CN104941554B - A kind of high efficiency reactor - Google Patents
A kind of high efficiency reactor Download PDFInfo
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- CN104941554B CN104941554B CN201510286165.4A CN201510286165A CN104941554B CN 104941554 B CN104941554 B CN 104941554B CN 201510286165 A CN201510286165 A CN 201510286165A CN 104941554 B CN104941554 B CN 104941554B
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Abstract
The invention discloses a kind of new and effective reactor, including reactor body, described reactor body includes reaction zone, top and lower reaction zone, intermediate heat transfer dividing plate it is provided with between reaction zone, described top and described lower reaction zone, running through inside described reactor body and be provided with shaft, the reductor that described shaft is provided with described reactor body top is connected；Reaction zone, described top is respectively equipped with heat exchange guide shell in top heat exchange jacket and top；Described lower reaction zone is respectively equipped with heat exchange guide shell in bottom heat exchange jacket and bottom；The temperature sensor that described reactor body is provided with is connected with automaton respectively with automatic regulating valve, it is achieved being automatically precisely controlled of reactor body materials inside reaction.Compared with prior art, present configuration is simple, and reaction operating mode can realize precisely automatically controlling, and equipment energy continuous high-efficient runs, it is ensured that material reaction effect, the effect of the most large-scale reactor is more prominent, opens the new world of novel reactor.
Description
Technical field
The present invention relates to chemical device technical field, be specifically related to a kind of high efficiency reactor.
Background technology
Reactor is the equipment realizing course of reaction, is widely used in the industrial departments such as chemical industry, oil refining, metallurgy, light industry.Reactor is mainly used in realizing single liquid phase course of reaction and liquid liquid, gas-liquid, liquid-solid, the heterogeneous reaction processes such as gas-liquid-solid, standing in device have stirring (mechanical agitation, airflow stirring etc.) device, when ratio of height to diameter is bigger, available multiple impellers leaf, when in course of reaction, material need to be heated or cooled, set or coil pipe can be added using heat exchange outside reactor, this structure is divided into again internal one or interior laminate layer, or in addition to using heat exchange except reactor and adding set or coil pipe, inside is also adopted by heat exchange coil, this structure is also classified into internal one or interior laminate layer.The former designs, and older efficiency is low, and material reaction operating mode is wayward, and operating cost is high；Latter configuration device efficiency is the lowest, easily causes feed blocking incrustation and equipment can not be made to run continuously.
Summary of the invention
For solving drawbacks described above, it is an object of the invention to provide a kind of high efficiency reactor, this structure of reactor advantages of simple, energy consumption is relatively low, and work efficiency is high, can meet the requirement that equipment runs the most continuously, it is achieved precisely Automated condtrol material reaction operating mode.
For reaching above-mentioned purpose, the present invention adopts the technical scheme that: a kind of high efficiency reactor, including reactor body, described reactor body includes reaction zone, top and lower reaction zone, intermediate heat transfer dividing plate it is provided with between reaction zone, described top and described lower reaction zone, running through inside described reactor body and be provided with shaft, the reductor that described shaft is provided with described reactor body top is connected；Surface, reaction zone, described top is respectively equipped with charging aperture and access hole, described charging aperture sidewall encloses and is provided with charging preventing scaring device, reaction zone, described top sidewall is respectively equipped with solution inlet port, top heat exchange jacket and temperature sensor, top heat transferring medium outlet and top heat transferring medium import it is respectively equipped with on the heat exchange jacket of described top, heat exchange guide shell in top it is provided with inside reaction zone, described top, heat transferring medium outlet in heat transferring medium import and top in top it is connected to outside heat exchange guide shell in described top, in described top heat transferring medium import department and top, heat transferring medium import department is equipped with automatic regulating valve, described shaft heat exchange guide shell position in described top is provided with top material propulsion plant；It is laid with multiple transition discharging opening on described intermediate heat transfer dividing plate, and described intermediate heat transfer dividing plate is connected to dividing plate heat transferring medium import and the outlet of dividing plate heat transferring medium on described reactor body sidewall；Described lower reaction zone sidewall is respectively equipped with thin brilliant floss hole, bottom heat exchange jacket and temperature sensor, bottom heat transferring medium outlet and bottom heat transferring medium import it is respectively equipped with on the heat exchange jacket of described bottom, heat exchange guide shell in bottom it is provided with inside described lower reaction zone, heat transferring medium outlet in heat transferring medium import and bottom in bottom it is connected to outside heat exchange guide shell in described bottom, in described bottom heat transferring medium import department and bottom, heat transferring medium import department is equipped with automatic regulating valve, described shaft heat exchange guide shell position in described bottom is provided with bottom material propulsion plant, drain is further respectively had bottom described lower reaction zone, discharging opening and rinse mouth.
