CN104490658A - Chinese herbal medicine liquid soap and preparation method thereof - Google Patents
Chinese herbal medicine liquid soap and preparation method thereof Download PDFInfo
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- CN104490658A CN104490658A CN201410712852.3A CN201410712852A CN104490658A CN 104490658 A CN104490658 A CN 104490658A CN 201410712852 A CN201410712852 A CN 201410712852A CN 104490658 A CN104490658 A CN 104490658A
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- 239000007788 liquid Substances 0.000 title claims abstract description 94
- 241000411851 herbal medicine Species 0.000 title claims abstract description 78
- 238000002360 preparation method Methods 0.000 title claims abstract description 25
- 239000000344 soap Substances 0.000 title abstract description 10
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 48
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 42
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 27
- 238000001914 filtration Methods 0.000 claims abstract description 20
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 18
- 238000000034 method Methods 0.000 claims abstract description 18
- 241001465754 Metazoa Species 0.000 claims abstract description 16
- 238000002156 mixing Methods 0.000 claims abstract description 13
- 239000002994 raw material Substances 0.000 claims abstract description 11
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 10
- 239000011780 sodium chloride Substances 0.000 claims abstract description 9
- 239000001509 sodium citrate Substances 0.000 claims abstract description 9
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 claims abstract description 9
- 238000002791 soaking Methods 0.000 claims abstract description 4
- 210000003278 egg shell Anatomy 0.000 claims abstract description 3
- 238000001354 calcination Methods 0.000 claims description 32
- 102000002322 Egg Proteins Human genes 0.000 claims description 15
- 108010000912 Egg Proteins Proteins 0.000 claims description 15
- 210000001136 chorion Anatomy 0.000 claims description 15
- 210000004681 ovum Anatomy 0.000 claims description 13
- 238000007654 immersion Methods 0.000 claims description 11
- 239000000706 filtrate Substances 0.000 claims description 9
- 125000000217 alkyl group Chemical group 0.000 claims description 8
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 8
- 241000287828 Gallus gallus Species 0.000 claims description 6
- 235000011201 Ginkgo Nutrition 0.000 claims description 6
- 235000008100 Ginkgo biloba Nutrition 0.000 claims description 6
- 210000000582 semen Anatomy 0.000 claims description 5
- 240000000560 Citrus x paradisi Species 0.000 claims description 4
- 241000272205 Columba livia Species 0.000 claims description 4
- 241000272522 Anas Species 0.000 claims description 3
- 241000270711 Malaclemys terrapin Species 0.000 claims description 2
- 244000194101 Ginkgo biloba Species 0.000 claims 1
- 239000000203 mixture Substances 0.000 abstract description 10
- 241000196324 Embryophyta Species 0.000 abstract description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract description 3
- 150000001875 compounds Chemical class 0.000 abstract description 3
- 239000011734 sodium Substances 0.000 abstract description 3
- 229910052708 sodium Inorganic materials 0.000 abstract description 3
- -1 alkyl glycoside Chemical class 0.000 abstract description 2
- 241000894006 Bacteria Species 0.000 abstract 1
- 241000037740 Coptis chinensis Species 0.000 abstract 1
- 244000179560 Prunella vulgaris Species 0.000 abstract 1
- 244000173853 Sanguisorba officinalis Species 0.000 abstract 1
- 235000008282 Sanguisorba officinalis Nutrition 0.000 abstract 1
- 235000019387 fatty acid methyl ester Nutrition 0.000 abstract 1
- 229930182470 glycoside Natural products 0.000 abstract 1
- 235000008113 selfheal Nutrition 0.000 abstract 1
- 238000004140 cleaning Methods 0.000 description 23
- 230000003115 biocidal effect Effects 0.000 description 16
- 230000000694 effects Effects 0.000 description 16
- 239000000047 product Substances 0.000 description 7
- 230000000844 anti-bacterial effect Effects 0.000 description 6
- 239000003814 drug Substances 0.000 description 6
- 241000218628 Ginkgo Species 0.000 description 5
- 239000004615 ingredient Substances 0.000 description 5
- 238000012360 testing method Methods 0.000 description 5
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- ICUTUKXCWQYESQ-UHFFFAOYSA-N triclocarban Chemical compound C1=CC(Cl)=CC=C1NC(=O)NC1=CC=C(Cl)C(Cl)=C1 ICUTUKXCWQYESQ-UHFFFAOYSA-N 0.000 description 4
- XEFQLINVKFYRCS-UHFFFAOYSA-N Triclosan Chemical compound OC1=CC(Cl)=CC=C1OC1=CC=C(Cl)C=C1Cl XEFQLINVKFYRCS-UHFFFAOYSA-N 0.000 description 3
- 230000033228 biological regulation Effects 0.000 description 3
- 239000003599 detergent Substances 0.000 description 3
- 235000008216 herbs Nutrition 0.000 description 3
