CN104479872B - A kind of tobacco aromaticss formula - Google Patents
A kind of tobacco aromaticss formula Download PDFInfo
- Publication number
- CN104479872B CN104479872B CN201410825490.9A CN201410825490A CN104479872B CN 104479872 B CN104479872 B CN 104479872B CN 201410825490 A CN201410825490 A CN 201410825490A CN 104479872 B CN104479872 B CN 104479872B
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- China
- Prior art keywords
- cigarette
- ketone
- electronic cigarette
- isophorone
- hydroxyl
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/32—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by acyclic compounds
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/34—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a carbocyclic ring other than a six-membered aromatic ring
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/36—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a heterocyclic ring
- A24B15/40—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a heterocyclic ring having only oxygen or sulfur as hetero atoms
- A24B15/403—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a heterocyclic ring having only oxygen or sulfur as hetero atoms having only oxygen as hetero atoms
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
- C11B9/0034—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing six carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0069—Heterocyclic compounds
- C11B9/0073—Heterocyclic compounds containing only O or S as heteroatoms
- C11B9/0076—Heterocyclic compounds containing only O or S as heteroatoms the hetero rings containing less than six atoms
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0069—Heterocyclic compounds
- C11B9/0073—Heterocyclic compounds containing only O or S as heteroatoms
- C11B9/008—Heterocyclic compounds containing only O or S as heteroatoms the hetero rings containing six atoms
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0069—Heterocyclic compounds
- C11B9/0073—Heterocyclic compounds containing only O or S as heteroatoms
- C11B9/0084—Heterocyclic compounds containing only O or S as heteroatoms the hetero rings containing more than six atoms
Abstract
The invention discloses a kind of tobacco aromaticss formula, it is characterised in that:It is made up of following a variety of fragrance components:Solvent;The ketone of 6 methyl, 3,5 heptadiene 2;The cyclohexanedione of 3 methyl 1,2;The ketone of 3 ethyl, 2 hydroxyl, 2 cyclopentene 1;3,4 dimethylcyclopentene alcohol ketone;Maltol;Isophorone;Aoxidize isophorone;γ caprolactones;The dimethyl 3 of 4 hydroxyl 2,5 (2H) furanone.This is formulated for that can significantly improve the burnt fragrant and sweet feature of flue gas in cigarette and electronic cigarette, and electronic cigarette is produced the odor characteristic of more approximate cigarette smoke, meets the electronic cigarette consumer demand for pursuing cigarette organoleptic features.
Description
Technical field
It is specifically a kind of burnt fragrant and sweet for lifting cigarette and electronic cigarette the invention belongs to tobacco product meat flavor formulating technology field
Tobacco aromaticss formula.
Background technology
It is burnt it is fragrant and sweet be Chinese-style cigarette flue gas aromatic style feature important note.Commented according to Chinese-style cigarette style and features sense organ
Valency method, burnt fragrant and sweet (caramel-like aroma) and nut are fragrant(nutty aroma)Collectively constitute and bakeed perfume (roast
Aroma) note.The smoking result of the representative brand cigarettes such as China, lotus king, sharp group, Mount Huang, Hongta, white sand, Yuxi shows
Show, bakee the important component that perfume is its style and features.And for most of Chinese-style cigarettes, fragrant and sweet Jiao is that it bakees perfume
The main note of note feature is adjusted, such as foregoing several cigarette brands, in addition to Baisha brand bakees perfume (or spice) and is mainly shown as that nut is fragrant, remaining
Bakee perfume and be mainly shown as burnt fragrant and sweet feature.Therefore, the burnt fragrant and sweet feature of flue gas is improved, for carrying for Chinese-style cigarette organoleptic quality
Rising has obvious impetus.