Preferably, described solution inlet port is internally connected with coil pipe in reaction zone, described top, and described coil surface is provided with solution spout.
Described top material propulsion plant and described bottom material propulsion plant all include the angle of several stirring vanes, described stirring vane scalable and described shaft.
Described high efficiency reactor also includes that automaton, described automaton are connected with described temperature sensor, described automatic regulating valve respectively.
Described charging preventing scaring device is externally connected to thermal medium.
Described thin brilliant floss hole is arranged near described dividing plate heat transferring medium import department.
The present invention uses when solid is with liquid reactions, in the top heat exchange jacket that is provided with inside described reactor body, top, in heat exchange guide shell, intermediate heat transfer dividing plate, bottom heat exchange jacket and bottom, heat exchange guide shell sets up heat transferring medium thermal cycle, keep the uniform of whole reactor body internal temperature, thus obtain the mixed reactant that quality is higher；Open solution inlet port feed liquor, the coil pipe being connected with the solution inlet port effect by solution spout, there is certain pressure preferably to merge with solid material, when solution reaches certain liquid level, it is separately turned on top material propulsion plant and bottom material propulsion plant, makes material hybrid reaction in reactor body；Making solid material be entered reactor by charging aperture again, form the curtain of rain during the spout hydrojet of described solution, depositing dust effect is played in the entrance to solid material；The each automatic regulating valve of heat transferring medium import and the chain control of temperature sensor are set, automatically adjust each heat transferring medium import automatic regulating valve to ensure that material reaction temperature in reactor is in span of control；Reactor top material is during reaction cycle, and the material that granule is bigger is entered lower reaction zone by the transition discharging opening on intermediate heat transfer dividing plate and reacts further；React material completely and be discharged to subsequent processing by discharging opening；React incomplete material to be discharged by thin brilliant floss hole.
The present invention in use, makes material internal reaction temperature control, optimal interval, to make material reaction uniform during material circulates in reaction zone, top；Bottom is reacted preferable material and is successively entered into lower reaction zone by central dividing plate, and same efficient lower reaction zone makes material fully react under the operating mode of regulation, last discharging；The access hole that surface, reaction zone, described top is provided with, it is simple to use when equipment breaks down maintenance or observation；The thermal medium of described charging preventing scaring device external connection, is to just make material be maintained at a uniform temperature at the beginning of reaction, thus is not easy incrustation blocking；The stirring vane that described top material propulsion plant and described bottom material propulsion plant are provided with can regulate angle, adapts to the stirring of different material, when material particles degree is big, turn stirring vane angle down, it is simple to slowly comminuting matter, material particles degree hour, tune up angle, it is simple to accelerate reaction efficiency；Described thin brilliant floss hole, near described dividing plate heat transferring medium import department, is to be near completion and under gravity, the mixed reactant that some concentration are low swims in above in bottom reaction, it is simple to discharge from thin brilliant floss hole.
Compared with prior art, the present invention uses when solid and liquid reactions and liquid are with liquid reactions, there is simple in construction, reaction operating mode can be precisely controlled, modularized design, automatically controls the most efficiently, equipment can run by continuous high-efficient, ensureing material reaction effect, the effect of the most large-scale reactor is more prominent, opens the new world of reactor.
Accompanying drawing explanation
With embodiment, the structure and features of the present invention is described further below in conjunction with the accompanying drawings.
Fig. 1 is the structural representation of the present invention.
null1. reductor，2. charging aperture，3. charging preventing scaring device，4. solution spout，5. solution inlet port，6. temperature sensor，7. top heat exchange jacket，8. heat exchange guide shell in top，9. top material propulsion plant，10. automatic regulating valve，11. top heat transferring medium imports，12. dividing plate heat transferring medium imports，13. thin brilliant floss holes，14. access holes，15. bottom heat exchange jackets，Heat exchange guide shell in 16. bottoms，17. top heat transferring medium outlets，18. bottom heat transferring medium imports，19. bottom material propulsion plants，20. drains，21. discharging openings，22. rinse mouths，Heat transferring medium import in 23. bottoms，24. bottom heat transferring medium outlets，25. lower reaction zone，Heat transferring medium outlet in 26. bottoms，27. intermediate heat transfer dividing plates，29. dividing plate heat transferring medium outlets，Heat transferring medium import in 30. tops，Heat transferring medium outlet in 32. tops，33. shafts，34. reaction zone, tops.
