CN104479773A - Heavy oil emulsifier and preparation method thereof - Google Patents
Heavy oil emulsifier and preparation method thereof Download PDFInfo
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- CN104479773A CN104479773A CN201410640805.2A CN201410640805A CN104479773A CN 104479773 A CN104479773 A CN 104479773A CN 201410640805 A CN201410640805 A CN 201410640805A CN 104479773 A CN104479773 A CN 104479773A
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- emulsifying agent
- oil
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- heavy oil
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Abstract
The invention relates to a heavy oil emulsifier and a preparation method thereof. The emulsifier enables water doped heavy oil to have a long stable period and stably maintains for 3-5 months without oil-water separation; an additive based on water greatly dilutes the viscosity of heavy oil and improves the fluidity of the heavy oil, so the heavy oil sprayed from a nozzle has a large dispersibility, fully contacts with air and can be completely combusted, thereby black smoke is eliminated, and environmental protection is facilitated; the water addition rate of the heavy oil is high and can reach 20-50%, the use amount of the additive is 1-30%, and the oil saving rate reaches 15-30%, so the fuel resource is saved; the oil nozzle cannot be coked, and a device pipeline cannot be corroded, so the maintenance frequency of the nozzle is greatly reduced; and the fuel cost per use unit is reduced, and the maintenance cost of a boiler and other combination devices is also reduced.
Description
Technical field
The invention belongs to additive for heavy oil field, particularly a kind of heavy-oil emulsifying agent and preparation method thereof.
Background technology
At present, energy shortage is the major issue that countries in the world face, and how to effectively utilize heavy oil also becomes the focus paid close attention to various countries thereupon, and the price of heavy oil is low, source has certain calorific value extensively, again, is therefore a kind of main source of fuel.Heavy oil also claims residual oil, and being crude oil extracts the Residual oil after distillate through normal pressure or vacuum distillation apparatus, or by the crack resid extracted out at the bottom of high-temperature pressurizing cracking evaporator tower, or by the two mixing, also or add the heavy crude fuel that appropriate crack resid makes.
The outstanding feature of heavy oil is that colloid, asphalt content are high, causes its viscosity large, poor fluidity, brings very large difficulty to exploitation and application.In addition, heavy oil is a kind of Residual oil, and therefore its viscosity is high, detrimental impurity content is high, complicated component.Containing detrimental impurity such as sulphur (S), sodium (Na), potassium (K), vanadium (V) in heavy oil, when residual oil is as fuel, the SO that sulfur-bearing composition generates
2, SO
3can react with NaCL, KCL Deng corrosives and generate Na
2sO
4and K
2sO
4, and vanadium is oxidized to V
2o
5.Work as V
2o
5, Na
2sO
4and K
2sO
4be deposited on hardware on the surface with molten state, serious vanadium corrosion mouth can be brought out.In heavy oil, Na, K equal size is higher, and it can cause metallic surface havoc to the thermal etching that equipment produces in combustion.
Therefore, often adopt physics, heavy oil that chemical process makes thickness becomes a kind of fluid at normal temperatures with good fluidity, to realize carrying out the object of heavy oil recovery, conveying and industrial combustion under the condition not having steam heating and companion's heat.The mining type of current viscous crude generally uses the methods such as injection thermal recovery, electrically heated oil reservoir, chemical viscosity reduction, wherein in the exploitation of viscous crude, accumulating, transportation, there is the unexistent advantage of additive method with the reducing viscosity by emulsifying technology chemical viscosity reduction that is representative and be subject to the common concern of people, there is very large development potentiality.
Emulsification heavy oil is exactly by the heavy oil of hot melt state, with the blended emulsification of the aqueous solution containing emulsifying agent under the mechanical effects such as high speed centrifugation, shearing, impact, form heavy oil milk sap, oil-in-water emulsion is formed for viscous crude general requirement, in the past water-in-oil-type is mainly for heavy oil milk sap, along with the raising that energy saving standard requires, its watering quantity constantly increases, and focuses on oil-in-water-type heavy oil mixed with water milk sap at present.Heavy oil emulsive technology effectively can reduce its viscosity, improve its mobility, improve many application performances of heavy oil, many fields such as viscous oil recovery and transport, industrial burnup, heavy oil fluid catalytic cracking, casting technique are now widely used in, and its range of application, also in continuous expansion, thus has wide market outlook.
