CN104542729A - Azadirachtin-containing botanical insect aerosol and preparation method thereof - Google Patents

Azadirachtin-containing botanical insect aerosol and preparation method thereof Download PDF

Info

Publication number
CN104542729A
CN104542729A CN201410811197.7A CN201410811197A CN104542729A CN 104542729 A CN104542729 A CN 104542729A CN 201410811197 A CN201410811197 A CN 201410811197A CN 104542729 A CN104542729 A CN 104542729A
Authority
CN
China
Prior art keywords
aerosol
nimbin
cosolvent
emulsifier
surfactant
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201410811197.7A
Other languages
Chinese (zh)
Other versions
CN104542729B (en
Inventor
张勇
黄耿
丁城峰
刘艳
朱新成
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
CHENGDU GREEN GOLD HIGH-TECH Co Ltd
Original Assignee
CHENGDU GREEN GOLD HIGH-TECH Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by CHENGDU GREEN GOLD HIGH-TECH Co Ltd filed Critical CHENGDU GREEN GOLD HIGH-TECH Co Ltd
Priority to CN201410811197.7A priority Critical patent/CN104542729B/en
Publication of CN104542729A publication Critical patent/CN104542729A/en
Application granted granted Critical
Publication of CN104542729B publication Critical patent/CN104542729B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

Landscapes

  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses azadirachtin-containing botanical insect aerosol and a preparation method thereof and aims at solving the problem that the effect of the existing insect aerosol is not ideal. The azadirachtin-containing botanical insect aerosol comprises the following components in percentage by weight: 0.1-3% of azadirachtin, 1-20% of neem oil, 0.1-3% of a surface active agent, 8-15% of a cosolvent, 1-10% of an emulsifying agent and the balance of a solvent. The azadirachtin-containing botanical insect aerosol has the advantages that azadirachtin and neem oil are botanical natural active substances, high efficiency, low toxicity, no residue and safety for a human body are realized, indoor environment is not polluted, the requirement of people for environmental friendliness of a hygienic insecticide is met, and the azadirachtin-containing botanical insect aerosol is applicable to control of health pests in places to live, working places, dining places and the like.

