CN104542729A - Azadirachtin-containing botanical insect aerosol and preparation method thereof - Google Patents
Azadirachtin-containing botanical insect aerosol and preparation method thereof Download PDFInfo
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- CN104542729A CN104542729A CN201410811197.7A CN201410811197A CN104542729A CN 104542729 A CN104542729 A CN 104542729A CN 201410811197 A CN201410811197 A CN 201410811197A CN 104542729 A CN104542729 A CN 104542729A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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Abstract
The invention discloses azadirachtin-containing botanical insect aerosol and a preparation method thereof and aims at solving the problem that the effect of the existing insect aerosol is not ideal. The azadirachtin-containing botanical insect aerosol comprises the following components in percentage by weight: 0.1-3% of azadirachtin, 1-20% of neem oil, 0.1-3% of a surface active agent, 8-15% of a cosolvent, 1-10% of an emulsifying agent and the balance of a solvent. The azadirachtin-containing botanical insect aerosol has the advantages that azadirachtin and neem oil are botanical natural active substances, high efficiency, low toxicity, no residue and safety for a human body are realized, indoor environment is not polluted, the requirement of people for environmental friendliness of a hygienic insecticide is met, and the azadirachtin-containing botanical insect aerosol is applicable to control of health pests in places to live, working places, dining places and the like.
Description
Technical field
The present invention relates to a kind of vegetable source pesticide aerosol containing nimbin and preparation method thereof.
Background technology
Nimbin, as good Plant antifeedant, has good repellent action to multiple sanitary insect pest, and low toxic and environment-friendly, to person poultry safety, has the potentiality being developed as hygienic insecticide simultaneously.Current azadirachtin preparation product is mainly used in above agricultural, does not also have sending out in nimbin hygienic biocide spray to open, belongs to the market vacancy.
Existing plant source sanitary insecticide kind is single: the sanitary insect pest taking mosquito as representative, by harassing, biting, the various ways harm humans life such as parasitic, and can spread disease cause of disease and the epidemic disease such as the plague, typhoid fever, the life security of serious threat people.Hygienic biocide aerosol and owing to being directly applied in human residential environment, contacts time long with human body, therefore higher to its security requirement.For a long time, the control of sanitary insect pest is mainly used to the pyrethroid pesticide of chemosynthesis, although compared with other chemical pesticides, its toxicity is very low, and Long-Time Service still has potential impact to living environment and health.
The plant source sanitary insecticide of current use, mainly based on natural pyrethrum, the feature due to natural pyrethrum is that knocking down property is strong but the lasting period is short, needs regular Reusability, also can affect to indoor environment when indoor use.
Summary of the invention
The object of the present invention is to provide a kind of vegetable source pesticide aerosol containing nimbin and preparation method thereof, solve the problem that existing insect aerosol effect is undesirable.
To achieve these goals, technical scheme of the present invention is as follows:
Containing a vegetable source pesticide aerosol for nimbin, described insect aerosol is made up of the component of following weight percents:
Nimbin 0.1 ~ 3%
Neem oil 1 ~ 20%
Surfactant 0.1 ~ 3%
Cosolvent 8 ~ 15%
Emulsifier 1 ~ 10%;
Finally, with solvent polishing to 100%.
Particularly, described insect aerosol is the nimbin of 0.3%, neem oil, the surfactant of 0.2%, cosolvent, the emulsifier of 3%, the solvent composition of 83.5% of 8% of 5% by percentage by weight.
Particularly, described insect aerosol is the nimbin of 0.1%, neem oil, the surfactant of 0.2%, cosolvent, the emulsifier of 5%, the solvent composition of 76.7% of 10% of 8% by percentage by weight.
Particularly, described insect aerosol is the nimbin of 1%, neem oil, the surfactant of 1%, cosolvent, the emulsifier of 7%, the solvent composition of 67% of 12% of 12% by percentage by weight.
Particularly, described insect aerosol is the nimbin of 2%, neem oil, the surfactant of 2%, cosolvent, the emulsifier of 4%, the solvent composition of 64% of 13% of 15% by percentage by weight.
Particularly, described insect aerosol is the nimbin of 1.5%, neem oil, the surfactant of 1.5%, cosolvent, the emulsifier of 1%, the solvent composition of 68% of 9% of 19% by percentage by weight.