Detailed description of the invention
Referring to Fig. 1, a kind of high efficiency reactor, including reactor body, described reactor body includes reaction zone, top 34 and lower reaction zone 25, it is provided with intermediate heat transfer dividing plate 27 between reaction zone, described top 34 and described lower reaction zone 25, running through inside described reactor body and be provided with shaft 33, the reductor 1 that described shaft 33 is provided with described reactor body top is connected；nullSurface, reaction zone 34, described top is respectively equipped with charging aperture 2 and access hole 14，Described charging aperture 2 sidewall is provided with charging preventing scaring device 3，Reaction zone 34, described top sidewall is respectively equipped with solution inlet port 5、Top heat exchange jacket 7 and temperature sensor 6，Top heat transferring medium outlet 17 and top heat transferring medium import 11 it is respectively equipped with on described top heat exchange jacket 7，Described solution inlet port 5 is internally connected with coil pipe in reaction zone, described top 34，Described coil surface is provided with solution spout 4，Reaction zone 34, described top is internal is provided with heat exchange guide shell 8 in top，In described top, heat exchange guide shell 8 is outside is connected to heat transferring medium outlet 32 in heat transferring medium import 30 and top in top，It is equipped with automatic regulating valve 10 at heat transferring medium import 30 at described top heat transferring medium import 11 and in described top，Described shaft 33 heat exchange guide shell 8 position in described top is provided with top material propulsion plant 9；It is laid with multiple transition discharging opening on described intermediate heat transfer dividing plate 27, and described intermediate heat transfer dividing plate 27 is respectively equipped with dividing plate heat transferring medium import 12 and dividing plate heat transferring medium outlet 29 on described reactor body sidewall；Described lower reaction zone 25 sidewall is respectively equipped with thin brilliant floss hole 13, bottom heat exchange jacket 15 and temperature sensor 6, bottom heat transferring medium outlet 24 and bottom heat transferring medium import 18 it is respectively equipped with on described bottom heat exchange jacket 15, described lower reaction zone 25 is internal is provided with heat exchange guide shell 16 in bottom, in described bottom, heat exchange guide shell 16 is outside is connected to heat transferring medium outlet 26 in heat transferring medium import 23 and bottom in bottom, heat transferring medium import department 23 is equipped with automatic regulating valve 10 at described bottom heat transferring medium import 18 and in bottom, described shaft 33 heat exchange guide shell 16 position in described bottom is provided with bottom material propulsion plant 19, drain 20 is further respectively had bottom described lower reaction zone, discharging opening 21 and rinse mouth 22；Described top material propulsion plant 9 and described bottom material propulsion plant 19 all include several stirring vanes；Described high efficiency reactor also includes automaton, and described automaton is connected with described temperature sensor 6, described automatic regulating valve 10 respectively.
The present invention uses when solid and liquid reactions, and in top heat exchange jacket 7 described reactor body within, top, in heat exchange guide shell 8, intermediate heat transfer dividing plate 27, bottom heat exchange jacket 15 and bottom, heat exchange guide shell 16 is set up heat transferring medium and circulated；Open solution inlet port 5 feed liquor, when reaching certain liquid level, be separately turned on top material propulsion plant 9 and bottom material propulsion plant 19, make solution circulate in reactor body；Solid material is made to be entered reactor body reaction by charging aperture 2 again；Top heat transferring medium import 11 and each automatic regulating valve of bottom heat transferring medium import 18 10 and the chain control of temperature sensor 6 are set, automatically adjust each heat transferring medium import automatic regulating valve 10 to ensure that material reaction temperature in reactor is in span of control；Material is during the reaction cycle of reaction zone, top, and the material that granule is bigger is entered lower reaction zone 25 by the transition discharging opening on intermediate heat transfer dividing plate 27 and reacts further；React material completely and be discharged to subsequent processing by discharging opening 21；React incomplete material to be discharged by thin brilliant floss hole 13.
Material internal reaction temperature is made to control, optimal interval, to make material reaction uniform during material circulates in reaction zone, top；Bottom is reacted preferable material and is successively entered into lower reaction zone by centre separation dividing plate, and same efficient lower reaction zone makes material fully react under the operating mode of regulation, last discharging.Compared with prior art, the present invention uses when solid and liquid reactions and liquid are with liquid reactions, there is simple in construction, reaction operating mode can be precisely controlled, modularized design, automatically controls the most efficiently, equipment can run by continuous high-efficient, ensureing material reaction effect, the effect of the most large-scale reactor is more prominent, opens the new world of reactor.
The present invention in actual use, can be used for solid with liquid reactions it can also be used to liquid and liquid reactions, and the thermal medium of use can be condensed water or heat steam, or other media.