- 244000005700 microbiome Species 0.000 description 3
- 230000001954 sterilising effect Effects 0.000 description 3
- 238000004659 sterilization and disinfection Methods 0.000 description 3
- 229960003500 triclosan Drugs 0.000 description 3
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 2
- 239000003242 anti bacterial agent Substances 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 239000002537 cosmetic Substances 0.000 description 2
- 239000006260 foam Substances 0.000 description 2
- 244000000010 microbial pathogen Species 0.000 description 2
- 231100000252 nontoxic Toxicity 0.000 description 2
- 230000003000 nontoxic effect Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229910021653 sulphate ion Inorganic materials 0.000 description 2
- 229960001325 triclocarban Drugs 0.000 description 2
- 244000099147 Ananas comosus Species 0.000 description 1
- 235000007119 Ananas comosus Nutrition 0.000 description 1
- VRGFDBUBESOYSN-UHFFFAOYSA-N C(C)NCCO.N1C(C=CC=C1)=O Chemical compound C(C)NCCO.N1C(C=CC=C1)=O VRGFDBUBESOYSN-UHFFFAOYSA-N 0.000 description 1
- 241001115402 Ebolavirus Species 0.000 description 1
- 241000315672 SARS coronavirus Species 0.000 description 1
- 206010040880 Skin irritation Diseases 0.000 description 1
- 230000000711 cancerogenic effect Effects 0.000 description 1
- 231100000315 carcinogenic Toxicity 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 238000004851 dishwashing Methods 0.000 description 1
- 239000006210 lotion Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 230000029058 respiratory gaseous exchange Effects 0.000 description 1
- 230000036556 skin irritation Effects 0.000 description 1
- 231100000475 skin irritation Toxicity 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 230000002110 toxicologic effect Effects 0.000 description 1
- 231100000027 toxicology Toxicity 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
Abstract
The invention discloses Chinese herbal medicine liquid soap and a preparation method thereof. The preparation method comprises the following steps: a, soaking a calcined mixture in water to obtain a plant ash liquid; b, soaking and decocting Chinese herbal medicines in water/alcohol and filtering to obtain a Chinese herbal medicine compound liquid; and c, mixing the prepared plant ash liquid, the Chinese herbal medicine compound liquid, alkyl glycoside, sodium citrate, sodium chloride, sodium fatty acid methyl ester sulfonate, glycerol, citric acid and water to obtain the Chinese herbal medicine liquid soap, wherein the Chinese herbal medicines are selected from one or more of coptis chinensis, radix sophorae flavescentis, cortex moutan, selfheal, mangnolia officinalis, radix angelicae and sanguisorba officinalis; the calcined mixture is prepared from raw materials selected from one or more of plant fruits/sheels/pericarps, plant stems, leaves and flowers and animal egg shells. The Chinese herbal medicine liquid soap prepared by the method has excellent decontaminating property and bacteria resistance and is mild to skin and harmless. Meanwhile, according to the preparation method, the raw materials are easily available and the cost is low.
Description
Technical field
The present invention relates to handwashing liquid, particularly, relate to a kind of Chinese herbal medicine handwashing liquid and preparation method thereof.
Background technology
The mankind endure pathogenic microorganism in environment to the fullest extent, invade the healthy disaster that the pathogenic microorganism of body and other harmful microorganism bring, the healthy disaster that the outburst as SARS virus in 2003 and Ebola virus in 2014 brings.Microorganism or be the body being entered people by breathing, or be entered by human body skin to recognize body, wherein human body and the maximum body part of extraneous contact are hands and arm, thus cause that hands and arm have a large amount of microorganisms.
Soap mostly was in the past for cleaning and sterilization, or even detergent.Although soap and detergent play effect that is clean, sterilization to a certain extent, have larger stimulation to skin, if life-time service can cause pachylosis, be chapped from the cold and even peel, simultaneously the easy skating of solid such as soap is also unfavorable for holding taking.At present, the clean multiplex cleaning mixture of the exposed body part of human body, cleaning mixture overcomes the defect that soap is easily slided.Cleaning mixture is generally that preparation of raw material forms by surfactant, conditioner and stabilizing agent, its alkalescence more moist human body skin less of fancy soap, and foam type handwashing liquid wherein utilizes the foam that enriches of generation to carry out cleaning skin of human body especially, its consumption few and rinse convenient.