On the other hand, with countries in the world pair《The Framework Convention on Tobacco Control》Fulfil it is continuous with smoking and health research
Deeply, electronic cigarette gradually obtains the attention in market as a kind of substitute products of cigarette.Although at present to the security of electronic cigarette
Remain and disputing on, but contrast traditional cigarette, the harmful components species or content of electronic cigarette, which all have, significantly to drop
It is low(Z. Cahn and M. Siegel,Journal of Public Health Policy, 2011, vol. 32 , 1,
16–31).But existing market it is on sale electronic cigarette fragrance style it is more dull, the mainly odor type such as peppermint, cocoa, fruit
Product, the fragrance characteristic enriched with cigarette smoke are far apart.For this reason, it is necessary to the main note rhythm design for cigarette smoke is corresponding
Fragrance formulations to strengthen the rich of electronic cigarette flue gas.
The content of the invention
It is an object of the invention to provide a kind of tobacco aromaticss formula to lift the burnt fragrant and sweet note feature of cigarette smoke, and solve
At present the problem of electronic cigarette smoke perfume style dullness.Perfumer can be directed to burnt fragrant and sweet feature, easily in cigarette and electronics
The fragrance formulations, rich and enhancing electronic cigarette and the cigarette fragrance characteristic of enhancing cigarette smoke fragrance are used in cigarette blending
Similarity.
Above-mentioned purpose of the present invention is achieved by the following technical programs:
A kind of tobacco aromaticss formula, it is made up of by mass percentage following components:Solvent 75-90%;6- methyl -3,5- heptan
Diene -2- ketone 1-2%;3- methyl isophthalic acids, 2- cyclohexanediones 0-1%;3- ethyl -2- hydroxyl -2- cyclopentene-1-ones 1-6%;3,4- bis-
Methyl cyclopentenyl ketone 1-4%;Maltol 1-4%;Isophorone 0.5-3%;Aoxidize isophorone 0-1%;γ-hexalactone 0-1%;
4- hydroxyl -2,5- dimethyl -3 (2H) furanone 1-8%, said components sum is 100%.
As a kind of preferred scheme, above-mentioned tobacco aromaticss formula is by as follows according to the various ingredients group of mass percentage
Into:Solvent 83.9%;6- methyl -3,5- heptadiene -2- ketone 1.4%;3- methyl isophthalic acids, 2- cyclohexanediones 0.3%;3- ethyl -2- hydroxyls
Base -2- cyclopentene-1-ones 4.0%;3,4- dimethylcyclopentenes alcohol ketone 2.0%;Maltol 2.5%;Isophorone 1.1%;Aoxidize different
Phorone 0.6%;γ-hexalactone 0.6%;4- hydroxyl -2,5- dimethyl -3 (2H) furanone 3.6%.
The solvent is that one or both of water, ethanol, propane diols, glycerine are mixed above.
In 9 kinds of compositions, 3- methyl isophthalic acids, 2- cyclohexanediones, 3- ethyl -2- hydroxyl -2- cyclopentene-1-ones, 3,4- bis-
Methyl cyclopentenyl ketone, maltol and 4- hydroxyl -2,5- dimethyl -3 (2H) furanone five class monomer perfume be respectively provided with typically
Caramel sample fragrance.6- methyl -3,5- heptadiene -2- ketone shows as the fragrance of Chinese cassia tree-similar nut with oxidation isophorone;Different Buddhist
Your ketone has the fragrance of sweet tea, similar honey-tobacco;γ-hexalactone has the gentle strong fragrance with herbal;This four class
Though it is fragrant and sweet that monomer perfume does not appear as directly Jiao, there is good compatibility with foregoing five kinds of monomer perfumes, and be cigarette
The intrinsic composition of flue gas, abundant fragrance intension can be played for tobacco and tobacco product, avoid the dull effect of fragrance.
It is raw materials used commercially available in tobacco aromaticss formula of the present invention;Preparation process, which is that blending field is conventional, to be stirred
Standing process, without special installation.
The invention has the advantages that:
(1)The composition of tobacco aromaticss formula of the present invention can significantly improve the burnt fragrant and sweet impression of cigarette and electronic cigarette flue gas, and
Electronic cigarette is set to produce the organoleptic feature for being more nearly cigarette smoke.
