CN104549105B - Epoxy soybean oil production and processing reactor - Google Patents
Epoxy soybean oil production and processing reactor Download PDFInfo
- Publication number
- CN104549105B CN104549105B CN201410845607.XA CN201410845607A CN104549105B CN 104549105 B CN104549105 B CN 104549105B CN 201410845607 A CN201410845607 A CN 201410845607A CN 104549105 B CN104549105 B CN 104549105B
- Authority
- CN
- China
- Prior art keywords
- stirring
- retort
- main shaft
- lid
- soybean oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/38—Compounds containing oxirane rings with hydrocarbon radicals, substituted by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals
- C07D303/40—Compounds containing oxirane rings with hydrocarbon radicals, substituted by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals by ester radicals
- C07D303/42—Acyclic compounds having a chain of seven or more carbon atoms, e.g. epoxidised fats
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Beans For Foods Or Fodder (AREA)
- Apparatuses For Bulk Treatment Of Fruits And Vegetables And Apparatuses For Preparing Feeds (AREA)
Abstract
The invention discloses epoxy soybean oil production and processing reactor, including retort and agitating device, retort is sealed by urceolus and inner core and forms, retort upper end seals and arranges lid, inner chamber body is formed between urceolus and inner core, arranging steam coil pipe around inner core in inner chamber body, the side that lid is relative is respectively provided with inclination feed well, and lid portion inside arranges and tilts the shunting disk that feed well is connected；Agitating device includes stirring main shaft, stirring main shaft two opposite sides are equidistantly positioned some stirring transverse axis from the top down, all being set up in parallel some stirring sheets on each stirring transverse axis upper surface and lower surface, each stirring sheet two opposite sides are fixedly connected with some taper stirrer gears；This reactor simple structure of the present invention, it is easy to operation, it is possible to realize uniform stirring, uniform feeding and thermally equivalent, thus improve the quality of production of epoxy soybean oil, production efficiency, and then increase economic efficiency.
Description
Technical field
The present invention relates to chemical industry equipment production field, particularly relate to a kind of epoxy soybean oil production and processing reactor
Background technology
It is light yellow sticky oily liquids at normal temperatures, and dissolubility in water < 0.01(25 DEG C), water 0.55%(25 ° of C of the dissolubility in these product), it is dissolved in the organic solvents such as hydro carbons, ketone, esters, higher alcohol, is slightly soluble in ethanol.These product are that a kind of most popular nontoxic polyvinyl chloride plasticizer is held concurrently stabilizer: good with the polyvinyl chloride resin compatibility, volatility is low, animal migration is little.There is excellent heat stability and light stability, resistance to water and oil resistivity the best, the good mechanical strength of goods, weatherability and electrical property, and avirulence can be given, be the chemical technology auxiliary agent for packaging material for food of international endorsement.These product can be used for all of polrvinyl chloride product.Such as varieties of food items packaging material, medical product, various thin film, sheet material, tubing, refrigerator strip of paper used for sealing, artificial leather, flooring laminate, plastic wallpaper, electric wire and other daily plastic goods etc., it may also be used for special ink, paint, coating, synthetic rubber and liquid composite stabilizing agent etc..
During actual use, it is the best that epoxy soybean oil there is also color and luster, problem of low quality, this is mainly relevant with epoxy soybean oil response situation in the reactor, existing reactor is primarily present following shortcoming, it causes the of low quality of epoxy soybean oil, one: the course of reaction of epoxy soybean oil is the most steady, mainly relevant with the speed adding dispensing, add the excessive velocities of dispensing or excessively all can affect reaction effect slowly, therefore, it is necessary for strictly controlling the charging rate of batch to prepare the epoxy soybean oil of better quality, it is impossible to too fast；Secondly, for the preparation of chemical field, stirring in course of reaction is also one of factor preparing preferable product, and existing stirring to arrange comparison traditional, only two panels stirring vane is used to complete the stirring reaction of epoxy soybean oil, make mixing evenness poor, thus cause the product quality produced to there is the phenomenons such as reaction is incomplete；Again, the reaction of epoxy soybean oil is to need to react in the environment of heating, because the rising of temperature can accelerate response speed and reaction effect, and steam of the prior art is to be passed directly into retort to heat, there is upper end and heat rapidly in this mode of heating, and lower end is heated relatively slow, there is the temperature difference, cause the reaction of upper end can not carry out with the reaction of lower end simultaneously, thus cause the existence mass discrepancy of top and bottom product.
Summary of the invention
Problem for above-mentioned existence, it is desirable to provide a kind of epoxy soybean oil production and processing reactor, this reactor simple structure, easily operated, it is capable of uniform stirring, uniform feeding and thermally equivalent, thus improves the quality of production of epoxy soybean oil, production efficiency, and then increase economic efficiency.