Described above is only presently preferred embodiments of the present invention, and above-mentioned specific embodiment is not limitation of the present invention, and retouching, amendment or the equivalent that all those of ordinary skill in the art are made as described above belongs to protection scope of the present invention.
Claims (6)
1. a high efficiency reactor, including reactor body, it is characterized in that: described reactor body includes reaction zone, top and lower reaction zone, intermediate heat transfer dividing plate it is provided with between reaction zone, described top and described lower reaction zone, running through inside described reactor body and be provided with shaft, the reductor that described shaft is provided with described reactor body top is connected；Surface, reaction zone, described top is respectively equipped with charging aperture and access hole, described charging aperture sidewall encloses and is provided with charging preventing scaring device, reaction zone, described top sidewall is respectively equipped with solution inlet port, top heat exchange jacket and temperature sensor, top heat transferring medium outlet and top heat transferring medium import it is respectively equipped with on the heat exchange jacket of described top, heat exchange guide shell in top it is provided with inside reaction zone, described top, heat transferring medium outlet in heat transferring medium import and top in top it is connected to outside heat exchange guide shell in described top, in described top heat transferring medium import department and top, heat transferring medium import department is equipped with automatic regulating valve, described shaft heat exchange guide shell position in described top is provided with top material propulsion plant；It is laid with multiple transition discharging opening on described intermediate heat transfer dividing plate, and described intermediate heat transfer dividing plate is connected to dividing plate heat transferring medium import and the outlet of dividing plate heat transferring medium on described reactor body sidewall；Described lower reaction zone sidewall is respectively equipped with thin brilliant floss hole, bottom heat exchange jacket and temperature sensor, bottom heat transferring medium outlet and bottom heat transferring medium import it is respectively equipped with on the heat exchange jacket of described bottom, heat exchange guide shell in bottom it is provided with inside described lower reaction zone, heat transferring medium outlet in heat transferring medium import and bottom in bottom it is connected to outside heat exchange guide shell in described bottom, in described bottom heat transferring medium import department and bottom, heat transferring medium import department is equipped with automatic regulating valve, described shaft heat exchange guide shell position in described bottom is provided with bottom material propulsion plant, drain is further respectively had bottom described lower reaction zone, discharging opening and rinse mouth.
High efficiency reactor the most according to claim 1, it is characterised in that: described solution inlet port is internally connected with coil pipe in reaction zone, described top, and described coil surface is provided with solution spout.
High efficiency reactor the most according to claim 1, it is characterised in that: described top material propulsion plant and described bottom material propulsion plant all include the angle of several stirring vanes, described stirring vane scalable and described shaft.
High efficiency reactor the most according to claim 1, it is characterised in that: described high efficiency reactor also includes that automaton, described automaton are connected with described temperature sensor, described automatic regulating valve respectively.
High efficiency reactor the most according to claim 1, it is characterised in that: described charging preventing scaring device is externally connected to thermal medium.
High efficiency reactor the most according to claim 1, it is characterised in that: described thin brilliant floss hole is arranged near described dividing plate heat transferring medium import department.
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| CN201510286165.4A CN104941554B (en) | 2015-05-29 | 2015-05-29 | A kind of high efficiency reactor |
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| CN105749848A (en) * | 2016-04-28 | 2016-07-13 | 庆丰鞋业（江苏）有限公司 | Reaction still for polymerization reaction of multiple monomers |
| CN105944647B (en) * | 2016-06-30 | 2017-11-17 | 江南大学 | A kind of efficient mass transfer, the gentle liquid-solid reactor device of extensive gas-liquid of heat transfer |
| CN106512909B (en) * | 2017-01-10 | 2019-11-12 | 山东豪迈化工技术有限公司 | A kind of sectional temperature-controlled reactor and its agitating shaft |
| CN109701477A (en) * | 2019-01-27 | 2019-05-03 | 河北科技大学 | A kind of device suitable for heterogeneous reaction |
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| CN101012214A (en) * | 2006-12-29 | 2007-08-08 | 浙江大学 | Reaction device for preparing oil soluble tea polypherals |
| CN203002374U (en) * | 2013-01-04 | 2013-06-19 | 珠海金鸡化工有限公司 | Polymerization reaction device for producing carboxylic butadiene-styrene latex |
| CN203778010U (en) * | 2014-03-03 | 2014-08-20 | 深圳高远通新材料科技有限公司 | Adhesive processing reaction kettle |
| CN104549105B (en) * | 2014-12-31 | 2016-09-28 | 丹阳市助剂化工厂有限公司 | Epoxy soybean oil production and processing reactor |
| CN204685100U (en) * | 2015-05-29 | 2015-10-07 | 吴巴特尔 | A kind of new and effective reactor |
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