Be such as must carry out purifying treatment to heavy oil before the GTCC power plant of fuel uses with heavy oil, namely use deionized water emulsification heavy oil, make the salt such as water-soluble Na, K be dissolved in water, then add special emulsifying agent water effective is removed, reach the object of purification heavy oil.Therefore, the dehydration effect of emulsifying agent directly affects the use of heavy oil and the operation of equipment.
Summary of the invention
The invention provides a kind of heavy-oil emulsifying agent and preparation method thereof, be to solve heavy oil detrimental impurity many, use after needing to utilize emulsifying agent purifying treatment; And viscosity is large, poor fluidity, combustion fumes are large and carbon deposit is many and additive does not affect the technical problem of temperature of combustion.
Technical solution of the present invention is as follows, and the present invention is made up of emulsifying agent, assistant for emulsifying agent, ignition dope, inhibiter, deionized water, is made up of the component of following number, and described number is weight part:
Emulsifying agent 20-40 part;
Assistant for emulsifying agent 10-20 part;
Ignition dope 5-15 part;
Inhibiter 4-7 part;
Deionized water 10-15 part.
Described emulsifying agent is made up of the component of following number, and described number is weight part:
Soxylat A 25-7 6-9 part;
Arlacel-60 5-8 part;
Polypropylene glycol 6-10 part;
Sodium dodecylbenzene sulfonate 3-13 part.
Described assistant for emulsifying agent is made up of the component of following number, and described number is weight part:
BDO 4-7 part;
Ethylene glycol 3-5 part;
Pentyl alcohol 3-8 part.
Described ignition dope is made up of the component of following number, and described number is weight part:
Methyl tertiary butyl ether 2-7 part;
Ethyl Tertisry Butyl Ether 3-8 part.
Described inhibiter is made up of the component of following number, and described number is weight part:
Amino Trimethylene Phosphonic Acid 2-3 part;
1-Hydroxy Ethylidene-1,1-Diphosphonic Acid 1-2 part.
In heavy-oil emulsifying agent of the present invention, emulsifying agent and help assistant for emulsifying agent, can be good at coordination and is distributed in water-oil interface, reduce the surface tension between profit, can make water droplet stable be dispersed in heavy oil, define stable microemulsion system.
Heavy-oil emulsifying agent preparation process of the present invention is as follows:
(1) at 20-50 DEG C, first emulsifying agent, assistant for emulsifying agent, water are added Mixer pot, stir 1-3h;
(2) in said mixture, add ignition dope, stir 1-2h;
(3) inhibiter is added said mixture and stir 2-3h, form microemulsion system, be heavy-oil emulsifying agent product of the present invention.
beneficial effect of the present invention:
Heavy-oil emulsifying agent of the present invention, and prior art has following distinguishing feature:
1. this additive can make water mixing heavy oil long for stationary phase, and the stable individual month profit of 3-5 that keeps is not separated;
2. the additive based on water, greatly dilutes heavy oil viscosity, improves its mobility, therefore large from the dispersiveness after nozzle ejection, and fully contact with air, burning completely, eliminates black smoke, is conducive to environment protection;
3. heavy oil mixed with water rate is high, generally can water mixing 20-50%, and additive amount is 1%-30%, and rate of economizing gasoline reaches 15-30%, fuel saving resource;
4. remarkable in economical benefits.The fuel cost of applying unit can be reduced, and the maintenance cost of the combustion equipment such as boiler;
5. oil nozzle not easily coking, equipment pipeline is not perishable, greatly reduces oil nozzle maintaining number of times.
Specific embodiment
Following embodiment is further illustrating invention, but the present invention is not limited only to this.
embodiment 1
The invention provides a kind of heavy-oil emulsifying agent and preparation method thereof, be made up of the component of following number, described number is weight part:
Soxylat A 25-7 6 parts;
Arlacel-60 5 parts;
Polypropylene glycol 6 parts;
Sodium dodecylbenzene sulfonate 3 parts.
BDO 4 parts;
Ethylene glycol 3 parts;
Pentyl alcohol 3 parts;
Ignition dope 5 parts;
Inhibiter 4 parts;
Deionized water 10 parts;
Methyl tertiary butyl ether 2 parts;
Ethyl Tertisry Butyl Ether 3 parts;
Amino Trimethylene Phosphonic Acid 2 parts;
1-Hydroxy Ethylidene-1,1-Diphosphonic Acid 1 part.
