CN104941554A - Novel high efficiency reactor - Google Patents
Novel high efficiency reactor Download PDFInfo
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- CN104941554A CN104941554A CN201510286165.4A CN201510286165A CN104941554A CN 104941554 A CN104941554 A CN 104941554A CN 201510286165 A CN201510286165 A CN 201510286165A CN 104941554 A CN104941554 A CN 104941554A
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Abstract
The invention discloses a novel high efficiency reactor, which comprises a reactor body, the reactor body comprises an upper reaction zone and a bottom reaction zone, an intermediate heat exchange separator plate is arranged between the upper reaction zone and the lower reaction zone, a mixer shaft passes through the reactor body, the mixer shaft is connected to a speed reducer arranged on the upper part of the reactor body, an upper heat exchange jacket and an upper inner heat exchange guide shell are respectively arranged on the upper reaction zone; a lower heat exchange jacket and an lower inner heat exchange guide shell are respectively arranged on the lower reaction zone; a temperature sensor arranged on the reactor body and an automatic regulating valve are respectively connected to an automatic control device, and automatic accurate control of the reaction of the materials in the reactor body can be realized. Compared with prior art, a structure of the high efficiency reactor is simple, accurate automatic control can be realized, continuous high efficiency operation of the high efficiency reactor can be carried out, material reaction effect is ensured, effect of the large-scale reactor is more protruding, and a novel development of the novel reactor can be provided.
Description
Technical field
The present invention relates to chemical device technical field, be specifically related to a kind of new and effective reactor.
Background technology
Reactor is the equipment of realization response process, is widely used in the industrial departments such as chemical industry, oil refining, metallurgy, light industry.Reactor is mainly used in realizing single liquid phase course of reaction and liquid liquid, gas-liquid, liquid-solid, the heterogeneous reaction processes such as gas-liquid-solid, standing in device have stirring (mechanical agitation, airflow stirring etc.) device, when ratio of height to diameter is larger, available multiple impellers leaf, when in course of reaction, material need heat or cool, heat exchange can adopted to add cover or coil pipe in reactor outside, this structure is divided into again inner one or interior laminate layer, or except reactor except outside adopts heat exchange to add except cover or coil pipe, inside also adopts heat exchange coil, this structure is also divided into inner one or interior laminate layer.The older efficiency of the former design is low, and material reaction operating mode is wayward, and operating cost is high; The latter's structural device efficiency is also low, easily causes feed blocking to form a scab and equipment can not be made to run continuously.
Summary of the invention
For addressing the aforementioned drawbacks, the object of this invention is to provide a kind of new and effective reactor, this structure of reactor advantages of simple, energy consumption is lower, and operating efficiency is high, can meet the requirement that equipment runs for a long time continuously, realizes accurate Automated condtrol material reaction operating mode.
For achieving the above object, the technical scheme that the present invention takes is: a kind of new and effective reactor, comprise reactor body, described reactor body comprises top reaction zone and lower reaction zone, intermediate heat transfer dividing plate is provided with between described top reaction zone and described lower reaction zone, described reactor body inside is run through and is provided with shaft, and the reductor that described shaft is provided with described reactor body top is connected, reaction zone surface, described top is respectively equipped with charging aperture and access hole, described charging aperture sidewall is arranged with charging preventing scaring device, described top reaction zone sidewall is respectively equipped with solution inlet port, top heat exchange jacket and temperature sensor, described top heat exchange jacket is respectively equipped with top heat transferring medium outlet and top heat transferring medium import, reaction zone inside, described top is provided with heat exchange guide shell in top, in described top, heat exchange guide shell outside is connected to heat transferring medium outlet in heat transferring medium import and top in top, in described top heat transferring medium import department and top, heat transferring medium import department is equipped with automatic regulating valve, described shaft heat exchange guide shell position in described top is provided with top material propulsion plant, described intermediate heat transfer dividing plate is laid with multiple transition discharging opening, and described intermediate heat transfer dividing plate is connected to the import of dividing plate heat transferring medium and the outlet of dividing plate heat transferring medium on described reactor body sidewall, described lower reaction zone sidewall is respectively equipped with thin brilliant floss hole, bottom heat exchange jacket and temperature sensor, described bottom heat exchange jacket is respectively equipped with bottom heat transferring medium outlet and bottom heat transferring medium import, inside, described lower reaction zone is provided with heat exchange guide shell in bottom, in described bottom, heat exchange guide shell outside is connected to heat transferring medium outlet in heat transferring medium import and bottom in bottom, in described bottom heat transferring medium import department and bottom, heat transferring medium import department is equipped with automatic regulating valve, described shaft heat exchange guide shell position in described bottom is provided with bottom material propulsion plant, also drain is respectively equipped with bottom described lower reaction zone, discharging opening and rinse mouth.