To achieve these goals, the technical solution adopted in the present invention is as follows:
Epoxy soybean oil production and processing reactor, including retort and agitating device, described retort is sealed by urceolus and inner core and forms, described retort upper end seals and arranges lid, in forming inner chamber body, described inner chamber body between described urceolus and described inner core, steam coil pipe, the through connection in described steam coil pipe top steam inlet duct are set around described inner core, the side that described lid is relative is respectively provided with inclination feed well, and described lid portion inside arranges the shunting disk being connected with described inclination feed well；Described agitating device includes stirring main shaft, the upper end of described stirring main shaft is fixed on described lid, and by driving driven by motor to drive, described stirring main shaft two opposite sides are equidistantly positioned some stirring transverse axis from the top down, all being set up in parallel some stirring sheets on each described stirring transverse axis upper surface and lower surface, each described stirring sheet two opposite sides are fixedly connected with some taper stirrer gears.
Further, described shunting disk arranging some blanking holes, in each described blanking hole, one connects shunting funnel.
Further, described shunting disk arranges protection set with the described stirring main shaft place of combining.
Further, described steam coil pipe has some cores.
Further, the range of tilt angles of each described inclination feed well is at 30～45 °, and vertically arranged charging aperture on each described inclination feed well.
The principle of the present invention and providing the benefit that: first, the present invention is utilized in stirring in the problem solving stirring inequality and is respectively provided with stirring sheet arranged side by side on transverse axis upper surface and lower surface, stirring sheet two relative side is all symmetrical arranged taper stirrer gear, during stirring main shaft drives stirring transverse axis agitation, epoxy soybean oil is thick because of it, so using taper stirrer gear by its sharp-pointed tapered portion potential energy enough to stirring one shearing force of liquid, under the common effect of multiple taper stirrer gear shearing forces, the stirring dynamics of stirring liquid reaches maximum, mixed effect reaches optimal, ensure that the reaction of reactant liquor is complete simultaneously, stir, by-product is few, yield can be improved；Secondly, the present invention is the binding pattern to the retort inside and outside cylinder of employing in the problem that heating is uneven solving, inner chamber body between inside and outside cylinder arranges steam coil pipe, steam disc pipe winding disk encloses around inner core one, can be to the reacting by heating simultaneously of upper and lower liquid in retort by steam coil pipe, the phenomenon avoiding reacting up and down uneven occurs, thus causes product quality slightly in the phenomenon of difference, improves the concordance of product in whole retort；Again, the present invention is too fast in solution blanking or slow problem excessively is to use to arrange a shunting disk, in addition with the inclination feed well being arranged on lid, batch is directly entered inclination feed well by charging aperture, tilt feed well and tilt advantage by it, to one impulsive force obliquely of batch, batch enters on shunting disk with speed faster, some funnel holes are had on shunting disk, fixed installation shunting funnel below funnel hole, can not only strictly be controlled the discharge quantity of batch by shunting funnel, it can also be ensured that the uniform blanking of batch, kill two birds with one stone.
Accompanying drawing explanation
Fig. 1 is schematic front view of the present invention.
Fig. 2 is the enlarged drawing of part A of the present invention.
Fig. 3 is retort inside top schematic diagram of the present invention.
Fig. 4 is the schematic top plan view of shunting disk of the present invention.
Fig. 5 is shunting disk of the present invention and stirring main spindle's graph of a relation.
Wherein: 1-urceolus, 2-inner core, 3-steam inlet duct; 4-steam coil pipe, 41-core, 5-stirs main shaft; 6-stirs transverse axis, and 7-stirs sheet, 8-taper stirrer gear; 9-shunting disk, 91-centre bore, 10-shunts funnel; 11-charging aperture, 12-tilts feed well, 13-lid; 14-base, 15-protects set, 16-inner chamber body.
Detailed description of the invention
In order to make those of ordinary skill in the art be better understood on technical scheme, with embodiment, technical scheme is further described below in conjunction with the accompanying drawings.
