CN104549105A - Efficient reactor for production and processing of epoxy soybean oil - Google Patents
Efficient reactor for production and processing of epoxy soybean oil Download PDFInfo
- Publication number
- CN104549105A CN104549105A CN201410845607.XA CN201410845607A CN104549105A CN 104549105 A CN104549105 A CN 104549105A CN 201410845607 A CN201410845607 A CN 201410845607A CN 104549105 A CN104549105 A CN 104549105A
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- China
- Prior art keywords
- stirring
- soybean oil
- epoxy soybean
- arranges
- high efficiency
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/38—Compounds containing oxirane rings with hydrocarbon radicals, substituted by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals
- C07D303/40—Compounds containing oxirane rings with hydrocarbon radicals, substituted by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals by ester radicals
- C07D303/42—Acyclic compounds having a chain of seven or more carbon atoms, e.g. epoxidised fats
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Beans For Foods Or Fodder (AREA)
- Apparatuses For Bulk Treatment Of Fruits And Vegetables And Apparatuses For Preparing Feeds (AREA)
Abstract
The invention discloses an efficient reactor for production and processing of epoxy soybean oil. The efficient reactor comprises a reaction tank and a stirring device, wherein the reaction tank comprises an outer barrel and an inner barrel which are sealed; a cover body is hermetically arranged at an upper end of the reaction tank; an inner cavity body is formed between the outer barrel and the inner barrel; a steam coil pipe is arranged in the inner cavity body in a manner of surrounding the inner barrel; inclined feeding grooves are formed in opposite side surfaces of the cover body; a flow diversion plate communicated with the inclined feeding grooves is arranged in the cover body; the stirring device comprises a main stirring shaft; a plurality of transverse stirring shafts are equidistantly arranged on two opposite sides of the main stirring shaft from top to bottom; a plurality of stirring blades are arranged on each of an upper end surface and a lower end surface of each transverse stirring shaft in parallel; a plurality of conical stirring teeth are fixedly connected to two opposite sides of each stirring blade. The reactor is simple in structure and easy to operate, and can realize uniform stirring, uniform feeding and uniform heating, so that the production quality and the production efficiency of the epoxy soybean oil is improved and the economic benefit is increased.
Description
Technical field
The present invention relates to chemical industry equipment production field, particularly relate to a kind of epoxy soybean oil process for processing high efficiency reactor.
Background technology
Be light yellow sticky oily liquids at normal temperatures, the solubleness <0.01(25 DEG C in water), the solubleness 0.55%(25 of water in these product ° C) and, be dissolved in the organic solvents such as hydro carbons, ketone, ester class, higher alcohols, be slightly soluble in ethanol.These product are that a kind of most popular nontoxic polyvinyl chloride softening agent is held concurrently stablizer: good with polyvinyl chloride resin consistency, volatility is low, transport property is little.Have excellent thermostability and light stability, water tolerance and oil-proofness are also good, can give the good physical strength of goods, weathering resistance and electrical property, and nontoxicity, be the chemical technology auxiliary agent for packaging material for food of international endorsement.These product can be used for all polrvinyl chloride products.As varieties of food items wrapping material, medical product, various film, sheet material, tubing, refrigerator strip of paper used for sealing, leatheroid, flooring laminate, plastic wallpaper, electric wire and other daily plastic goods etc., also can be used for special ink, paint, coating, synthetic rubber and liquid composite stabilizing agent etc.
In the use procedure of reality, it is not good also to there is color and luster in epoxy soybean oil, problem of low quality, this is mainly relevant with epoxy soybean oil response situation in the reactor, mainly there is following shortcoming in existing reactor, it causes the of low quality of epoxy soybean oil, one: the reaction process of epoxy soybean oil is steady not, main relevant with the speed adding batching, add the excessive velocities of batching or excessively all can affect reaction effect slowly, therefore, the epoxy soybean oil in order to obtained better quality just strictly must control the feed rate of admixtion, can not be too fast; Secondly, for the preparation of chemical field, stirring in reaction process is also one of factor of obtained better product, and existing stirring arranges more traditional, only two panels agitating vane is adopted to complete the stirring reaction of epoxy soybean oil, make mixing evenness poor, thus cause the quality product of producing to there is the phenomenons such as reaction is incomplete; Again, the reaction of epoxy soybean oil needs to react in the environment of heating, because the rising of temperature can fast reaction speed and reaction effect, and steam of the prior art directly passes into retort to heat, there is upper end and heat rapidly in this type of heating, and lower end is heated comparatively slow, there is the temperature difference, cause the reaction of the reaction of upper end and lower end not carry out simultaneously, thus cause top and bottom product there is mass discrepancy.
Summary of the invention
For above-mentioned Problems existing, the present invention aims to provide a kind of epoxy soybean oil process for processing high efficiency reactor, this reactor structure is simple, easy handling, can uniform stirring be realized, uniform feeding and thermally equivalent, thus improve the quality of production of epoxy soybean oil, production efficiency, and then increase economic efficiency.
To achieve these goals, the technical solution adopted in the present invention is as follows:
Epoxy soybean oil process for processing high efficiency reactor, comprise retort and whipping appts, described retort is sealed by urceolus and inner core and forms, the sealing of described retort upper end arranges lid, inner chamber body is formed between described urceolus and described inner core, in described inner chamber body, steam coil pipe is set around described inner core, the through connection steam inlet duct in described steam coil pipe top, the side that described lid is relative all arranges inclination feed chute, and described lid portion inside arranges the shunting disk be connected with described inclination feed chute; Described whipping appts comprises stirring main shaft, the upper end of described stirring main shaft is fixed on described lid, and drive driving by drive-motor, equidistant from the top down on described stirring main shaft two opposite sides some stirring transverse axis are set, each described stirring transverse axis upper surface and lower surface are all set up in parallel some stirring pieces, and each described stirring piece two opposite sides are all fixedly connected with some taper stirrer gears.
Further, described shunting disk arranges some blanking holes, in each described blanking hole, one connects shunting funnel.
Further, described shunting disk arranges protective sleeve with the described stirring main shaft place of combining.
Further, described steam coil pipe has some cores.
Further, the range of tilt angles of each described inclination feed chute at 30 ~ 45 °, and vertically arranges opening for feed on each described inclination feed chute.
Principle of the present invention and beneficial effect are: first, the present invention is adopt all to arrange stirring piece arranged side by side on stirring transverse axis upper surface and lower surface solving in the problem stirring inequality, stirring piece two relative side is all symmetrical arranged taper stirrer gear, stirring main shaft drives in the process stirring transverse axis stirring, epoxy soybean oil is thick because of it, so adopt taper stirrer gear by its sharp-pointed tapered portion potential energy enough to stirring liquid shearing force, under the acting in conjunction of multiple taper stirrer gear shearing force, the stirring dynamics stirring liquid reaches maximum, mixed effect reaches best, ensure that reacting completely of reaction solution simultaneously, stir, by product is few, output can be improved, secondly, the present invention is binding pattern retort being adopted to inside and outside cylinder solving in the uneven problem of heating, steam coil pipe is set in the inner chamber body between inside and outside cylinder, steam disc pipe winding disk encloses around inner core one, can to liquid upper and lower in retort reacting by heating simultaneously by steam coil pipe, avoid reacting up and down uneven phenomenon to occur, thus cause quality product slightly in the phenomenon of difference, improve the consistence of resultant in whole retort, again, the present invention solution blanking too fast or cross slow problem be adopt a shunting disk is set, in addition the inclination feed chute on lid is arranged in addition, admixtion directly enters inclination feed chute by opening for feed, inclination feed chute is by its inclination advantage, to admixtion one surging force obliquely, admixtion enters on shunting disk with speed faster, shunting disk there are some funnel holes, fixed installation shunting funnel below funnel hole, strictly can not only be controlled the discharge quantity of admixtion by shunting funnel, the even blanking of admixtion can also be ensured, kill two birds with one stone.
Accompanying drawing explanation
Fig. 1 is schematic front view of the present invention.
Fig. 2 is the enlarged view of part A of the present invention.
Fig. 3 is retort inside top schematic diagram of the present invention.
Fig. 4 is the schematic top plan view of shunting disk of the present invention.
Fig. 5 is shunting disk of the present invention and stirring main spindle's graph of a relation.
Wherein: 1-urceolus, 2-inner core, 3-steam inlet duct; 4-steam coil pipe, 41-core, 5-stirs main shaft; 6-stirs transverse axis, 7-stirring piece, 8-taper stirrer gear; 9-shunting disk, 91-centre hole, 10-shunts funnel; 11-opening for feed, 12-inclination feed chute, 13-lid; 14-base, 15-protective sleeve, 16-inner chamber body.
Embodiment
In order to make those of ordinary skill in the art can better understand technical scheme of the present invention, below in conjunction with drawings and Examples, technical scheme of the present invention is further described.
With reference to the epoxy soybean oil process for processing high efficiency reactor shown in accompanying drawing 1-5, comprise retort and whipping appts, described whipping appts comprises stirring main shaft 5, the upper end of described stirring main shaft 5 is fixed on described lid 13, and drive driving by drive-motor, equidistant from the top down on described stirring main shaft 5 two opposite sides some stirring transverse axis 6 are set, each described stirring transverse axis 6 upper surface and lower surface are all set up in parallel some stirring pieces 7, and each described stirring piece 7 two opposite sides are all fixedly connected with some taper stirrer gears 8, described retort is arranged on base 14, retort is raised by base 14, the convenient discharge of product can be made, described retort is sealed by urceolus 1 and inner core 2 and forms, the sealing of described retort upper end arranges lid 13, inner chamber body 16 is formed between described urceolus 1 and described inner core 2, in described inner chamber body 16, steam coil pipe 4 is set around described inner core 2, the through connection steam inlet duct 3 in described steam coil pipe 4 top, described steam coil pipe 4 has some cores 41, steam enters in steam coil pipe 4 by steam inlet duct 3, constantly steam is sprayed into inner core 2 surface by the core 41 on steam coil pipe 4, rapidly by bottom inner core 2, middle part and upper end are heated to temperature of reaction, simultaneously, in step of reaction, successively steam is provided by steam coil pipe 4, ensure that the reactant reaction of inner core 2 inside is complete, the side that described lid 13 is relative all arranges inclination feed chute 12, each described inclination feed chute 12 vertically arranges opening for feed 11, the range of tilt angles of each described inclination feed chute 12 is at 30 ~ 45 °, obliquity is crossed conference and is caused input speed too fast, be unfavorable for reacting to each other of admixtion and major ingredient, angle of inclination is too small, charging is too mild, cause input speed slower, the supply of title complex is inadequate, can cause reaction not exclusively, described lid 13 inside arranges the shunting disk 9 be connected with described inclination feed chute 12, centre hole 91 is had in the middle of described shunting disk 9, stir main shaft 5 pass centre hole 91 and extend to inner core 2 interior bottom portion, described shunting disk 9 arranges some blanking holes, in each described blanking hole, one connects shunting funnel 10, described shunting disk 9 arranges protective sleeve 15 with described stirring main shaft 5 place of combining.
Claims (5)
1. epoxy soybean oil process for processing high efficiency reactor, comprise retort and whipping appts, it is characterized in that: described retort is sealed by urceolus (1) and inner core (2) and forms, the sealing of described retort upper end arranges lid (13), inner chamber body (16) is formed between described urceolus (1) and described inner core (2), in described inner chamber body (16), steam coil pipe (4) is set around described inner core (2), the through connection steam inlet duct (3) in described steam coil pipe (4) top, the side that described lid (13) is relative all arranges inclination feed chute (12), described lid (13) inside arranges the shunting disk (9) be connected with described inclination feed chute (12), described whipping appts comprises stirring main shaft (5), the upper end of described stirring main shaft (5) is fixed on described lid (13), and drive driving by drive-motor, equidistant from the top down on described stirring main shaft (5) two opposite sides some stirring transverse axis (6) are set, each described stirring transverse axis (6) upper surface and lower surface are all set up in parallel some stirring pieces (7), and each described stirring piece (7) two opposite sides are all fixedly connected with some taper stirrer gears (8).
2. a kind of epoxy soybean oil process for processing high efficiency reactor according to claim 1, is characterized in that: (9) arrange some blanking holes to described shunting disk, and in each described blanking hole, one connects shunting funnel (10).
3. a kind of epoxy soybean oil process for processing high efficiency reactor according to claim 2, is characterized in that: described shunting disk (9) arranges protective sleeve (15) with described stirring main shaft (5) place of combining.
4. a kind of epoxy soybean oil process for processing high efficiency reactor according to claim 1, is characterized in that: described steam coil pipe (4) has some cores (41).
5. a kind of epoxy soybean oil process for processing high efficiency reactor according to claim 1, it is characterized in that: the range of tilt angles of each described inclination feed chute (12) at 30 ~ 45 °, and vertically arranges opening for feed (11) on each described inclination feed chute (12).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410845607.XA CN104549105B (en) | 2014-12-31 | 2014-12-31 | Epoxy soybean oil production and processing reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410845607.XA CN104549105B (en) | 2014-12-31 | 2014-12-31 | Epoxy soybean oil production and processing reactor |
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| Publication Number | Publication Date |
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| CN104549105A true CN104549105A (en) | 2015-04-29 |
| CN104549105B CN104549105B (en) | 2016-09-28 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410845607.XA Active CN104549105B (en) | 2014-12-31 | 2014-12-31 | Epoxy soybean oil production and processing reactor |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104941554A (en) * | 2015-05-29 | 2015-09-30 | 吴巴特尔 | Novel high efficiency reactor |
| CN105254596A (en) * | 2015-09-18 | 2016-01-20 | 丹阳市助剂化工厂有限公司 | Preparation method for epoxidized soybean oil |
| CN105771849A (en) * | 2016-03-07 | 2016-07-20 | 李云军 | Reaction kettle for preparing sucralose |
| CN108671864A (en) * | 2018-05-24 | 2018-10-19 | 周封 | Sticky material cooling reaction kettle |
| CN109107513A (en) * | 2018-09-07 | 2019-01-01 | 南京金陵化工厂有限责任公司 | A kind of mixing arrangement and preparation method based on Aqueous phase production calcium stearate |
| CN109420449A (en) * | 2017-09-01 | 2019-03-05 | 天津市盛鑫隆粉末涂料有限公司 | The powder agitating device of stirring more evenly |
| CN115075871A (en) * | 2022-07-21 | 2022-09-20 | 中勘资源勘探科技股份有限公司 | Mine grouting filling device and method |
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| CN203108465U (en) * | 2013-03-14 | 2013-08-07 | 内蒙古瑞盛新能源有限公司 | Mixing equipment for concentrated sulfuric acid and hydrogen peroxide |
| CN204429276U (en) * | 2014-12-31 | 2015-07-01 | 丹阳市助剂化工厂有限公司 | Epoxidized soybean oil production and processing high efficiency reactor |
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| CN86204318U (en) * | 1986-06-25 | 1987-08-12 | 清华大学 | Auto-sampler of liquid |
| US20030010217A1 (en) * | 2002-01-07 | 2003-01-16 | Claudio Torghele | Dough mixer with metering device |
| CN1765486A (en) * | 2004-10-28 | 2006-05-03 | 中国石油化工股份有限公司 | Continuous high temperature gas solid reactor |
| CN101785930A (en) * | 2010-03-18 | 2010-07-28 | 严旭明 | Tubular film evaporator |
| CN201643754U (en) * | 2010-03-18 | 2010-11-24 | 严旭明 | Tubular film evaporator |
| CN201744352U (en) * | 2010-07-30 | 2011-02-16 | 华南农业大学 | Suspension fertilizer reactor |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104941554A (en) * | 2015-05-29 | 2015-09-30 | 吴巴特尔 | Novel high efficiency reactor |
| CN105254596A (en) * | 2015-09-18 | 2016-01-20 | 丹阳市助剂化工厂有限公司 | Preparation method for epoxidized soybean oil |
| CN105771849A (en) * | 2016-03-07 | 2016-07-20 | 李云军 | Reaction kettle for preparing sucralose |
| CN109420449A (en) * | 2017-09-01 | 2019-03-05 | 天津市盛鑫隆粉末涂料有限公司 | The powder agitating device of stirring more evenly |
| CN108671864A (en) * | 2018-05-24 | 2018-10-19 | 周封 | Sticky material cooling reaction kettle |
| CN109107513A (en) * | 2018-09-07 | 2019-01-01 | 南京金陵化工厂有限责任公司 | A kind of mixing arrangement and preparation method based on Aqueous phase production calcium stearate |
| CN115075871A (en) * | 2022-07-21 | 2022-09-20 | 中勘资源勘探科技股份有限公司 | Mine grouting filling device and method |
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| Publication number | Publication date |
|---|---|
| CN104549105B (en) | 2016-09-28 |
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Denomination of invention: Reactor for production and processing of epoxy soybean oil Effective date of registration: 20191220 Granted publication date: 20160928 Pledgee: Industrial Bank Co., Ltd. Zhenjiang Branch Pledgor: DANYANG CITY AUXILIARIES CHEMICAL PLANT CO., LTD. Registration number: Y2019980001199 |