(2)Tobacco aromaticss of the present invention formula is with strong points, motivated during use, can facilitate blending process.
(3)Tobacco aromaticss formula of the present invention is raw materials used to be readily available, simple production process.
Embodiment
Son is described further to the present invention with reference to embodiments, but the model not limiting the invention in any way
Enclose.
Embodiment 1
Spices matches(Mass percentage)
Ethanol 83.9%;6- methyl -3,5- heptadiene -2- ketone 1.4%;3- methyl isophthalic acids, 2- cyclohexanediones 0.3%;3- ethyls-
2- hydroxyl -2- cyclopentene-1-ones 4.0%;3,4- dimethylcyclopentenes alcohol ketone 2.0%;Maltol 2.5%;Isophorone 1.1%;Oxygen
Change isophorone 0.6%;γ-hexalactone 0.6%;4- hydroxyl -2,5- dimethyl -3 (2H) furanone 3.6%.
Take cigarette Bright Yellow in Henan " great Jin circles " brand cigarette, the use that the spice solution of above-mentioned composition is propped up according to 10 μ L/
Amount carries out perfuming injection, and temperature (22 ± 1) DEG C is placed in after injection and is balanced 48 hours in the environment of relative humidity (60 ± 2) %.
Suction evaluation is carried out by 7 electronic cigarette sensory evaluation personnel.All evaluation personnels are experienced, with non-perfuming injection cigarette phase
Than the burnt fragrant and sweet note of cigarette that with the addition of this fragrance formulations protrudes, and fragrance is long abundant, the sufficient hair thoroughly of perfume quantity.
Embodiment 2
Spices matches(Mass percentage)
Ethanol 60.0%;Water 20.0%;6- methyl -3,5- heptadiene -2- ketone 1.4%;3- methyl isophthalic acids, 2- cyclohexanediones 1.0%;
3- ethyl -2- hydroxyl -2- cyclopentene-1-ones 5.0%;3,4- dimethylcyclopentenes alcohol ketone 2.0%;Maltol 3.1%;Isophorone
2.0%;γ-hexalactone 1.0%;4- hydroxyl -2,5- dimethyl -3 (2H) furanone 4.5%.
Take cigarette Bright Yellow in Henan " great Jin circles " brand cigarette, the use that the spice solution of above-mentioned composition is propped up according to 10 μ L/
Amount carries out perfuming injection, and temperature (22 ± 1) DEG C is placed in after injection and is balanced 48 hours in the environment of relative humidity (60 ± 2) %.
Suction evaluation is carried out by 7 electronic cigarette sensory evaluation personnel.All evaluation personnels are experienced, with non-perfuming injection cigarette phase
Than the burnt fragrant and sweet note of cigarette that with the addition of this fragrance formulations protrudes, while the mellow and full exquisiteness of cigarette smoke, pleasant, excitant
Gently.
Embodiment 3
Spices matches(Mass percentage)
Propane diols 50.0%;Glycerine 33.9%;6- methyl -3,5- heptadiene -2- ketone 1.7%;3- ethyl -2- hydroxyl -2- rings penta
Alkene -1- ketone 4.0%;3,4- dimethylcyclopentenes alcohol ketone 2.0%;Maltol 2.5%;Isophorone 1.1%;Aoxidize isophorone
0.6%;γ-hexalactone 0.6%;4- hydroxyl -2,5- dimethyl -3 (2H) furanone 3.6%.
The mL of spice solution 2 of above-mentioned composition is taken to add in the mL of tobacco juice for electronic smoke 10 of this laboratory development, uniformly mixing
After take 4 mL add electronic cigarette core in, stand 2 hours after, carry out suction evaluation by 7 electronic cigarette sensory evaluation personnel.It is all
Evaluation personnel is experienced, and with the addition of the electronic cigarette of this fragrance formulations has obvious burnt fragrant and sweet feature, with the original perfume (or spice) of electronic cigarette
Gas harmony is preferable, while the odor characteristic of electronic cigarette is closer to true cigarette smoke.