Preferably, described solution inlet port is internally connected with coil pipe at described top reaction zone, and described coil surface is provided with solution spout.
Described top material propulsion plant and described bottom material propulsion plant include several stirring vanes, the angle of the adjustable and described shaft of described stirring vane.
Described new and effective reactor also comprises automaton, and described automaton is connected with described temperature sensor, described automatic regulating valve respectively.
Described charging preventing scaring device is externally connected to thermal medium.
Described thin brilliant floss hole is arranged near described dividing plate heat transferring medium import department.
When the present invention is used in solid and liquid reactions, in the top heat exchange jacket that described reactor body inside is provided with, top, in heat exchange guide shell, intermediate heat transfer dividing plate, bottom heat exchange jacket and bottom, heat exchange guide shell sets up heat transferring medium thermal cycle, keep the even of whole reactor body internal temperature, thus obtain the higher mixed reactant of quality; Open solution inlet port feed liquor, the coil pipe be connected with solution inlet port is by the effect of solution spout, there is certain pressure energy and solid material better merges, when solution reaches certain liquid level, open top material propulsion plant and bottom material propulsion plant respectively, make material hybrid reaction in reactor body; Make solid material enter reactor by charging aperture again, form the curtain of rain in the spout hydrojet process of described solution, depositing dust effect is played to entering of solid material; Arrange each automatic regulating valve of heat transferring medium import and the chain control of temperature sensor, each heat transferring medium import automatic regulating valve of adjustment is to ensure that the reaction temperature of material in reactor is in control range automatically; Reactor top material is in reaction cycle process, and the material that particle is larger enters lower reaction zone by the transition discharging opening on intermediate heat transfer dividing plate and reacts further; The material reacted completely is discharged to subsequent processing by discharging opening; React incomplete material to be discharged by thin brilliant floss hole.
The present invention in use, when material makes internal batch reaction temperature control between optimal zone in the process of top reaction zone Inner eycle, makes material reaction even; Bottom is reacted better material and is successively entered into lower reaction zone by central dividing plate, and same lower reaction zone efficiently makes material fully react under the operating mode of regulation, last discharging; The access hole that reaction zone surface, described top is provided with, is convenient to use when equipment breaks down maintenance or observation; The thermal medium that described charging preventing scaring device outside connects, is in order under just making material remain on a uniform temperature at the beginning of reaction, thus is not easy incrustation blocking; The stirring vane that described top material propulsion plant and described bottom material propulsion plant are provided with can adjusting angle, adapt to the stirring of different material, when material particles degree is large, turn stirring vane angle down, be convenient to slow comminuting matter, material particles degree hour, tunes up angle, is convenient to accelerate reaction efficiency; Described thin brilliant floss hole, near described dividing plate heat transferring medium import department, is to be near completion in bottom reaction and under gravity, above the mixed reactant that some concentration are low swims in, being convenient to discharge from thin brilliant floss hole.
Compared with prior art, when the present invention is used in solid and liquid reactions and liquid and liquid reactions, there is structure simple, reaction operating mode can precisely control, modularized design, automatically controls precisely efficient, equipment can run by continuous high-efficient, ensure material reaction effect, the effect of especially large-scale reactor is more outstanding, opens the new world of novel reactor.
Accompanying drawing explanation
Below in conjunction with drawings and Examples, structure of the present invention and feature are described further.
Fig. 1 is structural representation of the present invention.
1. reductor, 2. charging aperture, 3. charging preventing scaring device, 4. solution spout, 5. solution inlet port, 6. temperature sensor, 7. top heat exchange jacket, 8. heat exchange guide shell in top, 9. top material propulsion plant, 10. automatic regulating valve, 11. top heat transferring medium imports, 12. dividing plate heat transferring medium imports, 13. thin brilliant floss holes, 14. access holes, 15. bottom heat exchange jackets, heat exchange guide shell in 16. bottoms, 17. top heat transferring medium outlets, 18. bottom heat transferring medium imports, 19. bottom material propulsion plants, 20. drains, 21. discharging openings, 22. rinse mouths, heat transferring medium import in 23. bottoms, 24. bottom heat transferring medium outlets, 25. lower reaction zone, heat transferring medium outlet in 26. bottoms, 27. intermediate heat transfer dividing plates, 29. dividing plate heat transferring medium outlets, heat transferring medium import in 30. tops, heat transferring medium outlet in 32. tops, 33. shafts, 34. top reaction zones.
Detailed description of the invention
Referring to Fig. 1, a kind of new and effective reactor, comprise reactor body, described reactor body comprises top reaction zone 34 and lower reaction zone 25, intermediate heat transfer dividing plate 27 is provided with between described top reaction zone 34 and described lower reaction zone 25, described reactor body inside is run through and is provided with shaft 33, and the reductor 1 that described shaft 33 is provided with described reactor body top is connected, reaction zone 34 surface, described top is respectively equipped with charging aperture 2 and access hole 14, described charging aperture 2 sidewall is provided with charging preventing scaring device 3, described top reaction zone 34 sidewall is respectively equipped with solution inlet port 5, top heat exchange jacket 7 and temperature sensor 6, described top heat exchange jacket 7 is respectively equipped with top heat transferring medium outlet 17 and top heat transferring medium import 11, described solution inlet port 5 is internally connected with coil pipe at described top reaction zone 34, described coil surface is provided with solution spout 4, reaction zone 34 inside, described top is provided with heat exchange guide shell 8 in top, in described top, heat exchange guide shell 8 outside is connected to heat transferring medium outlet 32 in heat transferring medium import 30 and top in top, in heat transferring medium import 11 place, described top and described top, heat transferring medium import 30 place is equipped with automatic regulating valve 10, described shaft 33 heat exchange guide shell 8 position in described top is provided with top material propulsion plant 9, described intermediate heat transfer dividing plate 27 is laid with multiple transition discharging opening, and described intermediate heat transfer dividing plate 27 is respectively equipped with dividing plate heat transferring medium import 12 and dividing plate heat transferring medium outlet 29 on described reactor body sidewall, described lower reaction zone 25 sidewall is respectively equipped with thin brilliant floss hole 13, bottom heat exchange jacket 15 and temperature sensor 6, described bottom heat exchange jacket 15 is respectively equipped with bottom heat transferring medium outlet 24 and bottom heat transferring medium import 18, inside, described lower reaction zone 25 is provided with heat exchange guide shell 16 in bottom, in described bottom, heat exchange guide shell 16 outside is connected to heat transferring medium outlet 26 in heat transferring medium import 23 and bottom in bottom, in heat transferring medium import 18 place, described bottom and bottom, heat transferring medium import department 23 is equipped with automatic regulating valve 10, described shaft 33 heat exchange guide shell 16 position in described bottom is provided with bottom material propulsion plant 19, drain 20 is also respectively equipped with bottom described lower reaction zone, discharging opening 21 and rinse mouth 22, described top material propulsion plant 9 and described bottom material propulsion plant 19 include several stirring vanes, described new and effective reactor also comprises automaton, and described automaton is connected with described temperature sensor 6, described automatic regulating valve 10 respectively.
When the present invention is used in solid and liquid reactions, in the top heat exchange jacket 7 of described reactor body inside, top, in heat exchange guide shell 8, intermediate heat transfer dividing plate 27, bottom heat exchange jacket 15 and bottom, heat exchange guide shell 16 sets up heat transferring medium circulation; Open solution inlet port 5 feed liquor, when reaching certain liquid level, open top material propulsion plant 9 and bottom material propulsion plant 19 respectively, make solution at reactor body Inner eycle; Make solid material enter reactor body by charging aperture 2 again to react; Arrange top heat transferring medium import 11 and each automatic regulating valve of bottom heat transferring medium import 18 10 and the chain control of temperature sensor 6, each heat transferring medium import automatic regulating valve 10 of adjustment is to ensure that the reaction temperature of material in reactor is in control range automatically; Material is in the reaction zone reaction cycle process of top, and the material that particle is larger enters lower reaction zone 25 by the transition discharging opening on intermediate heat transfer dividing plate 27 and reacts further; The material reacted completely is discharged to subsequent processing by discharging opening 21; React incomplete material to be discharged by thin brilliant floss hole 13.
When material makes internal batch reaction temperature control between optimal zone in the process of top reaction zone Inner eycle, make material reaction even; Bottom is reacted better material and is successively entered into lower reaction zone by the middle dividing plate that is separated, and same lower reaction zone efficiently makes material fully react under the operating mode of regulation, last discharging.Compared with prior art, when the present invention is used in solid and liquid reactions and liquid and liquid reactions, there is structure simple, reaction operating mode can precisely control, modularized design, automatically controls precisely efficient, equipment can run by continuous high-efficient, ensure material reaction effect, the effect of especially large-scale reactor is more outstanding, opens the new world of novel reactor.
The present invention in actual use, can be used for solid and liquid reactions, also can be used for liquid and liquid reactions, and the thermal medium of use can be condensed water or heat steam, or other media.
Described above is only preferred embodiment of the present invention, and above-mentioned specific embodiment is not limitation of the present invention, and all those of ordinary skill in the art, according to describing retouching, the amendment made above or equivalent replacing, all belong to protection scope of the present invention.
Claims (6)
1. a new and effective reactor, comprise reactor body, it is characterized in that: described reactor body comprises top reaction zone and lower reaction zone, intermediate heat transfer dividing plate is provided with between described top reaction zone and described lower reaction zone, described reactor body inside is run through and is provided with shaft, and the reductor that described shaft is provided with described reactor body top is connected, reaction zone surface, described top is respectively equipped with charging aperture and access hole, described charging aperture sidewall is arranged with charging preventing scaring device, described top reaction zone sidewall is respectively equipped with solution inlet port, top heat exchange jacket and temperature sensor, described top heat exchange jacket is respectively equipped with top heat transferring medium outlet and top heat transferring medium import, reaction zone inside, described top is provided with heat exchange guide shell in top, in described top, heat exchange guide shell outside is connected to heat transferring medium outlet in heat transferring medium import and top in top, in described top heat transferring medium import department and top, heat transferring medium import department is equipped with automatic regulating valve, described shaft heat exchange guide shell position in described top is provided with top material propulsion plant, described intermediate heat transfer dividing plate is laid with multiple transition discharging opening, and described intermediate heat transfer dividing plate is connected to the import of dividing plate heat transferring medium and the outlet of dividing plate heat transferring medium on described reactor body sidewall, described lower reaction zone sidewall is respectively equipped with thin brilliant floss hole, bottom heat exchange jacket and temperature sensor, described bottom heat exchange jacket is respectively equipped with bottom heat transferring medium outlet and bottom heat transferring medium import, inside, described lower reaction zone is provided with heat exchange guide shell in bottom, in described bottom, heat exchange guide shell outside is connected to heat transferring medium outlet in heat transferring medium import and bottom in bottom, in described bottom heat transferring medium import department and bottom, heat transferring medium import department is equipped with automatic regulating valve, described shaft heat exchange guide shell position in described bottom is provided with bottom material propulsion plant, also drain is respectively equipped with bottom described lower reaction zone, discharging opening and rinse mouth.