Description

A kind of vegetable source pesticide aerosol containing nimbin and preparation method thereof
Technical field
The present invention relates to a kind of vegetable source pesticide aerosol containing nimbin and preparation method thereof.
Background technology
Nimbin, as good Plant antifeedant, has good repellent action to multiple sanitary insect pest, and low toxic and environment-friendly, to person poultry safety, has the potentiality being developed as hygienic insecticide simultaneously.Current azadirachtin preparation product is mainly used in above agricultural, does not also have sending out in nimbin hygienic biocide spray to open, belongs to the market vacancy.
Existing plant source sanitary insecticide kind is single: the sanitary insect pest taking mosquito as representative, by harassing, biting, the various ways harm humans life such as parasitic, and can spread disease cause of disease and the epidemic disease such as the plague, typhoid fever, the life security of serious threat people.Hygienic biocide aerosol and owing to being directly applied in human residential environment, contacts time long with human body, therefore higher to its security requirement.For a long time, the control of sanitary insect pest is mainly used to the pyrethroid pesticide of chemosynthesis, although compared with other chemical pesticides, its toxicity is very low, and Long-Time Service still has potential impact to living environment and health.
The plant source sanitary insecticide of current use, mainly based on natural pyrethrum, the feature due to natural pyrethrum is that knocking down property is strong but the lasting period is short, needs regular Reusability, also can affect to indoor environment when indoor use.
Summary of the invention
The object of the present invention is to provide a kind of vegetable source pesticide aerosol containing nimbin and preparation method thereof, solve the problem that existing insect aerosol effect is undesirable.
To achieve these goals, technical scheme of the present invention is as follows:
Containing a vegetable source pesticide aerosol for nimbin, described insect aerosol is made up of the component of following weight percents:
Nimbin 0.1 ~ 3%
Neem oil 1 ~ 20%
Surfactant 0.1 ~ 3%
Cosolvent 8 ~ 15%
Emulsifier 1 ~ 10%;
Finally, with solvent polishing to 100%.
Particularly, described insect aerosol is the nimbin of 0.3%, neem oil, the surfactant of 0.2%, cosolvent, the emulsifier of 3%, the solvent composition of 83.5% of 8% of 5% by percentage by weight.
Particularly, described insect aerosol is the nimbin of 0.1%, neem oil, the surfactant of 0.2%, cosolvent, the emulsifier of 5%, the solvent composition of 76.7% of 10% of 8% by percentage by weight.
Particularly, described insect aerosol is the nimbin of 1%, neem oil, the surfactant of 1%, cosolvent, the emulsifier of 7%, the solvent composition of 67% of 12% of 12% by percentage by weight.
Particularly, described insect aerosol is the nimbin of 2%, neem oil, the surfactant of 2%, cosolvent, the emulsifier of 4%, the solvent composition of 64% of 13% of 15% by percentage by weight.
Particularly, described insect aerosol is the nimbin of 1.5%, neem oil, the surfactant of 1.5%, cosolvent, the emulsifier of 1%, the solvent composition of 68% of 9% of 19% by percentage by weight.
Particularly, described insect aerosol is the nimbin of 0.8%, neem oil, the surfactant of 0.8%, cosolvent, the emulsifier of 9%, the solvent composition of 76.4% of 10% of 3% by percentage by weight.
Preferred as one, described solvent is eucalyptus oil, mineral oil or turpentine-based vegetable oil.Described cosolvent is isopropyl alcohol or By-120.
Containing a preparation method for the vegetable source pesticide aerosol of nimbin, comprise the following steps:
(1) nimbin and neem oil are dissolved in cosolvent;
(2) add surfactant, emulsifier, solvent, be then stirred well to evenly, obtain aerosol liquid;
(3) aerosol liquid is loaded in aerosol container, and be pressed into propellant under elevated pressure conditions, obtain aerosol products; Wherein be pressed into the temperature of propellant process lower than 54 DEG C.
The present invention compared with prior art, has the following advantages and beneficial effect:
The nimbin that the present invention adopts and neem oil all have natural plant active substance, high-efficiency low-toxicity, noresidue, to human-body safety, and do not pollute indoor environment, meet the green of people to hygienic insecticide, the requirement of environmental protection, be applicable to the health pest control in the places such as inhabitation, office, dining; The processing technology of this product is simple simultaneously, is suitable for batch production.
Solvent of the present invention selects vegetable oil solvent, abandons the solvent of traditional arene; Because carry out the hygienic insecticide that uses in indoor and people and animals time of contact is long and for a long time, traditional aromatic hydrocarbon solvent is comparatively large to people and animals' harm, is not suitable for using in indoor.This formulation product adopts the vegetable oil solvent coming from plant, and low toxic and environment-friendly, and fragrant odour, meet the demand of hygienic insecticide.
Embodiment
Below in conjunction with embodiment, the invention will be further described, and embodiments of the present invention include but not limited to the following example.
Embodiment 1
Containing the vegetable source pesticide aerosol of nimbin, described insect aerosol is the nimbin of 0.3%, neem oil, the surfactant of 0.2%, cosolvent, the emulsifier of 3%, the solvent composition of 83.5% of 8% of 5% by percentage by weight.Wherein, preferred as one, the solvent of the present embodiment is eucalyptus oil, and cosolvent is isopropyl alcohol.