At present, handwashing liquid can be divided into two classes according to its composition: a class adds the cleaning mixture of chemical industry synthetic antibacterial agents, as publication number handwashing liquid disclosed in the patent of CN 102429833B, contains BIT as antibacterial in this handwashing liquid; As publication number sterilizing skin moistening liquid soap disclosed in the patent of CN 101785749B, containing TCC, 1-hydroxy-4-methyl-6-(2 in this handwashing liquid, 4,4-tri-methyl-amyl)-2 (1H)-pyridone-2-ethylaminoethanol salt are as antibacterial; As publication number anti-bacterial hand lotion disclosed in the patent of CN104083294A, contain triclosan in this handwashing liquid as antibacterial.Another kind of interpolation chemical industry synthetic antibacterial agents adds the handwashing liquid of Chinese medicine antibacterial composition simultaneously.As publication number nontoxic handwashing liquid disclosed in the patent of CN 103893044A, containing Efficacious Disinfeitant in this handwashing liquid; As publication number nontoxic handwashing liquid disclosed in the patent of CN 104042501A, containing Sodium Alcohol Ether Sulphate in this handwashing liquid.In above-mentioned disclosed cleaning mixture or containing harmful antibacterial, as 1,2-benzisothiazole-3-ketone, TCC, 1-hydroxy-4-methyl-6-(2,4,4-tri-methyl-amyl)-2 (1H)-pyridone-2-ethylaminoethanol salt, triclosan, triclocarban and KF88, especially there is carcinogenic risk in triclosan and triclocarban etc.; Containing having larger irritating Sodium Alcohol Ether Sulphate to human body skin.
Summary of the invention
The object of this invention is to provide a kind of Chinese herbal medicine handwashing liquid and preparation method thereof, the Chinese herbal medicine handwashing liquid obtained by the method has excellent cleaning effect, antibiotic property and, fanout free region gentle to skin, and the raw material simultaneously in the method is easy to get, with low cost.
To achieve these goals, the invention provides a kind of preparation method of Chinese herbal medicine handwashing liquid, described preparation method comprises:
A, calcining mixt soaked in water obtained vegetation lixivium;
B, Chinese herbal medicine soaked in water after decocts and filters and obtain combined Chinese herb liquid;
C, by the obtained Chinese herbal medicine handwashing liquid of described vegetation lixivium, combined Chinese herb liquid, alkyl polyglucoside, sodium citrate, sodium chloride, methyl sodiosul foaliphatate, glycerol, citric acid and water mixing;
Wherein, described Chinese herbal medicine is selected from one or more in Rhizoma Coptidis, Radix Sophorae Flavescentis, Cortex Moutan, Spica Prunellae, Cortex Magnoliae Officinalis, the Radix Angelicae Dahuricae and Radix Sanguisorbae; The raw material of described calcining mixt comprise in fruit/shell/peel, axis and animal chorion one or more.
Present invention provides a kind of Chinese herbal medicine handwashing liquid, described Chinese herbal medicine handwashing liquid is prepared from by above-mentioned method.
Pass through technique scheme, the present invention by calcining raw materials is comprised fruit/shell/peel, axis/stalk, axis, animal chorion calcining mixt soak in water and form vegetation lixivium, decoct after Chinese medicine and Chinese medicine composition thereof being soaked in water simultaneously and filter and obtain combined Chinese herb liquid; Then by obtained for the mixing of vegetation lixivium, combined Chinese herb liquid, alkyl polyglucoside, sodium citrate, sodium chloride, methyl sodiosul foaliphatate, glycerol, citric acid and water Chinese herbal medicine handwashing liquid.Chinese herbal medicine handwashing liquid provided by the invention utilizes the synergism of each raw material, makes this Chinese herbal medicine handwashing liquid have excellent cleaning effect, antibiotic property and, fanout free region gentle to skin.
Other features and advantages of the present invention are described in detail in detailed description of the invention part subsequently.
Detailed description of the invention
Below the specific embodiment of the present invention is described in detail.Should be understood that, detailed description of the invention described herein, only for instruction and explanation of the present invention, is not limited to the present invention.
The invention provides the preparation method of a kind of Chinese herbal medicine washing hands liquid, described preparation method comprises:
A, calcining mixt soaked in water obtained vegetation lixivium;
B, Chinese herbal medicine soaked in water after decocts and filters and obtain combined Chinese herb liquid;
C, by the obtained Chinese herbal medicine handwashing liquid of described vegetation lixivium, combined Chinese herb liquid, alkyl polyglucoside, sodium citrate, sodium chloride, methyl sodiosul foaliphatate, glycerol, citric acid and water mixing;
Wherein, described Chinese herbal medicine is selected from one or more in Rhizoma Coptidis, Radix Sophorae Flavescentis, Cortex Moutan, Spica Prunellae, Cortex Magnoliae Officinalis, the Radix Angelicae Dahuricae and Radix Sanguisorbae; The raw material of described calcining mixt comprise in fruit/shell/peel, axis, leaf, flower and animal chorion one or more.
In the present invention, described fruit/shell/peel can be the fruit of any one plant, shell or peel, but in order to make the Chinese herbal medicine handwashing liquid obtained, there is more excellent cleaning effect and antibiotic property, preferably, described shell/peel is selected from pomelo peel, Pericarpium Musae or orange peel, Retinervus Luffae Fructus; More preferably, Pericarppium arachidis hypogaeae and pineapple peel.
In the present invention, axis can be the branch of any one plant, but in order to make the Chinese herbal medicine handwashing liquid obtained have more excellent cleaning effect and antibiotic property, preferably, described axis is selected from Semen Ginkgo branch, Ramulus Mori or Ramulus Salicis Babylonicae; More preferably, described branch is branck of Lignum cinnamomi camphorae.
In the present invention, described animal chorion can be any one animal chorion, but in order to make the Chinese herbal medicine handwashing liquid obtained have more excellent cleaning effect and antibiotic property, preferably, described animal chorion is selected from Chinese terrapin egg shell, Ovum Columba livia shell, Ovum crusta Gallus domesticus, Ovum Anas domestica putamina or Ovum-crusta Anseris domestica.
In the present invention, the order by merging in the preparation method of described calcining mixt can be selected in wide scope, can by the obtained calcining mixt of calcining after shell/peel, axis, Retinervus Luffae Fructus, the mixing of animal chorion before step a; Also shell/peel, axis, Retinervus Luffae Fructus, animal chorion can be remixed obtained calcining mixt after calcining respectively.But in order to make the Chinese herbal medicine handwashing liquid obtained have more excellent cleaning effect and antibiotic property, preferably, before step a, calcining after shell/peel, axis, Retinervus Luffae Fructus, the mixing of animal chorion is obtained calcining mixt.
In the preparation method of calcining mixt, the temperature and time of described calcining can be selected in wide scope, but in order to make the Chinese herbal medicine handwashing liquid obtained have more excellent cleaning effect and antibiotic property, preferably, the temperature of described calcining is 100-500 DEG C, and the time of described calcining is 2-6h.
In the preparation method of calcining mixt, the consumption of the raw material of each calcining mixt can be selected in wide scope, but in order to make the Chinese herbal medicine handwashing liquid obtained, there is more excellent cleaning effect and antibiotic property, preferably, relative to the described shell/peel of 3 weight portions, the consumption of described axis is 1-5 weight portion, and the consumption of described Retinervus Luffae Fructus is 1-5 weight portion, and the consumption of described animal chorion is 1-5 weight portion.
In step a provided by the invention, the consumption of described calcining mixt and water can be selected in wide scope, but in order to make the Chinese herbal medicine handwashing liquid obtained, there is more excellent cleaning effect and antibiotic property, preferably, in step a, relative to the described water of 10 weight portions, the consumption of described calcining mixt is 1-5 weight portion.
In step a provided by the invention, the temperature and time of described immersion can be selected in wide scope, but can expand in water fully to make described calcining mixt, preferably, but in order to make the Chinese herbal medicine handwashing liquid obtained, there is more excellent cleaning effect and antibiotic property, the temperature and time of described immersion can be selected in wide region, but in order to make the Chinese herbal medicine handwashing liquid obtained, there is more excellent cleaning effect and antibiotic property, preferably, in step a, the temperature of described immersion is 4-100 DEG C, the time 1-48h of described immersion.
In step b provided by the invention, the temperature and time of described immersion also can you select in wide scope, but in order to make each Chinese herbal medicine can expand completely in water, preferably, the temperature of the described immersion in step b is 4-100 DEG C, and the time of described immersion is 1-120h.
In the described soaking step of step b provided by the invention, the consumption of described each taste Chinese medicine and water can be selected in wide scope, but in order to make the Chinese herbal medicine handwashing liquid obtained, there is more excellent cleaning effect and antibiotic property, preferably, relative to the described water of 10 weight portions, described in each taste, the consumption of Chinese herbal medicine is 0.1-5 weight portion.
In step b provided by the invention, the step of described decoction and filtration can once complete, also can be carry out several times decocting and filtering, can fully enter in water to make the effective ingredient in each middle medicinal herbs, preferably, decoct and filter to collect filtrate after Chinese herbal medicine is soaked in water, then filtering residue is mixed with water, decoct and filter to collect filtrate, back and forth filtering residue is mixed with water with this, decoct and filter repeatedly to collect filtrate, finally the filtrate combination system of gained is obtained Chinese herbal medicine basal liquid.
When step part of described decoction and filtration repeatedly completes, the temperature and time of each decoction can be selected in wide scope, but can fully enter in water to make the effective ingredient in each middle medicinal herbs, preferably, the temperature of described decoction is 70-100 DEG C, and the time of described decoction is 20-40min.
When step part of described decoction and filtration repeatedly completes, the number of times of decoction can be selected in wide scope, but in order to make the effective ingredient in each middle medicinal herbs fully to enter in water, preferably, the number of times of described decoction is 2-3 time.
In the above-mentioned decoction step at filtering residue be mentioned to, the consumption of each filtering residue and water can be selected in wide scope, but in order to make the effective ingredient in filtering residue to be immersed in the water fully, preferably, the weight ratio of described filtering residue and water is 1:5-7.
After obtained Chinese herbal medicine basal liquid, in order to make the concentration of the effective ingredient in combined Chinese herb liquid be improved, preferably, the step described Chinese herbal medicine basal liquid being concentrated obtained combined Chinese herb liquid is also being comprised in stepb.
In the step of inventing the concentrated Chinese herbal medicine basal liquid provided, described concentrated temperature and time also can be selected in wide scope, and preferably, described concentrated temperature is 4-100 DEG C, and the described concentrated time is 3-6h.
In step c provided by the invention, the consumption of each raw material also can be selected in wide scope, but in order to make the Chinese herbal medicine handwashing liquid obtained, there is more excellent cleaning effect and antibiotic property, preferably, with the gross weight of obtained Chinese herbal medicine handwashing liquid for benchmark, the consumption of described vegetation lixivium is 1-40 % by weight, the consumption of described combined Chinese herb liquid is 1-15 % by weight, the consumption of described alkyl polyglucoside is 2-30 % by weight, the consumption of described sodium citrate is 1-25 % by weight, the consumption of described sodium chloride is 0.1-15 % by weight, the consumption of described methyl sodiosul foaliphatate is 0.1-10 % by weight, the consumption of described citric acid is 0.1-10 % by weight, all the other are water.
In step c provided by the invention, the temperature and time of described mixing can be selected in wide scope, and preferably, the temperature of described mixing is 4-100 DEG C, and the time of described mixing is 1-72h.
In the present invention, in order to make the Chinese herbal medicine handwashing liquid obtained have more excellent moisture retention, preferably, in step c, described Chinese herbal medicine handwashing liquid also contains wetting agent as glycerol.
Under Chinese herbal medicine handwashing liquid contains sweet oil condition, the consumption of described glycerol can be selected in wide scope, but in order to the cleaning effect that improves Chinese herbal medicine handwashing liquid further and antibiotic property, preferably, in step c, with the gross weight of obtained Chinese herbal medicine handwashing liquid for benchmark, the consumption of glycerol is 0.1-25 % by weight.
Present invention provides a kind of Chinese herbal medicine handwashing liquid, described Chinese herbal medicine handwashing liquid is prepared from by above-mentioned method.
Present invention also offers a kind of according to the application of said herbal medicine handwashing liquid in cleaning human hands.
Below will be described the present invention by embodiment.In following examples, Rhizoma Coptidis, Radix Sophorae Flavescentis, Cortex Moutan, Spica Prunellae, Cortex Magnoliae Officinalis, the Radix Angelicae Dahuricae and Radix Sanguisorbae are the commercially available product in the large pharmacy of Wuhu City citizen, the commercially available product that the commercially available product that the commercially available product that the commercially available product that alkyl polyglucoside is Chizhou Haifeng Pharmaceutical Co., Ltd., sodium citrate are Tianjin Chemical Co., Ltd.'s all generations, sodium chloride are Wuxi City prospect chemical reagent company limited, methyl sodiosul foaliphatate are Linyi City Lanshan District Lv Sen Chemical Co., Ltd., glycerol is the commercially available product of Shanghai biological engineering company limited, and citric acid is the commercially available product of Chinese Bangbu chemical reagent factory.
Embodiment 1
Chinese medicine compositional liquor (mass percent is 1%), vegetation lixivium (mass percent is 10%), alkyl polyglucoside (mass percent is 5%), sodium citrate (mass percent is 4%), sodium chloride (mass percent is 1%), methyl sodiosul foaliphatate (mass percent is 1%), citric acid (mass percent is 0.2%) and deionized water are mixed 2h at 30 DEG C and obtains Chinese herbal medicine handwashing liquid A1.
Wherein, vegetation lixivium first Pericarpium Musae, Retinervus Luffae Fructus, Semen Ginkgo branch and Ovum crusta Gallus domesticus is mixed by the mass ratio of 3:2:2:2 and calcine 2h to form calcining mixt, filters and obtain after then calcining mixt and water being soaked 24h by the mass ratio of 1:10 at 30 DEG C; Combined Chinese herb liquid is soaked 12 hours at 30 DEG C by Rhizoma Coptidis, Spica Prunellae, Cortex Magnoliae Officinalis and the water mass ratio according to 1:1:1:10, then at 80 DEG C, 20min is decocted and collecting by filtration filter, repeat twice and filtering residue is decocted 20min and collecting by filtration filter at 80 DEG C, finally all filtrate merged and at 60 DEG C, concentrate 3h and obtain, wherein filtering residue and the mass ratio for the water decocting filtering residue are 1:6.
Embodiment 2
Obtain Chinese herbal medicine handwashing liquid A2 according to the method for embodiment 1, difference be Rhizoma Coptidis is changed to Cortex Moutan, Spica Prunellae is changed to the Radix Angelicae Dahuricae, Cortex Magnoliae Officinalis is changed to Radix Sanguisorbae; Semen Ginkgo branch is changed to branck of Lignum cinnamomi camphorae, and Ovum crusta Gallus domesticus is changed to Ovum Anas domestica putamina.
Embodiment 3
Obtain Chinese herbal medicine handwashing liquid A3 according to the method for embodiment 1, difference is containing glycerol, and the mass fraction of glycerol in Chinese herbal medicine handwashing liquid A3 is 25%.
Embodiment 4
Obtain Chinese herbal medicine handwashing liquid A4 according to the method for embodiment 1, difference is that Pericarpium Musae is changed to pomelo peel, and Semen Ginkgo branch is changed to branck of Lignum cinnamomi camphorae, and Ovum crusta Gallus domesticus is changed to Ovum Columba livia shell; This Chinese herbal medicine handwashing liquid is also containing glycerol, and the mass fraction of glycerol in Chinese herbal medicine handwashing liquid A4 is 0.8%.
Embodiment 5
Obtain Chinese herbal medicine handwashing liquid A5 according to the method for embodiment 1, difference is that Pericarpium Musae is changed to pomelo peel, and Semen Ginkgo branch is changed to branck of Lignum cinnamomi camphorae, and Ovum crusta Gallus domesticus is changed to Ovum Columba livia shell; This Chinese herbal medicine handwashing liquid is also containing glycerol, and the mass fraction of glycerol in Chinese herbal medicine handwashing liquid A5 is 15%.
Comparative example 1
Carry out obtained Chinese herbal medicine handwashing liquid B1 according to the method for embodiment 1, difference is: not containing vegetation lixivium.
Comparative example 2
Carry out obtained Chinese herbal medicine handwashing liquid B2 according to the method for embodiment 2, difference is: not containing Chinese medicine compositional liquor.
Test example 1
In this test example, the method that soil removal efficiency parameter is specified by " manual dishwashing detergent " (GB 9985-2000) " mensuration of detergency " records; Biocidal property parameter sends out regulation in [2002] No. 229 " disinfection technology standard " (version in 2002) method by defending method prison records; Toxicological test parameter sends out regulation in [2007] No. 1 " cosmetics health specification " (version in 2007) method by defending supervision records; Skin irritation parameter sends out regulation in [2007] No. 1 " cosmetics health specification " (version in 2007) method by defending supervision records.Concrete testing result is in table 1.
Table 1
From above-described embodiment and test example, Chinese herbal medicine handwashing liquid provided by the invention has excellent cleaning effect, antibiotic property and, fanout free region gentle to skin.
More than describe the preferred embodiment of the present invention in detail; but the present invention is not limited to the detail in above-mentioned embodiment, within the scope of technical conceive of the present invention; can carry out multiple simple variant to technical scheme of the present invention, these simple variant all belong to protection scope of the present invention.
It should be noted that in addition, each concrete technical characteristic described in above-mentioned detailed description of the invention, in reconcilable situation, can be combined by any suitable mode, in order to avoid unnecessary repetition, the present invention illustrates no longer separately to various possible compound mode.
In addition, also can carry out combination in any between various different embodiment of the present invention, as long as it is without prejudice to thought of the present invention, it should be considered as content disclosed in this invention equally.
Claims (9)
1. a preparation method for Chinese herbal medicine handwashing liquid, is characterized in that, described preparation method comprises:
A, calcining mixt soaked in water obtained vegetation lixivium;
B, Chinese herbal medicine soaked in water after decocts and filters and obtain combined Chinese herb liquid;
C, by the obtained Chinese herbal medicine handwashing liquid of described vegetation lixivium, combined Chinese herb liquid, alkyl polyglucoside, sodium citrate, sodium chloride, methyl sodiosul foaliphatate, citric acid and water mixing;
Wherein, described Chinese herbal medicine is selected from one or more in Rhizoma Coptidis, Radix Sophorae Flavescentis, Cortex Moutan, Spica Prunellae, Cortex Magnoliae Officinalis, the Radix Angelicae Dahuricae and Radix Sanguisorbae; The raw material of described calcining mixt comprise in fruit/shell/peel, axis and animal chorion one or more.
2. preparation method according to claim 1, wherein, described fruit/shell/peel is selected from Semen arachidis hypogaeae shell, pomelo peel, Retinervus Luffae Fructus, Pericarpium Musae or Fructus Citri tangerinae peel;
Preferably, described axis is selected from branck of Lignum cinnamomi camphorae, Ramulus Mori, Semen Ginkgo branch or Ramulus Salicis Babylonicae;
More preferably, described animal chorion is selected from Chinese terrapin egg shell, Ovum Columba livia shell, Ovum crusta Gallus domesticus, Ovum Anas domestica putamina or Ovum-crusta Anseris domestica.
3. preparation method according to claim 2, wherein, described preparation method also comprises: by the obtained calcining mixt of calcining after fruit/shell/peel, axis, Retinervus Luffae Fructus, the mixing of animal chorion before step a; Or, fruit/shell/peel, axis, leaf, flower, animal chorion are remixed obtained calcining mixt after calcining respectively;
Preferably, the time of described calcining is 2-6h;
More preferably, relative to the described shell/peel of 3 weight portions, the consumption of described axis is 1-5 weight portion, and the consumption of described Retinervus Luffae Fructus is 1-5 weight portion, and the consumption of described animal chorion is 1-5 weight portion;
Further preferably, in step a, relative to the described water of 10 weight portions, the consumption of described calcining mixt is 1-5 weight portion;
Still more preferably, in step a, the temperature of described immersion is 4-100 DEG C, and the time of described immersion is 1-48h.
4. preparation method according to claim 3, wherein, in stepb, the temperature of described immersion is 4-100 DEG C, and the time of described immersion is 1-120h;
Preferably, in the described soaking step of step b, relative to the described water of 10 weight portions, described in each taste, the consumption of Chinese herbal medicine is 0.1-5 weight portion.
5. preparation method according to claim 4, wherein, in stepb, decoct and filter to collect filtrate after Chinese herbal medicine is soaked in water, then filtering residue is mixed with water, decoct and filter to collect filtrate, back and forth filtering residue is mixed with water with this, decoct and filter to collect filtrate, finally the filtrate combination system of gained is obtained Chinese herbal medicine basal liquid;
Preferably, the temperature of described decoction is 70-100 DEG C, and described decocting time is 20-40min;
More preferably, described decoction number of times is 2-3 time;
Further preferably, in the decoction step of filtering residue, relative to the described filtering residue of 1 weight portion, the consumption of described water is 5-7 weight portion.
6. preparation method according to claim 5, wherein, also comprises the step described Chinese herbal medicine basal liquid being concentrated obtained combined Chinese herb liquid in stepb;
Preferably, described concentrated temperature is 4-100 DEG C, and the described concentrated time is 3-6h.
7. preparation method according to claim 6, wherein, in step c, with the gross weight of obtained Chinese herbal medicine handwashing liquid for benchmark, the consumption of described vegetation lixivium is 1-40 % by weight, the consumption of described combined Chinese herb liquid is 1-15 % by weight, the consumption of described alkyl polyglucoside is 2-30 % by weight, the consumption of described sodium citrate is 1-25 % by weight, the consumption of described sodium chloride is 0.1-15 % by weight, the consumption of described methyl sodiosul foaliphatate is 0.1-10 % by weight, and the consumption of described citric acid is 0.1-10 % by weight, and all the other are water;
Preferably, in step c, the temperature of described mixing is 30-90 DEG C, and the time of described mixing is 1-10h.
8. the preparation method according to any one in claim 1-7, wherein, in step c, described Chinese herbal medicine handwashing liquid is also containing glycerol;
Preferably, in step c, with the gross weight of obtained Chinese herbal medicine handwashing liquid for benchmark, the consumption of glycerol is 0.1-25 % by weight.
9. a Chinese herbal medicine handwashing liquid, is characterized in that, described Chinese herbal medicine handwashing liquid is prepared from by the method described in any one in claim 1-8.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106691950A (en) * | 2017-02-27 | 2017-05-24 | 陕西理工学院 | Selfheal-containing Chinese herbal hand sanitizer and preparation method |
| CN107854350A (en) * | 2017-10-20 | 2018-03-30 | 芜湖皮皮鲁网络技术有限公司 | Main broadcaster's Environmentally-friehand hand sanitizer and preparation method thereof |
| CN107898675A (en) * | 2017-12-12 | 2018-04-13 | 佛山早稻田科技服务有限公司 | A kind of Environmentally-friehand hand sanitizer |
| CN108451843A (en) * | 2018-02-12 | 2018-08-28 | 华南理工大学 | Disposable hand cleanser of one Plant Extracts and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1824743A (en) * | 2005-02-22 | 2006-08-30 | 楼国富 | Cleaning powder |
| CN101569600A (en) * | 2009-06-08 | 2009-11-04 | 昆明理工大学 | Antibacterial traditional Chinese medicine additive for bath lotion and preparation method thereof |
| CN102167999A (en) * | 2010-06-08 | 2011-08-31 | 李静 | Cleanser and cleansing method for food or cooking utensils |
| CN102198059A (en) * | 2011-04-29 | 2011-09-28 | 安徽师范大学 | Novel cleaning material |
| CN102559408A (en) * | 2011-12-30 | 2012-07-11 | 北京绿伞化学股份有限公司 | Pure plant type antibacterial cleanser and preparation method thereof |
-
2014
- 2014-11-27 CN CN201410712852.3A patent/CN104490658B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1824743A (en) * | 2005-02-22 | 2006-08-30 | 楼国富 | Cleaning powder |
| CN101569600A (en) * | 2009-06-08 | 2009-11-04 | 昆明理工大学 | Antibacterial traditional Chinese medicine additive for bath lotion and preparation method thereof |
| CN102167999A (en) * | 2010-06-08 | 2011-08-31 | 李静 | Cleanser and cleansing method for food or cooking utensils |
| CN102198059A (en) * | 2011-04-29 | 2011-09-28 | 安徽师范大学 | Novel cleaning material |
| CN102559408A (en) * | 2011-12-30 | 2012-07-11 | 北京绿伞化学股份有限公司 | Pure plant type antibacterial cleanser and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 胡云峰 主编: "《瓜类蔬菜保鲜与加工技术》", 31 January 2008 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106691950A (en) * | 2017-02-27 | 2017-05-24 | 陕西理工学院 | Selfheal-containing Chinese herbal hand sanitizer and preparation method |
| CN107854350A (en) * | 2017-10-20 | 2018-03-30 | 芜湖皮皮鲁网络技术有限公司 | Main broadcaster's Environmentally-friehand hand sanitizer and preparation method thereof |
| CN107898675A (en) * | 2017-12-12 | 2018-04-13 | 佛山早稻田科技服务有限公司 | A kind of Environmentally-friehand hand sanitizer |
| CN108451843A (en) * | 2018-02-12 | 2018-08-28 | 华南理工大学 | Disposable hand cleanser of one Plant Extracts and preparation method thereof |
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| CN104490658B (en) | 2017-09-19 |
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