Particularly, described insect aerosol is the nimbin of 0.8%, neem oil, the surfactant of 0.8%, cosolvent, the emulsifier of 9%, the solvent composition of 76.4% of 10% of 3% by percentage by weight.
Preferred as one, described solvent is eucalyptus oil, mineral oil or turpentine-based vegetable oil.Described cosolvent is isopropyl alcohol or By-120.
Containing a preparation method for the vegetable source pesticide aerosol of nimbin, comprise the following steps:
(1) nimbin and neem oil are dissolved in cosolvent;
(2) add surfactant, emulsifier, solvent, be then stirred well to evenly, obtain aerosol liquid;
(3) aerosol liquid is loaded in aerosol container, and be pressed into propellant under elevated pressure conditions, obtain aerosol products; Wherein be pressed into the temperature of propellant process lower than 54 DEG C.
The present invention compared with prior art, has the following advantages and beneficial effect:
The nimbin that the present invention adopts and neem oil all have natural plant active substance, high-efficiency low-toxicity, noresidue, to human-body safety, and do not pollute indoor environment, meet the green of people to hygienic insecticide, the requirement of environmental protection, be applicable to the health pest control in the places such as inhabitation, office, dining; The processing technology of this product is simple simultaneously, is suitable for batch production.
Solvent of the present invention selects vegetable oil solvent, abandons the solvent of traditional arene; Because carry out the hygienic insecticide that uses in indoor and people and animals time of contact is long and for a long time, traditional aromatic hydrocarbon solvent is comparatively large to people and animals' harm, is not suitable for using in indoor.This formulation product adopts the vegetable oil solvent coming from plant, and low toxic and environment-friendly, and fragrant odour, meet the demand of hygienic insecticide.
Embodiment
Below in conjunction with embodiment, the invention will be further described, and embodiments of the present invention include but not limited to the following example.
Embodiment 1
Containing the vegetable source pesticide aerosol of nimbin, described insect aerosol is the nimbin of 0.3%, neem oil, the surfactant of 0.2%, cosolvent, the emulsifier of 3%, the solvent composition of 83.5% of 8% of 5% by percentage by weight.Wherein, preferred as one, the solvent of the present embodiment is eucalyptus oil, and cosolvent is isopropyl alcohol.
Its preparation method is as follows:
(1) nimbin of above-mentioned percentage by weight and neem oil are dissolved in cosolvent;
(2) add surfactant, emulsifier, solvent, be then stirred well to evenly, obtain aerosol liquid;
(3) aerosol liquid is loaded in aerosol container, and be pressed into propellant under elevated pressure conditions, obtain aerosol products; Wherein be pressed into the temperature of propellant process lower than 54 DEG C.
What deserves to be explained is, because nimbin is comparatively responsive to temperature, so need the impact considering temperature when preparing this product, when more than 54 DEG C, nimbin is very easily degraded, so the pressure needing control to be pressed in propellant process of press in and temperature are on the impact of stability of azadirachtin.So propellant process of press in temperature of the present invention controls below 54 DEG C.
The test performance that table 1 is the embodiment of the present invention 1 products made thereby and domestic be up to the standard comparing at present.
Table 1
As can be seen from Table 1, the performance test data of product of the present invention is all better than domestic existing level.
Embodiment 2
Containing the vegetable source pesticide aerosol of nimbin, described insect aerosol is the nimbin of 0.1%, neem oil, the surfactant of 0.2%, cosolvent, the emulsifier of 5%, the solvent composition of 76.7% of 10% of 8% by percentage by weight.Wherein, preferred as one, the solvent of the present embodiment is eucalyptus oil, and cosolvent is By-120.
Its preparation method is as follows:
(1) nimbin of above-mentioned percentage by weight and neem oil are dissolved in cosolvent;
(2) add surfactant, emulsifier, solvent, be then stirred well to evenly, obtain aerosol liquid;
(3) aerosol liquid is loaded in aerosol container, and be pressed into propellant under elevated pressure conditions, obtain aerosol products; Wherein be pressed into the temperature of propellant process lower than 54 DEG C.
Embodiment 3
Containing the vegetable source pesticide aerosol of nimbin, described insect aerosol is the nimbin of 1%, neem oil, the surfactant of 1%, cosolvent, the emulsifier of 7%, the solvent composition of 67% of 12% of 12% by percentage by weight.Wherein, preferred as one, the solvent of the present embodiment is turpentine-based vegetable oil, and cosolvent is isopropyl alcohol.
