation method thereof, the wash and wear finisher is made up of the raw material of following parts by weight:35 parts of magnesium chloride, 35 parts of citric acid, 5 10 parts of sodium acid carbonate, 35 parts of borax, 35 parts of triethanolamine, 5 10 parts of hydroxymethyl cellulose, 5 10 parts of double amido organosilicon emulsions, 35 parts of AEO, 10 15 parts of ethanol, 37 parts of cactus powder, 10 20 parts of deionized water.After the wash and wear finisher application fabric of the present invention, fabric has excellent crease and shrink resistance performance, and outward appearance is well-pressed, is not required to press again after washing, line ball is kept for a long time;It is non-ignitable not quick-fried without free formaldehyde.The wash and wear finisher manufacturing process of the present invention is simple to operation, and low in raw material price is easily obtained, and nontoxic, and human body is not stimulated, and volatility is low, and the fabric after arrangement its toughness, intensity, feel are substantially unaffected.

Description

A kind of wash and wear finisher and preparation method thereof
Technical field
The invention belongs to technical field of textile auxiliary agent, specifically relates to a kind of wash and wear finisher and preparation method thereof.
Background technology
Hi-tech development makes rapid progress, and people's living standard improves constantly, and is no longer limited to for the demand of textile The intrinsic characteristic of the fabrics such as cold-proof comfort, according to different industries, crowd, purposes, requirement of the people to textile is also increasingly It is more, clothes are proposed with the requirement such as comfortable, hygienic, attractive in appearance, health care, protection, the finishing technique of textile also continues to bring out.
Natural cotton has excellent performance, is preferable dress materials, but bafta needs to press after washing Scald, this just brings very big trouble to user.Although the protein fibres such as wool fibre, cocoon fiber in natural fiber are than fine Cellulose fiber is better, but wet elasticity and wrinkle resistance are all not as good as synthetic fibers.Therefore, it is required for pressing after this kind of clothes washing Scald.
In recent years, wash and wear finisher was popular, but traditional N- methylol amide class wash and wear finishers, effect are good It is good, but the fabric after it is handled can discharge harmful formaldehyde during processing, storage kimonos are used.
The content of the invention
It is an object of the invention to provide a kind of wash and wear finisher and preparation method, to solve to propose in above-mentioned background technology The problem of.
To achieve the above object, the present invention provides following technical scheme:
A kind of wash and wear finisher, according to parts by weight, including following components:Magnesium chloride 3-5 parts, citric acid 3-5 parts, carbonic acid Hydrogen sodium 5-10 parts, borax 3-5 parts, triethanolamine 3-5 parts, hydroxymethyl cellulose 5-10 parts, double amido organosilicon emulsion 5-10 parts, AEO 3-5 parts, ethanol 10-15 parts, cactus powder 3-7 parts, deionized water 10-20 parts.
Preferably, the ethanol is absolute ethyl alcohol, and purity is pure to analyze.
Preferably, the cactus powder diameter is 1-200nm.
Preferably, the cactus powder is that grinding screening obtains after cactus high temperature is dried.
Preferably, described wash and wear finisher, according to parts by weight, including following components:3 parts of magnesium chloride, citric acid 3 Part, 5 parts of sodium acid carbonate, 3 parts of borax, 3 parts of triethanolamine, 5 parts of hydroxymethyl cellulose, 5 parts of double amido organosilicon emulsions, fatty alcohol 3 parts of APEO, 10 parts of ethanol, 3 parts of cactus powder, 10 parts of deionized water.
Preferably, described wash and wear finisher, according to parts by weight, including following components:4 parts of magnesium chloride, citric acid 4 Part, 8 parts of sodium acid carbonate, 4 parts of borax, 4 parts of triethanolamine, 8 parts of hydroxymethyl cellulose, 8 parts of double amido organosilicon emulsions, fatty alcohol 4 parts of APEO, 13 parts of ethanol, 5 parts of cactus powder, 15 parts of deionized water.