Embodiment 4
Spices matches(Mass percentage)
Ethanol 50.0%;Propane diols 24.0%;Water 10.0%;6- methyl -3,5- heptadiene -2- ketone 2.0%;3- methyl isophthalic acids, 2-
The % of cyclohexanedione 1.0;3- ethyl -2- hydroxyl -2- cyclopentene-1-ones 3.5%;3,4- dimethylcyclopentenes alcohol ketone 2.5%;Maltol
2.3%;Isophorone 1.1%;4- hydroxyl -2,5- dimethyl -3 (2H) furanone 3.6%.
Take the mL of spice solution 1 of above-mentioned composition to add in the commercially available mL of tobacco juice for electronic smoke 10, uniformly take 4 mL after mixing
Add in electronic cigarette core, after standing 2 hours, suction evaluation is carried out by 7 electronic cigarette sensory evaluation personnel.All evaluation personnels
Experience, with the addition of the electronic cigarette liquid of this fragrance formulations compared with when being not added with, burnt fragrant and sweet note feature is significantly increased, together
The original fragrance harmony of electronic cigarette is preferable, while the odor characteristic of electronic cigarette is closer to true cigarette smoke.
Claims (2)
- A kind of 1. tobacco aromaticss, it is characterised in that:It is made up of by mass percentage following components:Solvent 75-90%;6- methyl -3, 5- heptadiene -2- ketone 1-2%;3- methyl isophthalic acids, 2- cyclohexanediones 0-1%;3- ethyl -2- hydroxyl -2- cyclopentene -1- Ketone 1-6%;3,4- dimethylcyclopentene alcohol ketone 1-4%;Maltol 1-4%;Isophorone 0.5-3%;Aoxidize isophorone 0- 1% ;γ-caprolactone 0-1%;4- hydroxyls -2,5- dimethyl -3 (2H) furanone 1-8%, said components sum are 100%.
- 2. the tobacco aromaticss according to claim 1, it is characterised in that:The solvent is in water, ethanol, propane diols, glycerine One or more kinds of mixing.
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CN201410825490.9A CN104479872B (en) | 2014-12-28 | 2014-12-28 | A kind of tobacco aromaticss formula |
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CN201410825490.9A CN104479872B (en) | 2014-12-28 | 2014-12-28 | A kind of tobacco aromaticss formula |
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CN104479872B true CN104479872B (en) | 2018-03-09 |
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CN104774688B (en) * | 2015-04-10 | 2018-03-09 | 云南中烟工业有限责任公司 | A kind of essence for highlighting fresh and sweet fragrant style and features and its application in cigarette |
CN107912803B (en) * | 2016-10-10 | 2021-07-02 | 湖南中烟工业有限责任公司 | Method for weakening baking aroma in product obtained by tobacco heat treatment |
CN107604748B (en) * | 2017-07-28 | 2020-08-28 | 河南中烟工业有限责任公司 | Baked sweet cigarette paper with moisturizing function and preparation method thereof |
CN109181869A (en) * | 2018-09-29 | 2019-01-11 | 中国烟草总公司郑州烟草研究院 | A kind of burnt fragrant and sweet essence of cigarette |
CN110897188A (en) * | 2019-11-07 | 2020-03-24 | 河南中烟工业有限责任公司 | Roasted sweet potato flavor, preparation method and application in cigarettes |
CN111165779A (en) * | 2019-12-24 | 2020-05-19 | 福建正味生物科技有限公司 | Broad-spectrum flavouring agent for food and its preparing process |
CN111588067B (en) * | 2020-05-28 | 2023-03-21 | 浙江中烟工业有限责任公司 | Fragrance base module capable of highlighting baking fragrance characteristics of cigarettes and application of fragrance base module |
CN111713740B (en) * | 2020-06-28 | 2022-08-26 | 云南中烟工业有限责任公司 | Additive with angelica sinensis aroma style characteristics, preparation method thereof and cigarette containing additive |
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