Its preparation method is as follows:
(1) nimbin of above-mentioned percentage by weight and neem oil are dissolved in cosolvent;
(2) add surfactant, emulsifier, solvent, be then stirred well to evenly, obtain aerosol liquid;
(3) aerosol liquid is loaded in aerosol container, and be pressed into propellant under elevated pressure conditions, obtain aerosol products; Wherein be pressed into the temperature of propellant process lower than 54 DEG C.
Embodiment 4
Containing the vegetable source pesticide aerosol of nimbin, described insect aerosol is the nimbin of 2%, neem oil, the surfactant of 2%, cosolvent, the emulsifier of 4%, the solvent composition of 64% of 13% of 15% by percentage by weight.Wherein, preferred as one, the solvent of the present embodiment is turpentine-based vegetable oil, and cosolvent is By-120.
Its preparation method is as follows:
(1) nimbin of above-mentioned percentage by weight and neem oil are dissolved in cosolvent;
(2) add surfactant, emulsifier, solvent, be then stirred well to evenly, obtain aerosol liquid;
(3) aerosol liquid is loaded in aerosol container, and be pressed into propellant under elevated pressure conditions, obtain aerosol products; Wherein be pressed into the temperature of propellant process lower than 54 DEG C.
Embodiment 5
Containing the vegetable source pesticide aerosol of nimbin, described insect aerosol is the nimbin of 1.5%, neem oil, the surfactant of 1.5%, cosolvent, the emulsifier of 1%, the solvent composition of 68% of 9% of 19% by percentage by weight.Its preparation method is identical with embodiment 1.Wherein, preferred as one, the solvent of the present embodiment is mineral oil, and cosolvent is isopropyl alcohol.
Embodiment 6
Containing the vegetable source pesticide aerosol of nimbin, described insect aerosol is the nimbin of 0.8%, neem oil, the surfactant of 0.8%, cosolvent, the emulsifier of 9%, the solvent composition of 76.4% of 10% of 3% by percentage by weight.Its preparation method is identical with embodiment 1.Wherein, preferred as one, the solvent of the present embodiment is mineral oil, and cosolvent is By-120.
Embodiment 7
Containing the vegetable source pesticide aerosol of nimbin, described insect aerosol is the nimbin of 2.5%, neem oil, the surfactant of 0.1%, cosolvent, the emulsifier of 2%, the solvent composition of 66.9% of 9.5% of 19% by percentage by weight.Its preparation method is identical with embodiment 1.Wherein, preferred as one, the solvent of the present embodiment is turpentine-based vegetable oil, and cosolvent is isopropyl alcohol.
What deserves to be explained is, neem oil has good protective effect to nimbin, after being prepared, has good food refusal and repellent effect to insect by preparation.In addition, due to nimbin complicated component, the synergy of itself and neem oil is various to the insect mode of action, and insect not easily develops immunity to drugs.
According to above-described embodiment, just the present invention can be realized well.What deserves to be explained is; under prerequisite based on above-mentioned design, for solving same technical problem, even if some making on the invention are without substantial change or polishing; the essence of the technical scheme adopted is still the same with the present invention, therefore it also should in protection scope of the present invention.
Claims (10)
1., containing a vegetable source pesticide aerosol for nimbin, it is characterized in that, described insect aerosol is made up of the component of following weight percents:
Nimbin 0.1 ~ 3%
Neem oil 1 ~ 20%
Surfactant 0.1 ~ 3%
Cosolvent 8 ~ 15%
Emulsifier 1 ~ 10%;
Finally, with solvent polishing to 100%.
2. a kind of vegetable source pesticide aerosol containing nimbin according to claim 1, it is characterized in that, described insect aerosol is the nimbin of 0.3%, neem oil, the surfactant of 0.2%, cosolvent, the emulsifier of 3%, the solvent composition of 83.5% of 8% of 5% by percentage by weight.
3. a kind of vegetable source pesticide aerosol containing nimbin according to claim 1, it is characterized in that, described insect aerosol is the nimbin of 0.1%, neem oil, the surfactant of 0.2%, cosolvent, the emulsifier of 5%, the solvent composition of 76.7% of 10% of 8% by percentage by weight.
4. a kind of vegetable source pesticide aerosol containing nimbin according to claim 1, it is characterized in that, described insect aerosol is the nimbin of 1%, neem oil, the surfactant of 1%, cosolvent, the emulsifier of 7%, the solvent composition of 67% of 12% of 12% by percentage by weight.
5. a kind of vegetable source pesticide aerosol containing nimbin according to claim 1, it is characterized in that, described insect aerosol is the nimbin of 2%, neem oil, the surfactant of 2%, cosolvent, the emulsifier of 4%, the solvent composition of 64% of 13% of 15% by percentage by weight.
6. a kind of vegetable source pesticide aerosol containing nimbin according to claim 1, it is characterized in that, described insect aerosol is the nimbin of 1.5%, neem oil, the surfactant of 1.5%, cosolvent, the emulsifier of 1%, the solvent composition of 68% of 9% of 19% by percentage by weight.
7. a kind of vegetable source pesticide aerosol containing nimbin according to claim 1, it is characterized in that, described insect aerosol is the nimbin of 0.8%, neem oil, the surfactant of 0.8%, cosolvent, the emulsifier of 9%, the solvent composition of 76.4% of 10% of 3% by percentage by weight.
8. a kind of vegetable source pesticide aerosol containing nimbin according to any one of claim 1 ~ 7, it is characterized in that, described solvent is eucalyptus oil, mineral oil or turpentine-based vegetable oil.
9. the preparation method of a kind of vegetable source pesticide aerosol containing nimbin described in any one of claim 1 ~ 8, is characterized in that, comprise the following steps:
(1) nimbin and neem oil are dissolved in cosolvent;
(2) add surfactant, emulsifier, solvent, be then stirred well to evenly, obtain aerosol liquid.
10. the preparation method of a kind of vegetable source pesticide aerosol containing nimbin according to claim 9, is characterized in that, also comprise and being loaded in aerosol container by aerosol liquid, and be pressed into propellant under elevated pressure conditions, obtain aerosol products; Wherein be pressed into the temperature of propellant process lower than 54 DEG C.
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105145663A (en) * | 2015-10-08 | 2015-12-16 | 广西南宁益土生物科技有限责任公司 | Botanical pesticide composition containing azadirachtin and eucalyptus oil |
CN105284917A (en) * | 2015-10-08 | 2016-02-03 | 广西南宁益土生物科技有限责任公司 | Plant source pesticide composition containing azadirachtin and clove oil |
CN112369412A (en) * | 2020-10-27 | 2021-02-19 | 广州至简新材料有限公司 | Special plant essential oil fly-expelling spray for dairy cows and preparation method thereof |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1701663A (en) * | 2005-06-24 | 2005-11-30 | 福建省泉州德盛农药有限公司 | Pesticide auxiliary agent |
CN101703077A (en) * | 2009-09-22 | 2010-05-12 | 成都绿金高新技术股份有限公司 | Nimbin film-spreading oil solution |
-
2014
- 2014-12-19 CN CN201410811197.7A patent/CN104542729B/en active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1701663A (en) * | 2005-06-24 | 2005-11-30 | 福建省泉州德盛农药有限公司 | Pesticide auxiliary agent |
CN101703077A (en) * | 2009-09-22 | 2010-05-12 | 成都绿金高新技术股份有限公司 | Nimbin film-spreading oil solution |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105145663A (en) * | 2015-10-08 | 2015-12-16 | 广西南宁益土生物科技有限责任公司 | Botanical pesticide composition containing azadirachtin and eucalyptus oil |
CN105284917A (en) * | 2015-10-08 | 2016-02-03 | 广西南宁益土生物科技有限责任公司 | Plant source pesticide composition containing azadirachtin and clove oil |
CN105284917B (en) * | 2015-10-08 | 2018-04-24 | 广西南宁益土生物科技有限责任公司 | A kind of plant pesticide composition containing nimbin and caryophyllus oil |
CN105145663B (en) * | 2015-10-08 | 2018-10-30 | 李冬云 | A kind of plant pesticide composition containing nimbin and eucalyptus oil |
CN112369412A (en) * | 2020-10-27 | 2021-02-19 | 广州至简新材料有限公司 | Special plant essential oil fly-expelling spray for dairy cows and preparation method thereof |
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