Heavy-oil emulsifying agent preparation process of the present invention is as follows:
At (1) 20 DEG C, first emulsifying agent, assistant for emulsifying agent, water are added Mixer pot, stir 1h;
(2) in said mixture, add ignition dope, stir 1h;
(3) inhibiter is added said mixture and stir 2h, form microemulsion system, be heavy-oil emulsifying agent product of the present invention.
embodiment 2
The invention provides a kind of heavy-oil emulsifying agent and preparation method thereof, be made up of the component of following number, described number is weight part:
Soxylat A 25-7 7 parts;
Arlacel-60 6 parts;
Polypropylene glycol 8 parts;
Sodium dodecylbenzene sulfonate 5 parts;
BDO 5 parts;
Ethylene glycol 4 parts;
Pentyl alcohol 5 parts;
Ignition dope 6 parts;
Inhibiter 5 parts;
Deionized water 11 parts;
Methyl tertiary butyl ether 5 parts;
Ethyl Tertisry Butyl Ether 4 parts;
Amino Trimethylene Phosphonic Acid 2 parts;
1-Hydroxy Ethylidene-1,1-Diphosphonic Acid 1 part.
Heavy-oil emulsifying agent preparation process of the present invention is as follows:
At (1) 30 DEG C, first emulsifying agent, assistant for emulsifying agent, water are added Mixer pot, stir 1.5h;
(2) in said mixture, add ignition dope, stir 1h;
(3) inhibiter is added said mixture and stir 2.5h, form microemulsion system, be heavy-oil emulsifying agent product of the present invention.
embodiment 3
The invention provides a kind of heavy-oil emulsifying agent and preparation method thereof, be made up of the component of following number, described number is weight part:
Soxylat A 25-7 8 parts;
Arlacel-60 7 parts;
Polypropylene glycol 9 parts;
Sodium dodecylbenzene sulfonate 12 parts;
BDO 6 parts;
Ethylene glycol 4 parts;
Pentyl alcohol 7 parts;
Ignition dope 14 parts;
Inhibiter 6 parts;
Deionized water 13 parts;
Methyl tertiary butyl ether 5 parts;
Ethyl Tertisry Butyl Ether 7 parts;
Amino Trimethylene Phosphonic Acid 3 parts;
1-Hydroxy Ethylidene-1,1-Diphosphonic Acid 2 parts.
Heavy-oil emulsifying agent preparation process of the present invention is as follows:
At (1) 40 DEG C, first emulsifying agent, assistant for emulsifying agent, water are added Mixer pot, stir 2h;
(2) in said mixture, add ignition dope, stir 2h;
(3) inhibiter is added said mixture and stir 2.5h, form microemulsion system, be heavy-oil emulsifying agent product of the present invention.
embodiment 4
The invention provides a kind of heavy-oil emulsifying agent and preparation method thereof, be made up of the component of following number, described number is weight part:
Soxylat A 25-7 9 parts;
Arlacel-60 8 parts;
Polypropylene glycol 10 parts;
Sodium dodecylbenzene sulfonate 13 parts;
BDO 7 parts;
Ethylene glycol 5 parts;
Pentyl alcohol 8 parts;
Ignition dope 15 parts;
Inhibiter 7 parts;
Deionized water 15 parts;
Methyl tertiary butyl ether 7 parts;
Ethyl Tertisry Butyl Ether 8 parts;
Amino Trimethylene Phosphonic Acid 3 parts;
1-Hydroxy Ethylidene-1,1-Diphosphonic Acid 2 parts.
Heavy-oil emulsifying agent preparation process of the present invention is as follows:
At (1) 50 DEG C, first emulsifying agent, assistant for emulsifying agent, water are added Mixer pot, stir 3h;
(2) in said mixture, add ignition dope, stir 2h;
(3) inhibiter is added said mixture and stir 3h, form microemulsion system, be heavy-oil emulsifying agent product of the present invention.
Claims (8)
1. a heavy-oil emulsifying agent, is made up of following raw material, and described number is weight part:
Emulsifying agent 20-40 part;
Assistant for emulsifying agent 10-20 part;
Ignition dope 5-15 part;
Inhibiter 4-7 part;
Deionized water 10-15 part.
2. a kind of heavy-oil emulsifying agent of claim 1, it is characterized in that: described emulsifying agent is made up of the component of following number, described number is weight part:
Soxylat A 25-7 6-9 part;
Arlacel-60 5-8 part;
Polypropylene glycol 6-10 part;
Sodium dodecylbenzene sulfonate 3-13 part.
3. a kind of heavy-oil emulsifying agent of claim 1, it is characterized in that described assistant for emulsifying agent is made up of the component of following number, described number is weight part:
BDO 4-7 part;
Ethylene glycol 3-5 part;
Pentyl alcohol 3-8 part.
4. a kind of heavy-oil emulsifying agent of claim 1, it is characterized in that: described ignition dope is made up of the component of following number, described number is weight part:
For methyl tertiary butyl ether 2-7 part;
Ethyl Tertisry Butyl Ether 3-8 part.
5. a kind of heavy-oil emulsifying agent of claim 1, it is characterized in that: described inhibiter is made up of the component of following number, described number is weight part:
Amino Trimethylene Phosphonic Acid 2-3 part;
1-Hydroxy Ethylidene-1,1-Diphosphonic Acid 1-2 part.
6. the preparation method of a kind of heavy-oil emulsifying agent of claim 1, is characterized in that:
1) first emulsifying agent, assistant for emulsifying agent, water are added Mixer pot, stir 1-3h;
2) in said mixture, add ignition dope, stir 1-2h;
3) inhibiter is added said mixture to stir, form microemulsion system, be heavy-oil emulsifying agent product of the present invention.
7. the preparation method of a kind of heavy-oil emulsifying agent of claim 6, is characterized in that: carry out at 20-50 DEG C in step 1).
8. the preparation method of a kind of heavy-oil emulsifying agent of claim 6, is characterized in that: in step 3), inhibiter is added mixture and stir 2-3h.
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| CN201410640805.2A CN104479773B (en) | 2014-11-14 | 2014-11-14 | A kind of heavy-oil emulsifying agent and preparation method thereof |
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| CN201410640805.2A CN104479773B (en) | 2014-11-14 | 2014-11-14 | A kind of heavy-oil emulsifying agent and preparation method thereof |
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| CN104479773A true CN104479773A (en) | 2015-04-01 |
| CN104479773B CN104479773B (en) | 2015-12-30 |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105435841A (en) * | 2015-11-18 | 2016-03-30 | 苏同兴 | Water phase change catalyst and preparation method thereof |
| CN106479583A (en) * | 2016-11-10 | 2017-03-08 | 黑龙江省能源环境研究院 | Emulsification heavy oil of high stability and preparation method thereof |
| CN106520229A (en) * | 2016-11-10 | 2017-03-22 | 黑龙江省能源环境研究院 | Composite emulsification heavy oil additive and preparation method thereof |
| CN108179037A (en) * | 2018-01-15 | 2018-06-19 | 安徽龙谷商贸有限公司 | A kind of energy saving and environment friendly heavy oil emulsifying agent and its emulsifying process |
| CN108264943A (en) * | 2018-01-15 | 2018-07-10 | 安徽龙谷商贸有限公司 | A kind of novel built emulsifier |
| CN108300528A (en) * | 2018-02-09 | 2018-07-20 | 张可池 | A kind of heavy-oil emulsifying agent and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105435841A (en) * | 2015-11-18 | 2016-03-30 | 苏同兴 | Water phase change catalyst and preparation method thereof |
| CN106479583A (en) * | 2016-11-10 | 2017-03-08 | 黑龙江省能源环境研究院 | Emulsification heavy oil of high stability and preparation method thereof |
| CN106520229A (en) * | 2016-11-10 | 2017-03-22 | 黑龙江省能源环境研究院 | Composite emulsification heavy oil additive and preparation method thereof |
| CN108179037A (en) * | 2018-01-15 | 2018-06-19 | 安徽龙谷商贸有限公司 | A kind of energy saving and environment friendly heavy oil emulsifying agent and its emulsifying process |
| CN108264943A (en) * | 2018-01-15 | 2018-07-10 | 安徽龙谷商贸有限公司 | A kind of novel built emulsifier |
| CN108300528A (en) * | 2018-02-09 | 2018-07-20 | 张可池 | A kind of heavy-oil emulsifying agent and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN104479773B (en) | 2015-12-30 |
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