Preferably, described wash and wear finisher, according to parts by weight, including following components:5 parts of magnesium chloride, citric acid 5 Part, 10 parts of sodium acid carbonate, 5 parts of borax, 5 parts of triethanolamine, 10 parts of hydroxymethyl cellulose, 10 parts of double amido organosilicon emulsions, fat 5 parts of fat alcohol APEO, 15 parts of ethanol, 7 parts of cactus powder, 20 parts of deionized water.
A kind of preparation method of wash and wear finisher, is comprised the following steps that:
(1) citric acid 3-5 parts, hydroxymethyl cellulose 5-10 parts, double amido organosilicon emulsion 5-10 are added in a kettle Part, AEO 3-5 parts, rise temperature stir 20-30 minutes to 60-70 DEG C, 500-1000 revs/min;
(2) it is by borax 3-5 parts, triethanolamine 3-5 parts, ethanol 10-15 part ultrasonic disperses, ultrasonic disperse power first 500-1000W, jitter time are 10-20 minutes;
(3) solution of step (2) is added in the solution of step (1), 500-1000 revs/min, stirs 20-30 minutes;
(4) temperature is reduced to 30-40 DEG C, addition magnesium chloride 3-5 parts, sodium acid carbonate 5-10 parts, 500-1000 revs/min, Stir 10-20 minutes;
(5) cactus powder 3-7 parts, deionized water 10-20 parts are added, 500-1000 revs/min, stirs 20-30 minutes;
(6) stirring is closed down, the liquid wash and wear finisher prepared;
(7) stand and be cooled in stirred tank liquid wash and wear finisher and be less than 20 DEG C, blowing encapsulation, finished product.
Compared with prior art, the beneficial effects of the invention are as follows:
1st, after wash and wear finisher application fabric of the invention, fabric has excellent crease and shrink resistance performance, and outward appearance is well-pressed, It is not required to press again after washing, line ball is kept for a long time;It is non-ignitable not quick-fried without free formaldehyde.
2nd, wash and wear finisher manufacturing process of the invention is simple to operation, and low in raw material price easily obtains, and nontoxic, Human body is not stimulated, volatility is low, and the fabric after arrangement its toughness, intensity, feel are substantially unaffected.
3rd, mutual compatibility between various raw materials used in wash and wear finisher of the invention, synergy, it is excellent to collectively constitute performance Different product.
4th, technique is simplified, safe operation is simple, is easy to industrialized production.
5th, wash and wear finisher construction is simple of the invention, can by impregnating, spraying, roller coat etc. applied, production effect Rate improves.
6th, use of the invention can receive good economic benefit.
Example is embodied
The invention discloses a kind of wash and wear finisher, according to parts by weight, including following components:Magnesium chloride 3-5 parts, lemon Sour 3-5 parts, sodium acid carbonate 5-10 parts, borax 3-5 parts, triethanolamine 3-5 parts, hydroxymethyl cellulose 5-10 parts, double amino are organic Silicon emulsion 5-10 parts, AEO 3-5 parts, ethanol 10-15 parts, cactus powder 3-7 parts, deionized water 10-20 Part.
Present invention also offers a kind of preparation method of wash and wear finisher, comprise the following steps that:
(1) citric acid 3-5 parts, hydroxymethyl cellulose 5-10 parts, double amido organosilicon emulsion 5-10 are added in a kettle Part, AEO 3-5 parts, rise temperature stir 20-30 minutes to 60-70 DEG C, 500-1000 revs/min;
(2) it is by borax 3-5 parts, triethanolamine 3-5 parts, ethanol 10-15 part ultrasonic disperses, ultrasonic disperse power first 500-1000W, jitter time are 10-20 minutes;
(3) solution of step (2) is added in the solution of step (1), 500-1000 revs/min, stirs 20-30 minutes;
(4) temperature is reduced to 30-40 DEG C, addition magnesium chloride 3-5 parts, sodium acid carbonate 5-10 parts, 500-1000 revs/min, Stir 10-20 minutes;
(5) cactus powder 3-7 parts, deionized water 10-20 parts are added, 500-1000 revs/min, stirs 20-30 minutes;
(6) stirring is closed down, the liquid wash and wear finisher prepared;
(7) stand and be cooled in stirred tank liquid wash and wear finisher and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 1
The invention discloses a kind of wash and wear finisher, according to parts by weight, including following components:3 parts of magnesium chloride, citric acid 3 parts, 5 parts of sodium acid carbonate, 3 parts of borax, 3 parts of triethanolamine, 5 parts of hydroxymethyl cellulose, 5 parts of double amido organosilicon emulsions, fat 3 parts of alcohol APEO, 10 parts of ethanol, 3 parts of cactus powder, 10 parts of deionized water.
Present invention also offers a kind of preparation method of wash and wear finisher, comprise the following steps that:
(1) 3 parts of citric acid, 5 parts of hydroxymethyl cellulose, 5 parts of double amido organosilicon emulsions, fatty alcohol are added in a kettle 3 parts of APEO, rise temperature stir 20 minutes to 60 DEG C, 500 revs/min;
(2) by 3 parts of borax, 3 parts of triethanolamine, 10 parts of ethanol with ultrasonic disperse, ultrasonic disperse power it is first 500W, disperses Time is 10 minutes;
(3) solution of step (2) is added in the solution of step (1), 500 revs/min, is stirred 20 minutes;
(4) temperature is reduced to 30 DEG C, is added 3 parts of magnesium chloride, 5 parts of sodium acid carbonate, 500 revs/min, is stirred 10 minutes;
(5) 3 parts of cactus powder, 10 parts of deionized water are added, 500 revs/min, is stirred 20 minutes;
(6) stirring is closed down, the liquid wash and wear finisher prepared;
(7) stand and be cooled in stirred tank liquid wash and wear finisher and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 2
The invention discloses a kind of wash and wear finisher, according to parts by weight, including following components:4 parts of magnesium chloride, citric acid 4 parts, 8 parts of sodium acid carbonate, 4 parts of borax, 4 parts of triethanolamine, 8 parts of hydroxymethyl cellulose, 8 parts of double amido organosilicon emulsions, fat 4 parts of alcohol APEO, 13 parts of ethanol, 5 parts of cactus powder, 15 parts of deionized water.
Present invention also offers a kind of preparation method of wash and wear finisher, comprise the following steps that:
(1) 4 parts of citric acid, 8 parts of hydroxymethyl cellulose, 8 parts of double amido organosilicon emulsions, fatty alcohol are added in a kettle 4 parts of APEO, rise temperature stir 25 minutes to 65 DEG C, 800 revs/min;
(2) by 4 parts of borax, 4 parts of triethanolamine, 13 parts of ethanol with ultrasonic disperse, ultrasonic disperse power it is first 800W, disperses Time is 15 minutes;
(3) solution of step (2) is added in the solution of step (1), 800 revs/min, is stirred 25 minutes;
(4) temperature is reduced to 35 DEG C, is added 4 parts of magnesium chloride, 8 parts of sodium acid carbonate, 800 revs/min, is stirred 15 minutes;
(5) 5 parts of cactus powder, 15 parts of deionized water are added, 800 revs/min, is stirred 25 minutes;
(6) stirring is closed down, the liquid wash and wear finisher prepared;
(7) stand and be cooled in stirred tank liquid wash and wear finisher and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 3
The invention discloses a kind of wash and wear finisher, according to parts by weight, including following components:5 parts of magnesium chloride, citric acid 5 parts, 10 parts of sodium acid carbonate, 5 parts of borax, 5 parts of triethanolamine, 10 parts of hydroxymethyl cellulose, 10 parts of double amido organosilicon emulsions, fat 5 parts of fat alcohol APEO, 15 parts of ethanol, 7 parts of cactus powder, 20 parts of deionized water.
Present invention also offers a kind of preparation method of wash and wear finisher, comprise the following steps that:
(1) 5 parts of citric acid, 10 parts of hydroxymethyl cellulose, 10 parts of double amido organosilicon emulsions, fat are added in a kettle 5 parts of alcohol APEO, rise temperature stir 30 minutes to 70 DEG C, 1000 revs/min;
(2) by 5 parts of borax, 5 parts of triethanolamine, 15 parts of ethanol with ultrasonic disperse, ultrasonic disperse power it is first 1000W, point It is 20 minutes to dissipate the time;
(3) solution of step (2) is added in the solution of step (1), 1000 revs/min, is stirred 30 minutes;
(4) temperature is reduced to 40 DEG C, is added 5 parts of magnesium chloride, 10 parts of sodium acid carbonate, 1000 revs/min, is stirred 20 minutes;
(5) 7 parts of cactus powder, 20 parts of deionized water are added, 1000 revs/min, is stirred 30 minutes;
(6) stirring is closed down, the liquid wash and wear finisher prepared;
(7) stand and be cooled in stirred tank liquid wash and wear finisher and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 4
The invention discloses a kind of wash and wear finisher, according to parts by weight, including following components:3 parts of magnesium chloride, citric acid 3 parts, 5 parts of sodium acid carbonate, 5 parts of borax, 3 parts of triethanolamine, 10 parts of hydroxymethyl cellulose, 10 parts of double amido organosilicon emulsions, fat 3 parts of fat alcohol APEO, 10 parts of ethanol, 7 parts of cactus powder, 20 parts of deionized water.
Present invention also offers a kind of preparation method of wash and wear finisher, comprise the following steps that:
(1) 3 parts of citric acid, 10 parts of hydroxymethyl cellulose, 10 parts of double amido organosilicon emulsions, fat are added in a kettle 3 parts of alcohol APEO, rise temperature stir 20 minutes to 70 DEG C, 1000 revs/min;
(2) by 5 parts of borax, 3 parts of triethanolamine, 10 parts of ethanol with ultrasonic disperse, ultrasonic disperse power it is first 900W, disperses Time is 14 minutes;
(3) solution of step (2) is added in the solution of step (1), 900 revs/min, is stirred 30 minutes;
(4) temperature is reduced to 35 DEG C, is added 5 parts of magnesium chloride, 5 parts of sodium acid carbonate, 1000 revs/min, is stirred 10 minutes;
(5) 7 parts of cactus powder, 20 parts of deionized water are added, 900 revs/min, is stirred 30 minutes;
(6) stirring is closed down, the liquid wash and wear finisher prepared;
(7) stand and be cooled in stirred tank liquid wash and wear finisher and be less than 20 DEG C, blowing encapsulation, finished product.
Test case
4 pieces of identical fabrics are put into the noniron finish agent solution of embodiment 1,2,3,4 and padded, are rolled by two leachings two, 80-100 DEG C of prebake is then heated to, then is dried at 120-140 DEG C, is then cleaned with 40-50 DEG C of hot water, is finally rushed with cold water Wash, dried after cleaning, 4 pieces of cloth with ironing-free performance can be obtained.Test result is as follows:
Embodiment Creasy recovery angle (°)
1 252
2 265
3 278
4 269
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (8)

  1. A kind of 1. wash and wear finisher, it is characterised in that:The wash and wear finisher includes the raw material of following parts by weight:Magnesium chloride 3- 5 parts, it is citric acid 3-5 parts, sodium acid carbonate 5-10 parts, borax 3-5 parts, triethanolamine 3-5 parts, hydroxymethyl cellulose 5-10 parts, double Amido organosilicon emulsion 5-10 parts, AEO 3-5 parts, ethanol 10-15 parts, cactus powder 3-7 parts, deionization Water 10-20 parts.
  2. 2. wash and wear finisher according to claim 1, it is characterised in that:The ethanol is absolute ethyl alcohol, and purity is analysis It is pure.
  3. 3. wash and wear finisher according to claim 1, it is characterised in that:The cactus powder is dried for cactus high temperature Grinding screening afterwards obtains.
