CN104523460A - Whitening mask and making method thereof - Google Patents
Whitening mask and making method thereof Download PDFInfo
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- CN104523460A CN104523460A CN201410857488.XA CN201410857488A CN104523460A CN 104523460 A CN104523460 A CN 104523460A CN 201410857488 A CN201410857488 A CN 201410857488A CN 104523460 A CN104523460 A CN 104523460A
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Abstract
The invention discloses a whitening mask and a making method of the whitening mask. The whitening mask is made of, by weight, a first part of propylene glycol, xanthan gum and hyaluronic acid; hydrogenated castor oil, essence, a second part of propylene glycol, and glabridin; a first part of deionized water, allantoin, a first part of glycerinum, dipotassium glycyrrhizinate and ethylene diamine tetraacetic acid; a third part of propylene glycol, a second part of glycerinum and GM-BP preservative; arbutin and a second part of deionized water. The whitening mask can improve the whitening and freckle removal effects for the skin, meanwhile, the formula contains no product ingredient like hormone and antibiotic, and therefore the whitening mask has no toxic and side effects.
Description
Technical field
The present invention relates to a kind of facial film, be specially a kind of cleawhite pack and preparation method thereof.
Background technology
Facial film, be a classification in skin care item, principle utilizes the blink covering face, the air that temporarily isolation is extraneous and pollution, improve skin temperature, the pore expansion of skin, promotes sweat gland secretion and metabolism, makes the oxygen content of skin increase, be conducive to the oil substances that skin gets rid of the metabolic product of epidermis cell and accumulation, moisture in facial film infiltrates the horny layer of epidermis, and skin becomes soft, and skin naturally light is flexible.At present, facial film has become the requisite care products of facial-care, but there is the shortcoming of whitening effect difference in cleawhite pack of the prior art, and mostly all with the addition of chemosynthesis agent in formula, not only can not reach the skin effect of anticipation, life-time service can cause some beyond thought injuries to skin.
Summary of the invention
For overcoming the defect of prior art, of the present invention being provides a kind of cleawhite pack, and it can improve the whitening and speckle dispelling effect to skin, not containing any hormone, antibiotic product composition in formula, has no side effect meanwhile.
Another object of the present invention is to the preparation method that a kind of cleawhite pack is provided, there is step simple, easy to operate, the feature that cost is low.
The technical solution adopted in the present invention is as follows for achieving the above object:
A kind of cleawhite pack, it is characterized in that, be prepared from by following raw material by weight percentage:
The Part I propylene glycol of A phase materials: 4-8%, the HANSHENGJIAO of 0.1-0.5%, the hyaluronic acid of 0.1-0.5%;
The castor oil hydrogenated of B phase materials: 0.04-0.08%, the essence of 0.02-0.05%;
The Part II propylene glycol of C phase materials: 4-8%, the glabridin of 0.8-2%;
The Part I deionized water of D phase materials: 50-77%;
The glycyrrhizic acid dipotassium of the allantoin of E phase materials: 0.1-0.2%, the Part I glycerol of 2-5%, 0.1-0.5%, the disodiumedetate (EDTA-2NA) of 0.02-0.1%;
The germall BP antiseptic of the Part III propylene glycol of F phase materials: 4-8%, the Part II glycerol of 4-8%, 0.25-0.5%;
The arbutin of G phase materials: 0.01-0.1%, the Part II deionized water of 5-10%;
The percentage by weight sum of above-mentioned raw materials is 100%.
In the present invention, above-mentioned raw materials all obtains by buying.
Glabridin has the effect that outstanding antiinflammatory, antioxidation and anti-melanin are formed, external glabridin energy check melanin is formed, it has remarkable tyrosinase inhibitory activity, can prevent skin tanning, occurs lines speckle and sunburn, the phospholipid bilayer tunic of glabridin liposome especially of the present invention is similar to biomembrane, easy fusion, promote that functional component is to biomembranous penetrance, make functional component across skin barrier and biomembrane transport efficacy higher, there is positive role improving in its skin-whitening and speckle eliminating effect and other auxiliary effect etc.
Pharmacological action: glabridin is one of Main Flavonoids constituents in Glycyrrhiza glabra L..It demonstrates very strong free radical resisting Oxidation in Cytochrome P450/NADPH oxidative system, the free radical that can obviously suppress to produce in body intracellular metabolic process, with from the biomacromolecule (low density lipoprotein, LDL LDL, DNA) to oxidation-sensitive and cell wall etc. by Free radicals injury.Thus some pathological change relevant with free-radical oxidation can be prevented and treated, and as atherosclerosis, cell ageing etc.
The main mechanism of glabridin check melanin is as follows:
1, the generation of inhibit activities oxygen;
2, restraint of tyrosinase: human tyrosinase enzyme is a kind of indispensable enzyme, and it can produce melanin regularly, makes skin or eyes become black from brown.We know that Dermal exposure can cause some reactions (as occurred inflammation) under ultraviolet light, and the active oxygen destroys that the immobilized artificial membrane due to skin histology is produced by ultraviolet induction, the change on this histology just shows as and occurs erythema and pigmentation.Active oxygen is a kind of material that can cause cutaneous pigmentation, therefore suppresses it to generate the generation of just energy check melanin.
3, antiinflammatory action: the anti-inflammatory activity demonstrating glabridin by experiment, irradiates ultraviolet to Cavia porcellus and causes pigmentation, then use 0.5% glabridin solution to smear, and finding that glabridin alleviates stimulates by ultraviolet the scytitis caused.The erythema on skin is represented by a value.By record pre-irradiation, irradiate rear, to use glabridin a value (colorimeter reading), the degree that inflammation alleviates can be calculated.Research worker suppresses the activity of Cycloxygenase to be studied to glabridin.Cycloxygenase is enzyme arachidonic acid being converted into prostaglandin, and prostaglandin pro-inflammatory cytokine just.As compared to matched group (using existing cox-2 inhibitors, indomethacin), glabridin just can reach the effect suppressing Cycloxygenase.Credible is that glabridin affects arachidonic generation by suppressing Cycloxygenase, thus reduces inflammation.
4, antioxidation: glabridin has antioxidation, and can also whitening (formation of check melanin) and antiinflammatory.There is bibliographical information Radix Glycyrrhizae to can be used for reducing the 17-hydroxy-11-dehydrocorticosterone of infectious dermatosis, the effect of steroid can be strengthened.
Arbutin has another name called Arbutin, in white, needle-shaped crystals or powder.Extract the leaf from Folium Vaccinii vitis-idaeae, by suppressing the activity of tryrosinase in body, melanic generation can be stoped, thus reduce Skin pigmentation, dispelling stain and freckle, also have the effect of sterilization, antiinflammatory simultaneously.
The dissacharide units hyaluronic acid (Hyaluronan) of D-Glucose aldehydic acid and N-acetyl-glucosamine composition, also known as alduronic acid, hyaluronic acid, the large-scale polysaccharide that basic structure is made up of two dissacharide units D-Glucose aldehydic acid and N-acetyl-glucosamine.Different from other mucopolysaccharide, it is sulfur-bearing not.Its hyalomitome molecular energy carries the moisture of more than 500 times, after hyaluronic acid (hyaluronic acid) HA acts on the conditioning of skin inside, can automatically regulate in different environments, all the time moisture of skin is maintained at 25-30%, keep the moistening, salubrious of skin, make skin more high resilience, play the effect of crease-resistant wrinkle resistant, delaying human body skin aging, looks improving and the skin nourishing.Hyaluronic acid is wherein a kind of composition of human body skin corium, possesses the ability keeping moisture content, deal is more up to 100 times of itself weight, use the skin care products containing hyaluronic acid HA, the dry skin with having there is wrinkle can be improved, make it recover original smooth and elasticity, therefore, hyaluronic acid is the most ideal product improving dry and aged skin.Hyaluronic acid (hyaluronic acid) HA can also improve skin growth condition, and for the synthesis of dermal collagen and elastic fiber provides superior external environment condition, the supply of reinforced nutrition matter, plays the effect of skin-protecting face nursing.Research shows, hyaluronic acid HA can stop the generation of some enzymes in cell, reduce the formation of free radical, destroy cellularity preventing free radical, produce lipid peroxidation and cause the important roles such as senility of humanbody: low-molecular-weight hyaluronic acid has antiinflammatory, suppresses pathogenic bacteria to produce, keeps the effect that skin is bright and clean; For cell proliferation and differentiation provide suitable place, direct Promote cell's growth, differentiation, reconstruction and reparation etc.Hyaluronic acid can help skin to draw a large amount of moisture, and skin has had moisture, naturally just can keep elasticity and softness.Before soon, we can only be that skin supplements hyaluronic acid by medical injection means, class medical science skin care item then can using a small amount of hyaluronic acid as whitening agent, 1,000,000 molecular weight hyaluronic acid compression packings are acted on skin, just can absorb the water being about equivalent to own wt 1000 times, epidermis cell is made to fill once again, smooth out wrinkles.Repair and water conservation, can moment deep layer whitening, increase skin elasticity and tension force, help and recover the normal oil-water balance of skin, improve dry and lax skin.Hyaluronic acid is also the important composition of one in skin, has the function that epidermal tissue repairs.When skin histology is exposed under UVB ray, skin can be tanned severely, inflammation, and dermal tissue can stop producing hyaluronic acid, accelerates hyaluronic fading rate simultaneously.In the connective tissue that hyaluronic acid is present in human body in a large number and skin corium, have powerful water absorbing capacity and whitening function, can also strengthen the long water holding capacity of skin, elastic fibers and collagen protein can be helped to be in and be full of in the environment of moisture, what allow skin show is more flexible.
A preparation method for cleawhite pack, its concrete steps are as follows:
1) take raw material respectively according to formulation ratio, then prepare A phase prefabricated solution, B phase prefabricated solution, C phase prefabricated solution respectively;
A phase prefabricated solution: the HANSHENGJIAO in A phase materials, hyaluronic acid are added in Part I propylene glycol, stirs, for subsequent use;
B phase prefabricated solution: the essence in B phase materials is added in castor oil hydrogenated, fully stirs, until mix completely, for subsequent use;
C phase prefabricated solution: glabridin is dissolved completely with the Part II propylene glycol in C phase materials, stand-by;
2) the Part I deionized water of D phase materials is added in aqueous phase pot, open and stir, add A phase prefabricated solution, be warming up to 80 ~ 85 DEG C, be incubated after 20 minutes, add E phase materials, stir;
3) will through step 2) in material suction emulsifying pot in aqueous phase pot after process, start stirring, controlling mixing speed is 40 revs/min, and mixing time is 2 minutes;
4) start cooling, when temperature is down to 45 DEG C, add B phase prefabricated solution, C phase prefabricated solution, F phase materials, G phase materials respectively, low speed homogenizing, controlling mixing speed is 1400 revs/min, stirs more than 20 minutes, the discharging when temperature is down to below 38 DEG C;
5) leave standstill after discharging, subpackage, packaging, obtains cleawhite pack.
Preferably, step 2) in, keep vacuum-0.06MPa in insulating process.
Preferably, step 4) in, keep vacuum-0.06MPa in temperature-fall period.
Preferably, it is also included in step 5) packaging time, with facial mask cloth and PE bag heat-sealing fill.
Beneficial effect of the present invention is:
Containing bicarbonate ion and 5 kinds of oligo mineral factors in formula of the present invention, effectively promote cell regeneration, remove containing melanic dead skin cells, ascorbic acid can the generation of check melanin.Can for the colour of skin is dark yellow and the thicker dry skin of pore provides sufficient moist supply.The phospholipid bilayer tunic of the glabridin liposome of innovation is similar to biomembrane, easily and biological membrane fusion, promote that functional component is to biomembranous penetrance, make functional component across skin barrier and biomembrane transport efficacy higher, there is positive role improving in its skin-whitening and speckle eliminating effect and other auxiliary effect etc.Formula of the present invention adopts pure natural components, and not containing any hormone, antibiotic product composition, nurses one's health out pale Wu Xia skin.Have no side effect, not irritated, more there is no dependency whitening elite film, be applicable to any skin quality, make effect more thorough, use more relieved.Liposome beauty science and technology, block melanin layer by layer, safe speckle dispelling does not rebound.Beneficial effect is mainly reflected in the following aspects:
1, nourish: carry plant whitening, whitening composition to skin deep layer fast, supplement skin moisture content and nutrient comprehensively;
2, control: control the melanocyte quantity formed, use it no longer to increase diffusion
3, smash: multiple whitening plant component, go deep into skin deep layer, speckle is smashed into " melanin microgranule ";
4, upgrade: accelerate cell turnover, " melanin microgranule " and unnecessary old dead cell excretion are removed;
5, suppress: the colouring matter secretion amount of check melanin blast cell, stops the generation of excessive melanin from source, the metabolism of pigment of regulation of skin restores balance;
6, shiningly to adopt: skin melanin disappears thoroughly, and moisture content, nutrient are sufficient, and pale texture appears from the inner health of skin
7, defend: the free radical that blocking-up can cause skin ageing phenomenon to produce, skin is kept fit pale state for a long time.
Detailed description of the invention
Below in conjunction with concrete embodiment, the present invention is described in further detail.
Embodiment 1-3:
Get following raw material by weight percentage respectively:
A phase materials: Part I propylene glycol, HANSHENGJIAO, hyaluronic acid;
B phase materials: castor oil hydrogenated, essence;
C phase materials: Part II propylene glycol, glabridin;
D phase materials: Part I deionized water;
E phase materials: allantoin, Part I glycerol, glycyrrhizic acid dipotassium, disodiumedetate;
F phase materials: Part III propylene glycol, Part II glycerol, germall BP antiseptic;
G phase materials: arbutin, Part II deionized water.
Concrete proportioning is in table 1.
The proportioning table of table 1 embodiment 1-3
The preparation method of described cleawhite pack, its concrete steps are as follows:
1) take raw material respectively according to formulation ratio, then prepare A phase prefabricated solution, B phase prefabricated solution, C phase prefabricated solution respectively;
A phase prefabricated solution: the HANSHENGJIAO in A phase materials, hyaluronic acid are added in Part I propylene glycol, stirs, for subsequent use;
B phase prefabricated solution: the essence in B phase materials is added in castor oil hydrogenated, fully stirs, until mix completely, for subsequent use;
C phase prefabricated solution: glabridin is dissolved completely with the Part II propylene glycol in C phase materials, stand-by;
2) the Part I deionized water of D phase materials is added in aqueous phase pot, open and stir, add A phase prefabricated solution, be warming up to 80 ~ 85 DEG C, be incubated after 20 minutes, add E phase materials, stir; Vacuum-0.06MPa is kept in insulating process.
3) will through step 2) in material suction emulsifying pot in aqueous phase pot after process, start stirring, controlling mixing speed is 40 revs/min, and mixing time is 2 minutes;
4) start cooling, when temperature is down to 45 DEG C, add B phase prefabricated solution, C phase prefabricated solution, F phase materials, G phase materials respectively, low speed homogenizing, controlling mixing speed is 1400 revs/min, stirs more than 20 minutes, the discharging when temperature is down to below 38 DEG C; Vacuum-0.06MPa is kept in temperature-fall period.
5) leave standstill after discharging, subpackage, during packaging, with facial mask cloth and PE bag heat-sealing fill, obtain cleawhite pack.
Testing example 1: the impact that different materials generates check melanin.
1, reagent and instrument:
RPMI1640, Gibco company; Calf serum (FCS), Hangzhou Ilex purpurea Hassk.[I.chinensis Sims company; Lactic dehydrogenase enzyme reagent kit, company is built up in Nanjing; B16 cell, new drug center during China Medicine University is new;
BBHF-16CO2 incubator, Shanghai power Shengong department; TDL80-2B centrifuge, Anting Scientific Instrument Factory, Shanghai; 96 well culture plates, Corning company; DG5031 enzyme-linked immunosorbent assay instrument, East China Electronics Co., Ltd pipe factory.
2, method of testing:
Select the same generation cell of exponential phase, conventional trypsinization process after-blow breaks into single cell suspension cell counting and is quantitatively inoculated in 96 orifice plates.After 24 hours, abandoning supernatant, adds the culture fluid containing test material shown in following table 1 respectively.At 37 °, the CO of volume fraction 5%
2cultivate under saturated moist condition, control wells adds RPMI1640 culture fluid, cultivates three days, and middle replacing once cultivates liquid.Abandoning supernatant, after conventional trypsinization process, counting cells density, centrifugally obtain cell precipitation, rinse twice with PBS, centrifugal abandoning supernatant, quantitatively add the NAOH liquid of 1N of DMSO containing 10%, 80 ° of water-baths 50 minutes, then measure light absorption value at microplate reader 450nm place.
The suppression ratio (%)=100 (absorbance of the absorbance/matched group of each test material) that melanin generates, concrete outcome is in table 2.
Table 2
| Test material | The suppression ratio (%) that melanin generates |
| Glabridin | 33 |
| Arbutin | 30 |
| Certain branding cosmetic that market is bought | 29.5 |
| Glabridin+arbutin | 40.8 |
As can be seen from Table 2, check melanin generate on, arbutin, glabridin with the use of effect be used alone more excellent than them, there is good complementation and synergism.
Testing example 2: white-skinned face function is tested.
TYR enzyme is prevalent in people and animal and plant body, is requisite key enzyme in melanin synthesis process, and the synthesis of TYR enzyme and the rising of catalysis activity, make B16 cell in body increase, and causes mottle and melanomatous formation.The present invention adopts paper (Ren Bingru, thing chrysanthemum is blue, Deng, measure the impact [J] of 24 Plant Extracts on TYR enzymatic activity. Chinese aesthetic medicine, 2004,1 (3): 287-289) method recorded in is evaluated the inhibitory action of mask composition of the present invention to TYR enzyme, test with TYR enzyme as substrate, the inhibitory action of facial film of the present invention to TYR enzymatic activity is detected by tube assay, finally calculate the suppression ratio to TYR enzyme, concrete outcome refers to table 3:
Table 3: embodiment 1-3 facial film is to the suppression ratio tables of data of TYR enzyme
| Group | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Suppression ratio | 33％ | 37％ | 34％ |
As can be seen from Table 3, in whitening, the effect of the use of cleawhite pack described in embodiment 1-3 is all very excellent, and described in embodiment 2, the result of use of cleawhite pack is best.
Above-mentioned embodiment is only the preferred embodiment of the present invention; can not limit the scope of protection of the invention with this, change and the replacement of any unsubstantiality that those skilled in the art does on basis of the present invention all belong to the present invention's scope required for protection.
Claims (5)
1. a cleawhite pack, is characterized in that, is to be prepared from by following raw material by weight percentage:
The Part I propylene glycol of A phase materials: 4-8%, the HANSHENGJIAO of 0.1-0.5%, the hyaluronic acid of 0.1-0.5%;
The castor oil hydrogenated of B phase materials: 0.04-0.08%, the essence of 0.02-0.05%;
The Part II propylene glycol of C phase materials: 4-8%, the glabridin of 0.8-2%;
The Part I deionized water of D phase materials: 50-77%;
The allantoin of E phase materials: 0.1-0.2%, the Part I glycerol of 2-5%, the glycyrrhizic acid dipotassium of 0.1-0.5%, the disodiumedetate of 0.02-0.1%;
The germall BP antiseptic of the Part III propylene glycol of F phase materials: 4-8%, the Part II glycerol of 4-8%, 0.25-0.5%;
The arbutin of G phase materials: 0.01-0.1%, the Part II deionized water of 5-10%;
The percentage by weight sum of above-mentioned raw materials is 100%.
2. a preparation method for cleawhite pack according to claim 1, is characterized in that, its concrete steps are as follows:
1) take raw material respectively according to formulation ratio, then prepare A phase prefabricated solution, B phase prefabricated solution, C phase prefabricated solution respectively;
A phase prefabricated solution: the HANSHENGJIAO in A phase materials, hyaluronic acid are added in Part I propylene glycol, stirs, for subsequent use;
B phase prefabricated solution: the essence in B phase materials is added in castor oil hydrogenated, fully stirs, until mix completely, for subsequent use;
C phase prefabricated solution: glabridin is dissolved completely with the Part II propylene glycol in C phase materials, stand-by;
2) the Part I deionized water of D phase materials is added in aqueous phase pot, open and stir, add A phase prefabricated solution, be warming up to 80 ~ 85 DEG C, be incubated after 20 minutes, add E phase materials, stir;
3) will through step 2) in material suction emulsifying pot in aqueous phase pot after process, start stirring, controlling mixing speed is 40 revs/min, and mixing time is 2 minutes;
4) start cooling, when temperature is down to 45 DEG C, add B phase prefabricated solution, C phase prefabricated solution, F phase materials, G phase materials respectively, low speed homogenizing, controlling mixing speed is 1400 revs/min, stirs more than 20 minutes, the discharging when temperature is down to below 38 DEG C;
5) leave standstill after discharging, subpackage, packaging, obtains cleawhite pack.
3. the preparation method of cleawhite pack according to claim 2, is characterized in that: step 2) in, keep vacuum to be-0.06MPa in insulating process.
4. the preparation method of cleawhite pack according to claim 2, is characterized in that: step 4) in, keep vacuum to be-0.06MPa in temperature-fall period.
5. the preparation method of cleawhite pack according to claim 2, is characterized in that: it is also included in step 5) packaging time, with facial mask cloth and PE bag heat-sealing fill.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410857488.XA CN104523460A (en) | 2014-12-31 | 2014-12-31 | Whitening mask and making method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410857488.XA CN104523460A (en) | 2014-12-31 | 2014-12-31 | Whitening mask and making method thereof |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005527549A (en) * | 2002-03-28 | 2005-09-15 | コティ ビー．ヴィ． | Cosmetics that whiten the skin |
| CN101590003A (en) * | 2009-06-23 | 2009-12-02 | 广州保税区雅兰国际化妆品有限公司 | A kind of whitening spot-relieving cream cosmetic and preparation method thereof |
| CN102793655A (en) * | 2012-08-10 | 2012-11-28 | 彭再辉 | Regenerating and repairing mask liquid by applying snail mucus extract and preparation method thereof |
-
2014
- 2014-12-31 CN CN201410857488.XA patent/CN104523460A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005527549A (en) * | 2002-03-28 | 2005-09-15 | コティ ビー．ヴィ． | Cosmetics that whiten the skin |
| CN101590003A (en) * | 2009-06-23 | 2009-12-02 | 广州保税区雅兰国际化妆品有限公司 | A kind of whitening spot-relieving cream cosmetic and preparation method thereof |
| CN102793655A (en) * | 2012-08-10 | 2012-11-28 | 彭再辉 | Regenerating and repairing mask liquid by applying snail mucus extract and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 木合布力·阿布力孜等: "甘草中光甘草定的提取和抗氧化活性研究", 《天然产物研究与开发》 * |
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