Its preparation method is as follows:
(1) nimbin of above-mentioned percentage by weight and neem oil are dissolved in cosolvent;
(2) add surfactant, emulsifier, solvent, be then stirred well to evenly, obtain aerosol liquid;
(3) aerosol liquid is loaded in aerosol container, and be pressed into propellant under elevated pressure conditions, obtain aerosol products; Wherein be pressed into the temperature of propellant process lower than 54 DEG C.
What deserves to be explained is, because nimbin is comparatively responsive to temperature, so need the impact considering temperature when preparing this product, when more than 54 DEG C, nimbin is very easily degraded, so the pressure needing control to be pressed in propellant process of press in and temperature are on the impact of stability of azadirachtin.So propellant process of press in temperature of the present invention controls below 54 DEG C.
The test performance that table 1 is the embodiment of the present invention 1 products made thereby and domestic be up to the standard comparing at present.
Table 1
As can be seen from Table 1, the performance test data of product of the present invention is all better than domestic existing level.
Embodiment 2
Containing the vegetable source pesticide aerosol of nimbin, described insect aerosol is the nimbin of 0.1%, neem oil, the surfactant of 0.2%, cosolvent, the emulsifier of 5%, the solvent composition of 76.7% of 10% of 8% by percentage by weight.Wherein, preferred as one, the solvent of the present embodiment is eucalyptus oil, and cosolvent is By-120.
Its preparation method is as follows:
(1) nimbin of above-mentioned percentage by weight and neem oil are dissolved in cosolvent;
(2) add surfactant, emulsifier, solvent, be then stirred well to evenly, obtain aerosol liquid;
(3) aerosol liquid is loaded in aerosol container, and be pressed into propellant under elevated pressure conditions, obtain aerosol products; Wherein be pressed into the temperature of propellant process lower than 54 DEG C.
Embodiment 3
Containing the vegetable source pesticide aerosol of nimbin, described insect aerosol is the nimbin of 1%, neem oil, the surfactant of 1%, cosolvent, the emulsifier of 7%, the solvent composition of 67% of 12% of 12% by percentage by weight.Wherein, preferred as one, the solvent of the present embodiment is turpentine-based vegetable oil, and cosolvent is isopropyl alcohol.
Its preparation method is as follows:
(1) nimbin of above-mentioned percentage by weight and neem oil are dissolved in cosolvent;
(2) add surfactant, emulsifier, solvent, be then stirred well to evenly, obtain aerosol liquid;
(3) aerosol liquid is loaded in aerosol container, and be pressed into propellant under elevated pressure conditions, obtain aerosol products; Wherein be pressed into the temperature of propellant process lower than 54 DEG C.
Embodiment 4
Containing the vegetable source pesticide aerosol of nimbin, described insect aerosol is the nimbin of 2%, neem oil, the surfactant of 2%, cosolvent, the emulsifier of 4%, the solvent composition of 64% of 13% of 15% by percentage by weight.Wherein, preferred as one, the solvent of the present embodiment is turpentine-based vegetable oil, and cosolvent is By-120.
Its preparation method is as follows:
(1) nimbin of above-mentioned percentage by weight and neem oil are dissolved in cosolvent;
(2) add surfactant, emulsifier, solvent, be then stirred well to evenly, obtain aerosol liquid;
(3) aerosol liquid is loaded in aerosol container, and be pressed into propellant under elevated pressure conditions, obtain aerosol products; Wherein be pressed into the temperature of propellant process lower than 54 DEG C.
Embodiment 5
Containing the vegetable source pesticide aerosol of nimbin, described insect aerosol is the nimbin of 1.5%, neem oil, the surfactant of 1.5%, cosolvent, the emulsifier of 1%, the solvent composition of 68% of 9% of 19% by percentage by weight.Its preparation method is identical with embodiment 1.Wherein, preferred as one, the solvent of the present embodiment is mineral oil, and cosolvent is isopropyl alcohol.
Embodiment 6
Containing the vegetable source pesticide aerosol of nimbin, described insect aerosol is the nimbin of 0.8%, neem oil, the surfactant of 0.8%, cosolvent, the emulsifier of 9%, the solvent composition of 76.4% of 10% of 3% by percentage by weight.Its preparation method is identical with embodiment 1.Wherein, preferred as one, the solvent of the present embodiment is mineral oil, and cosolvent is By-120.
Embodiment 7
Containing the vegetable source pesticide aerosol of nimbin, described insect aerosol is the nimbin of 2.5%, neem oil, the surfactant of 0.1%, cosolvent, the emulsifier of 2%, the solvent composition of 66.9% of 9.5% of 19% by percentage by weight.Its preparation method is identical with embodiment 1.Wherein, preferred as one, the solvent of the present embodiment is turpentine-based vegetable oil, and cosolvent is isopropyl alcohol.
What deserves to be explained is, neem oil has good protective effect to nimbin, after being prepared, has good food refusal and repellent effect to insect by preparation.In addition, due to nimbin complicated component, the synergy of itself and neem oil is various to the insect mode of action, and insect not easily develops immunity to drugs.
According to above-described embodiment, just the present invention can be realized well.What deserves to be explained is; under prerequisite based on above-mentioned design, for solving same technical problem, even if some making on the invention are without substantial change or polishing; the essence of the technical scheme adopted is still the same with the present invention, therefore it also should in protection scope of the present invention.