2. new and effective reactor according to claim 1, is characterized in that: described solution inlet port is internally connected with coil pipe at described top reaction zone, and described coil surface is provided with solution spout.
3. new and effective reactor according to claim 1, is characterized in that: described top material propulsion plant and described bottom material propulsion plant include several stirring vanes, the angle of the adjustable and described shaft of described stirring vane.
4. new and effective reactor according to claim 1, is characterized in that: described automaton is connected with described temperature sensor, described automatic regulating valve respectively.
5. new and effective reactor according to claim 1, is characterized in that: described charging preventing scaring device is externally connected to thermal medium.
6. new and effective reactor according to claim 1, is characterized in that: described thin brilliant floss hole is arranged near described dividing plate heat transferring medium import department.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105749848A (en) * | 2016-04-28 | 2016-07-13 | 庆丰鞋业（江苏）有限公司 | Reaction still for polymerization reaction of multiple monomers |
| CN105944647A (en) * | 2016-06-30 | 2016-09-21 | 江南大学 | Large-scale gas-liquid and gas-liquid-solid reactor device with efficient mass transfer and heat transfer |
| CN106512909A (en) * | 2017-01-10 | 2017-03-22 | 山东豪迈化工技术有限公司 | Staged-temperature-controlled reactor and stirring shaft thereof |
| CN109701477A (en) * | 2019-01-27 | 2019-05-03 | 河北科技大学 | A kind of device suitable for heterogeneous reaction |
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| CN101012214A (en) * | 2006-12-29 | 2007-08-08 | 浙江大学 | Reaction device for preparing oil soluble tea polypherals |
| CN203002374U (en) * | 2013-01-04 | 2013-06-19 | 珠海金鸡化工有限公司 | Polymerization reaction device for producing carboxylic butadiene-styrene latex |
| CN203778010U (en) * | 2014-03-03 | 2014-08-20 | 深圳高远通新材料科技有限公司 | Adhesive processing reaction kettle |
| CN104549105A (en) * | 2014-12-31 | 2015-04-29 | 丹阳市助剂化工厂有限公司 | Efficient reactor for production and processing of epoxy soybean oil |
| CN204685100U (en) * | 2015-05-29 | 2015-10-07 | 吴巴特尔 | A kind of new and effective reactor |
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2015
- 2015-05-29 CN CN201510286165.4A patent/CN104941554B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101012214A (en) * | 2006-12-29 | 2007-08-08 | 浙江大学 | Reaction device for preparing oil soluble tea polypherals |
| CN203002374U (en) * | 2013-01-04 | 2013-06-19 | 珠海金鸡化工有限公司 | Polymerization reaction device for producing carboxylic butadiene-styrene latex |
| CN203778010U (en) * | 2014-03-03 | 2014-08-20 | 深圳高远通新材料科技有限公司 | Adhesive processing reaction kettle |
| CN104549105A (en) * | 2014-12-31 | 2015-04-29 | 丹阳市助剂化工厂有限公司 | Efficient reactor for production and processing of epoxy soybean oil |
| CN204685100U (en) * | 2015-05-29 | 2015-10-07 | 吴巴特尔 | A kind of new and effective reactor |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105749848A (en) * | 2016-04-28 | 2016-07-13 | 庆丰鞋业（江苏）有限公司 | Reaction still for polymerization reaction of multiple monomers |
| CN105944647A (en) * | 2016-06-30 | 2016-09-21 | 江南大学 | Large-scale gas-liquid and gas-liquid-solid reactor device with efficient mass transfer and heat transfer |
| CN105944647B (en) * | 2016-06-30 | 2017-11-17 | 江南大学 | A kind of efficient mass transfer, the gentle liquid-solid reactor device of extensive gas-liquid of heat transfer |
| CN106512909A (en) * | 2017-01-10 | 2017-03-22 | 山东豪迈化工技术有限公司 | Staged-temperature-controlled reactor and stirring shaft thereof |
| CN109701477A (en) * | 2019-01-27 | 2019-05-03 | 河北科技大学 | A kind of device suitable for heterogeneous reaction |
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| CN104941554B (en) | 2017-01-04 |
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