Epoxy soybean oil production and processing reactor shown in 1-5 referring to the drawings, including retort and agitating device, described agitating device includes stirring main shaft 5, the upper end of described stirring main shaft 5 is fixed on described lid 13, and by driving driven by motor to drive, described stirring main shaft 5 two opposite sides are equidistantly positioned some stirring transverse axis 6 from the top down, all being set up in parallel some stirring sheets 7 on each described stirring transverse axis 6 upper surface and lower surface, each described stirring sheet 7 two opposite sides are fixedly connected with some taper stirrer gears 8；nullDescribed retort is arranged on base 14，Retort is raised by base 14，Enable to the convenient discharge of product，Described retort is sealed by urceolus 1 and inner core 2 and forms，Described retort upper end seals and arranges lid 13，Inner chamber body 16 is formed between described urceolus 1 and described inner core 2，In described inner chamber body 16, steam coil pipe 4 is set around described inner core 2，The through connection in described steam coil pipe 4 top steam inlet duct 3，Some cores 41 are had on described steam coil pipe 4，Steam is entered in steam coil pipe 4 by steam inlet duct 3，Steam is constantly sprayed into inner core 2 surface by the core 41 on steam coil pipe 4，Rapidly by bottom inner core 2、Middle part and upper end are heated to reaction temperature，Simultaneously，In the stage of reaction，Steam is successively provided by steam coil pipe 4，Ensure that the reactant reaction within inner core 2 is complete，The side that described lid 13 is relative is respectively provided with inclination feed well 12，Vertically arranged charging aperture 11 on each described inclination feed well 12，The range of tilt angles of each described inclination feed well 12 is at 30～45 °，Gradient is crossed conference and is caused charging rate too fast，It is unfavorable for reacting to each other of batch and major ingredient，Angle of inclination is too small，Feed the mildest，Cause charging rate slower，The supply of coordination compound is inadequate，Can cause reaction not exclusively，Described lid 13 is internal arranges the shunting disk 9 being connected with described inclination feed well 12，Centre bore 91 is had in the middle of described shunting disk 9，Stirring main shaft 5 through centre bore 91 and extends to inner core 2 interior bottom portion，On described shunting disk 9, some blanking holes are set，In each described blanking hole, one connects shunting funnel 10，Described shunting disk 9 arranges protection set 15 with described stirring main shaft 5 place of combining.
Claims (2)
1. epoxy soybean oil production and processing reactor, including retort and agitating device, it is characterized in that: described retort is sealed by urceolus (1) and inner core (2) and forms, described retort upper end seals and arranges lid (13), inner chamber body (16) is formed between described urceolus (1) and described inner core (2), in described inner chamber body (16), steam coil pipe (4) is set around described inner core (2), the through connection in described steam coil pipe (4) top steam inlet duct (3), the side that described lid (13) is relative is respectively provided with inclination feed well (12), the range of tilt angles of each described inclination feed well (12) is at 30～45 °, and at the upper vertically arranged charging aperture (11) of each described inclination feed well (12)；Described lid (13) is internal arranges the shunting disk (9) being connected with described inclination feed well (12); described shunting disk arranges some blanking holes on (9); in each described blanking hole, one connects shunting funnel (10), and described shunting disk (9) arranges protection set (15) with described stirring main shaft (5) place of combining；Described agitating device includes stirring main shaft (5), the upper end of described stirring main shaft (5) is fixed on described lid (13), and by driving driven by motor to drive, described stirring main shaft (5) two opposite sides are equidistantly positioned some stirring transverse axis (6) from the top down, all being set up in parallel some stirring sheets (7) on each described stirring transverse axis (6) upper surface and lower surface, each described stirring sheet (7) two opposite sides are fixedly connected with some taper stirrer gears (8).
A kind of epoxy soybean oil production and processing reactor the most according to claim 1, it is characterised in that: have some cores (41) on described steam coil pipe (4).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410845607.XA CN104549105B (en) | 2014-12-31 | 2014-12-31 | Epoxy soybean oil production and processing reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410845607.XA CN104549105B (en) | 2014-12-31 | 2014-12-31 | Epoxy soybean oil production and processing reactor |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104549105A CN104549105A (en) | 2015-04-29 |
| CN104549105B true CN104549105B (en) | 2016-09-28 |
Family
ID=53066815
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410845607.XA Active CN104549105B (en) | 2014-12-31 | 2014-12-31 | Epoxy soybean oil production and processing reactor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104549105B (en) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104941554B (en) * | 2015-05-29 | 2017-01-04 | 吴巴特尔 | A kind of high efficiency reactor |
| CN105254596A (en) * | 2015-09-18 | 2016-01-20 | 丹阳市助剂化工厂有限公司 | Preparation method for epoxidized soybean oil |
| CN105771849A (en) * | 2016-03-07 | 2016-07-20 | 李云军 | Reaction kettle for preparing sucralose |
| CN109420449A (en) * | 2017-09-01 | 2019-03-05 | 天津市盛鑫隆粉末涂料有限公司 | The powder agitating device of stirring more evenly |
| CN108671864B (en) * | 2018-05-24 | 2020-12-29 | 荣成惠德环保科技有限公司 | Viscous material cooling reaction kettle |
| CN109107513A (en) * | 2018-09-07 | 2019-01-01 | 南京金陵化工厂有限责任公司 | A kind of mixing arrangement and preparation method based on Aqueous phase production calcium stearate |
| CN115075871A (en) * | 2022-07-21 | 2022-09-20 | 中勘资源勘探科技股份有限公司 | Mine grouting filling device and method |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN86204318U (en) * | 1986-06-25 | 1987-08-12 | 清华大学 | Auto-sampler of liquid |
| US6863429B2 (en) * | 2002-01-07 | 2005-03-08 | Artos, S.A. | Dough mixer with metering device |
| CN100344361C (en) * | 2004-10-28 | 2007-10-24 | 中国石油化工股份有限公司 | Continuous high temperature gas solid reactor |
| CN101785930B (en) * | 2010-03-18 | 2012-04-25 | 严旭明 | Tubular film evaporator |
| CN201643754U (en) * | 2010-03-18 | 2010-11-24 | 严旭明 | Tubular film evaporator |
| CN201744352U (en) * | 2010-07-30 | 2011-02-16 | 华南农业大学 | Suspension fertilizer reactor |
| CN201793376U (en) * | 2010-09-13 | 2011-04-13 | 化学工业第二设计院宁波工程有限公司 | Silane generation reactor |
| CN202036994U (en) * | 2011-04-21 | 2011-11-16 | 钱玉芳 | Improved reactor |
| CN202122922U (en) * | 2011-06-20 | 2012-01-25 | 扬州五亭桥缸套有限公司 | Paint mixing machine |
| CN202191908U (en) * | 2011-08-24 | 2012-04-18 | 安徽亚兰德新能源材料有限公司 | Special reactor for ternary material precursors |
| CN202860527U (en) * | 2012-09-24 | 2013-04-10 | 广东佳景科技有限公司 | High-efficiency reaction kettle |
| CN203108465U (en) * | 2013-03-14 | 2013-08-07 | 内蒙古瑞盛新能源有限公司 | Mixing equipment for concentrated sulfuric acid and hydrogen peroxide |
| CN204429276U (en) * | 2014-12-31 | 2015-07-01 | 丹阳市助剂化工厂有限公司 | Epoxidized soybean oil production and processing high efficiency reactor |
-
2014
- 2014-12-31 CN CN201410845607.XA patent/CN104549105B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN104549105A (en) | 2015-04-29 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104549105B (en) | Epoxy soybean oil production and processing reactor | |
| CN207786495U (en) | A kind of emulsion paint agitator tank | |
| CN204710311U (en) | A kind of accurate temperature control type stirred tank of chemical industry half dry material | |
| CN203874692U (en) | Stirring device | |
| CN203648423U (en) | Mixing tank | |
| CN105435682A (en) | Stirring tank for adhesive processing | |
| CN204768652U (en) | Reation kettle with compounding device | |
| CN108393015A (en) | A kind of liquid charging stock mechanical mixing apparatus for Chemical Manufacture | |
| CN204429276U (en) | Epoxidized soybean oil production and processing high efficiency reactor | |
| CN107551972A (en) | A kind of high efficiency reactor | |
| CN204564132U (en) | There is the reactor of bottom stirrer | |
| CN205323776U (en) | A reation kettle for processing wall paper wall cloth is wet to glue | |
| CN109926013A (en) | A kind of chemical industry stirred autoclave | |
| CN209138480U (en) | A kind of water paint blending tank | |
| CN103861549B (en) | For the production of the reactor of scouring agent | |
| CN207237962U (en) | A kind of reaction kettle for producing liquid barium zinc heat stabilizer | |
| CN206996599U (en) | Automatic charging reactor is used in a kind of liquid barium zinc heat stabilizer production | |
| CN204583186U (en) | A kind of resin reactor | |
| CN206230709U (en) | One kind injection dolly | |
| CN104437332B (en) | A stirring reation kettle for cutting fluid | |
| CN210584908U (en) | Saponification reation kettle that production disproportionated potassium rosinate soap was used | |
| CN209974318U (en) | Device for preparing zinc oxide crystal | |
| CN207371512U (en) | A kind of polyethylene wax retort | |
| CN206082515U (en) | Reaction kettle | |
| CN111705547A (en) | Gloss oil waterproof process capable of replacing film |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Reactor for production and processing of epoxy soybean oil Effective date of registration: 20191220 Granted publication date: 20160928 Pledgee: Industrial Bank Co., Ltd. Zhenjiang Branch Pledgor: DANYANG CITY AUXILIARIES CHEMICAL PLANT CO., LTD. Registration number: Y2019980001199 |
|
| PE01 | Entry into force of the registration of the contract for pledge of patent right |