Claims (10)

1., containing a vegetable source pesticide aerosol for nimbin, it is characterized in that, described insect aerosol is made up of the component of following weight percents:
Nimbin 0.1 ~ 3%
Neem oil 1 ~ 20%
Surfactant 0.1 ~ 3%
Cosolvent 8 ~ 15%
Emulsifier 1 ~ 10%;
Finally, with solvent polishing to 100%.
2. a kind of vegetable source pesticide aerosol containing nimbin according to claim 1, it is characterized in that, described insect aerosol is the nimbin of 0.3%, neem oil, the surfactant of 0.2%, cosolvent, the emulsifier of 3%, the solvent composition of 83.5% of 8% of 5% by percentage by weight.
3. a kind of vegetable source pesticide aerosol containing nimbin according to claim 1, it is characterized in that, described insect aerosol is the nimbin of 0.1%, neem oil, the surfactant of 0.2%, cosolvent, the emulsifier of 5%, the solvent composition of 76.7% of 10% of 8% by percentage by weight.
4. a kind of vegetable source pesticide aerosol containing nimbin according to claim 1, it is characterized in that, described insect aerosol is the nimbin of 1%, neem oil, the surfactant of 1%, cosolvent, the emulsifier of 7%, the solvent composition of 67% of 12% of 12% by percentage by weight.
5. a kind of vegetable source pesticide aerosol containing nimbin according to claim 1, it is characterized in that, described insect aerosol is the nimbin of 2%, neem oil, the surfactant of 2%, cosolvent, the emulsifier of 4%, the solvent composition of 64% of 13% of 15% by percentage by weight.
6. a kind of vegetable source pesticide aerosol containing nimbin according to claim 1, it is characterized in that, described insect aerosol is the nimbin of 1.5%, neem oil, the surfactant of 1.5%, cosolvent, the emulsifier of 1%, the solvent composition of 68% of 9% of 19% by percentage by weight.
7. a kind of vegetable source pesticide aerosol containing nimbin according to claim 1, it is characterized in that, described insect aerosol is the nimbin of 0.8%, neem oil, the surfactant of 0.8%, cosolvent, the emulsifier of 9%, the solvent composition of 76.4% of 10% of 3% by percentage by weight.
8. a kind of vegetable source pesticide aerosol containing nimbin according to any one of claim 1 ~ 7, it is characterized in that, described solvent is eucalyptus oil, mineral oil or turpentine-based vegetable oil.
9. the preparation method of a kind of vegetable source pesticide aerosol containing nimbin described in any one of claim 1 ~ 8, is characterized in that, comprise the following steps:
(1) nimbin and neem oil are dissolved in cosolvent;
(2) add surfactant, emulsifier, solvent, be then stirred well to evenly, obtain aerosol liquid.
10. the preparation method of a kind of vegetable source pesticide aerosol containing nimbin according to claim 9, is characterized in that, also comprise and being loaded in aerosol container by aerosol liquid, and be pressed into propellant under elevated pressure conditions, obtain aerosol products; Wherein be pressed into the temperature of propellant process lower than 54 DEG C.
CN201410811197.7A 2014-12-19 2014-12-19 A kind of vegetable source pesticide aerosol containing nimbin and preparation method thereof Active CN104542729B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410811197.7A CN104542729B (en) 2014-12-19 2014-12-19 A kind of vegetable source pesticide aerosol containing nimbin and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410811197.7A CN104542729B (en) 2014-12-19 2014-12-19 A kind of vegetable source pesticide aerosol containing nimbin and preparation method thereof

Publications (2)

Publication Number Publication Date
CN104542729A true CN104542729A (en) 2015-04-29
CN104542729B CN104542729B (en) 2017-09-26

Family

ID=53060660

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201410811197.7A Active CN104542729B (en) 2014-12-19 2014-12-19 A kind of vegetable source pesticide aerosol containing nimbin and preparation method thereof