  4. 4. wash and wear finisher according to claim 1, it is characterised in that:The cactus powder diameter is 1-200nm.
  5. 5. wash and wear finisher according to claim 1, it is characterised in that:According to parts by weight, including following components:Chlorination 3 parts of magnesium, 3 parts of citric acid, 5 parts of sodium acid carbonate, 3 parts of borax, 3 parts of triethanolamine, 5 parts of hydroxymethyl cellulose, double amido organosilicons 5 parts of emulsion, 3 parts of AEO, 10 parts of ethanol, 3 parts of cactus powder, 10 parts of deionized water.
  6. 6. wash and wear finisher according to claim 1, it is characterised in that:According to parts by weight, including following components:Chlorination 4 parts of magnesium, 4 parts of citric acid, 8 parts of sodium acid carbonate, 4 parts of borax, 4 parts of triethanolamine, 8 parts of hydroxymethyl cellulose, double amido organosilicons 8 parts of emulsion, 4 parts of AEO, 13 parts of ethanol, 5 parts of cactus powder, 15 parts of deionized water.
  7. 7. wash and wear finisher according to claim 1, it is characterised in that:According to parts by weight, including following components:Chlorination 5 parts of magnesium, 5 parts of citric acid, 10 parts of sodium acid carbonate, 5 parts of borax, 5 parts of triethanolamine, 10 parts of hydroxymethyl cellulose, double amino are organic 10 parts of silicon emulsion, 5 parts of AEO, 15 parts of ethanol, 7 parts of cactus powder, 20 parts of deionized water.
  8. A kind of 8. preparation method of any described wash and wear finisher in 1-7 using the claims, it is characterised in that:Specifically Step is as follows:
    Step 1, citric acid 3-5 parts, hydroxymethyl cellulose 5-10 parts, double amido organosilicon emulsion 5-10 are added in a kettle Part, AEO 3-5 parts, rise temperature stir 20-30 minutes to 60-70 DEG C, 500-1000 revs/min;
    Step 2, it is by borax 3-5 parts, triethanolamine 3-5 parts, ethanol 10-15 part ultrasonic disperses, ultrasonic disperse power first 500-1000W, jitter time are 10-20 minutes;
    Step 3, the solution of step 2 is added in the solution of step 1,500-1000 revs/min, stirs 20-30 minutes;
    Step 4, temperature is reduced to 30-40 DEG C, is added magnesium chloride 3-5 parts, sodium acid carbonate 5-10 parts, 500-1000 revs/min, is stirred Mix 10-20 minutes;
    Step 5, cactus powder 3-7 parts, deionized water 10-20 parts are added, 500-1000 revs/min, stirs 20-30 minutes;
    Step 6, stirring is closed down, the liquid wash and wear finisher prepared;
    Step 7, stand and be cooled in stirred tank liquid wash and wear finisher and be less than 20 DEG C, blowing encapsulation, finished product.
CN201710897076.2A 2017-09-28 2017-09-28 A kind of wash and wear finisher and preparation method thereof Pending CN107780200A (en)

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CN101215780A (en) * 2007-12-27 2008-07-09 浙江嘉得莱有限公司 Pure natural ultra-violet radiation resisting finishing method for knitting plus material
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CN104562386A (en) * 2015-02-03 2015-04-29 湖州新创丝织品有限公司 Novel non-ironing textile and preparation method thereof
CN106592223A (en) * 2016-12-21 2017-04-26 阜阳市豹子头服饰科技有限公司 Water-proofing, oil-proofing and antifouling type easy-care finishing liquid of shirt and finishing method of water-proofing, oil-proofing and antifouling type easy-care finishing liquid
CN106592224A (en) * 2016-12-21 2017-04-26 阜阳市豹子头服饰科技有限公司 Wear-resisting ironing-free finishing liquid of shirt and finishing method of wear-resisting ironing-free finishing liquid

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Application publication date: 20180309