Country Status (1)

Country Link
CN (1) CN104542729B (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105145663A (en) * 2015-10-08 2015-12-16 广西南宁益土生物科技有限责任公司 Botanical pesticide composition containing azadirachtin and eucalyptus oil
CN105284917A (en) * 2015-10-08 2016-02-03 广西南宁益土生物科技有限责任公司 Plant source pesticide composition containing azadirachtin and clove oil
CN112369412A (en) * 2020-10-27 2021-02-19 广州至简新材料有限公司 Special plant essential oil fly-expelling spray for dairy cows and preparation method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1701663A (en) * 2005-06-24 2005-11-30 福建省泉州德盛农药有限公司 Pesticide auxiliary agent
CN101703077A (en) * 2009-09-22 2010-05-12 成都绿金高新技术股份有限公司 Nimbin film-spreading oil solution

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1701663A (en) * 2005-06-24 2005-11-30 福建省泉州德盛农药有限公司 Pesticide auxiliary agent
CN101703077A (en) * 2009-09-22 2010-05-12 成都绿金高新技术股份有限公司 Nimbin film-spreading oil solution

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105145663A (en) * 2015-10-08 2015-12-16 广西南宁益土生物科技有限责任公司 Botanical pesticide composition containing azadirachtin and eucalyptus oil
CN105284917A (en) * 2015-10-08 2016-02-03 广西南宁益土生物科技有限责任公司 Plant source pesticide composition containing azadirachtin and clove oil
CN105284917B (en) * 2015-10-08 2018-04-24 广西南宁益土生物科技有限责任公司 A kind of plant pesticide composition containing nimbin and caryophyllus oil
CN105145663B (en) * 2015-10-08 2018-10-30 李冬云 A kind of plant pesticide composition containing nimbin and eucalyptus oil
CN112369412A (en) * 2020-10-27 2021-02-19 广州至简新材料有限公司 Special plant essential oil fly-expelling spray for dairy cows and preparation method thereof

Also Published As

Publication number Publication date
CN104542729B (en) 2017-09-26

Similar Documents

Publication Publication Date Title
CN103141526B (en) Botanical insecticide aerosol containing natural pyrethrin and plant essential oil and method
CN107996622B (en) Mosquito repellent containing plant essential oil
US7947311B2 (en) Insect repellent concentrate formulation
WO2015043986A1 (en) Pesticide based on natural extracts
JP2018530602A (en) Pyrethrin-rich insecticide
CN104542729A (en) Azadirachtin-containing botanical insect aerosol and preparation method thereof
JP2011251922A (en) Spray agent for small fly control
CN110384113A (en) A kind of prevention and treatment mosquitos and flies insecticide and its preparation method and application
CN108419810A (en) A kind of natural plant composition compound bio insect aerosol
CN110537555A (en) Preparation of mosquito repellent liquid with bactericidal effect based on natural plant extract
CN102246827B (en) Compound pesticide
CN104757025B (en) A kind of wide spectrum expelling worm plant and agricultural chemicals product
CN104522000B (en) A kind of miticide composition containing cyflumetofen and ivermectin
JP2005520842A (en) A herbal synergistic formulation effective against mosquito larvae and its use in controlling malaria vectors
CN104206405A (en) Pesticide and method for preventing and controlling evergestis extimalis scopoli
CN104621195A (en) Environment-friendly mosquito repellent
CN103444731A (en) Cnidium lactone plant source pesticidal missible oil
CN101027987B (en) Active insecticide
KR101915411B1 (en) Herbicide compositions for controlling pests of horticultural products comprising rare-earth elements as active ingredients
CN107865005A (en) A kind of plant source sterilization pesticide
CN108402061B (en) Biopesticide composition for preventing and treating tea geometrid
CN104938530A (en) Botanical electric warming mosquito incense mat synergist and electric warming mosquito incense mat
CN103918705A (en) Pesticidal composition containing spirotetramat and lambda-cyhalothrin and application thereof
CN109452269A (en) Avermectin emulsion formulations and preparation method and application
CN107251913A (en) A kind of microbial pesticide

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant