CN104479398A - Pterocarpus santalinus extract and preparation method and application thereof - Google Patents

Pterocarpus santalinus extract and preparation method and application thereof Download PDF

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Publication number
CN104479398A
CN104479398A CN201410778969.1A CN201410778969A CN104479398A CN 104479398 A CN104479398 A CN 104479398A CN 201410778969 A CN201410778969 A CN 201410778969A CN 104479398 A CN104479398 A CN 104479398A
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leaflet
rosewood
extractive
dyeing
fabric
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CN104479398B (en
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纪俊玲
王东方
汪媛
陈群
陈海群
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CHANGZHOU MEISHENG BIOLOGICAL MATERIALS CO LTD
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CHANGZHOU MEISHENG BIOLOGICAL MATERIALS CO LTD
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B61/00Dyes of natural origin prepared from natural sources, e.g. vegetable sources
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/20Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B67/00Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
    • C09B67/0096Purification; Precipitation; Filtration
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M16/00Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/34General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs

Abstract

The invention belongs to the field of research of natural plant extracts, and particularly relates to a pterocarpus santalinus extract and a preparation method and application thereof. The pterocarpus santalinus extract is prepared by adopting an ethanol extracted method. The method comprises the following steps: washing pterocarpus santalinus, airing, and mechanically crushing the pterocarpus santalinus; adding to alkaline ethanol water, refluxing and extracting for 2 hours, and filtering; and carrying out spray drying on filtrate, so as to obtain pterocarpus santalinus extract powder. The pterocarpus santalinus extract can be used for dyeing textile as a natural dye, and has a good dyeing effect.

Description

A kind of leaflet rosewood extractive and preparation method thereof and application
Technical field
The invention belongs to natural plant extracts research field, particularly the extract and preparation method thereof of a kind of leaflet red sandalwood and application.
Background technology
In people today to environmental issue pay attention to day by day, more and more natural plant resource is widely used, vegetable dye is also used in fabric dyeing process more and more, but there is quite a few plant milk extract dyestuff to the upper dye poor effect of textiles, as color and luster is not dark, colour purity is not high, poor visual effect etc.Therefore the dyeing much relating to vegetable dye only rests on the experimental study stage, also really cannot replace chemical synthetic dye, realizes the industrialization of natural dyeing technique.
The timber kind belonging to Pterocarpus is various, but the red sandalwood of generally acknowledging in plant educational circles only has one, " red sandalwood ", and be commonly called as " leaflet red sandalwood ", Classification system is P.santalinus.Red sandalwood is fine work in red sandalwood, and density is large, pinhole is little is its outstanding feature, and wood is highly stable, not easily strain cracking.Red sandalwood fecund is in the torrid zone, subtropics virgin forest, optimum with the red sandalwood that Mysore nation of India area produces.Compendium of Material Medica record: leaflet red sandalwood can be stopped blooding, pain relieving, adjustment qi and blood.Leaflet red sandalwood can give out the material that one is called " wooden oxygen ", and this material can not only play the effect of tranquilization and refreshment, and life-time service can also promote that cell reproduces, the appearance of Ginseng Extract.Leaflet red sandalwood cured leaf is made the pillow of boudoir, have certain effect of releiving to gastroenteropathy.But so far, to the research of leaflet rosewood extractive and application aspect thereof or fewer.
Summary of the invention
Technical problem to be solved by this invention is: provide a kind of leaflet rosewood extractive and relevant extracting method, and about this leaflet rosewood extractive as dyestuff, the application in textile dyeing.
For solving the problems of the technologies described above, the technical solution used in the present invention is: adopt the method for extraction using alcohol to extract leaflet red sandalwood, concrete steps are as follows:
Granular leaflet red sandalwood is cleaned, dries, mechanical disintegration to 20-50 order, obtain leaflet red sandalwood crushed material, again leaflet red sandalwood crushed material is joined pH value 7-9, concentration of volume percent is in 50-85% aqueous ethanolic solution, obtain extraction system, the mass ratio of leaflet red sandalwood crushed material and aqueous ethanolic solution is 1: 35; Described extraction system is warming up to 95 DEG C of refluxing extraction 2h; Filter, the filtrate obtained carried out spraying dry, obtains leaflet rosewood extractive powder,
Wherein, the pH value of above-mentioned aqueous ethanolic solution is regulated by sodium bicarbonate or sodium carbonate;
Above-mentioned spray-dired inlet temperature is 140 DEG C, and air outlet temperature is 80 DEG C.
Present invention also offers the above-mentioned leaflet rosewood extractive of a kind of employing as natural dyestuff, fabric is carried out to the technique of upper dye, concrete steps are:
Leaflet rosewood extractive powder is dissolved in ethanol, every 5g leaflet rosewood extractive powder dissolution is in 1 ~ 2ml ethanol, add deionized water dispersion again, obtain uniform diluent, and to control the mass concentration of leaflet rosewood extractive in diluent be 0.8-1.6%, and the pH value of diluent is regulated to be 4-6; Be immersed in by fabric in the diluent of gained, dye to fabric, controlling dyeing condition is that bath raio is 1:10-30, and dyeing temperature is 95 DEG C, and dyeing time is 20-40 minutes, washes and dry after dyeing, obtains DYED FABRICS.
Present invention also offers the application of a kind of leaflet rosewood extractive as UV light absorber, using leaflet rosewood extractive as natural dyestuff, to giving fabric uvioresistant performance after textile dyeing;
Present invention also offers a kind of leaflet rosewood extractive as natural antibacterial staining agent, while dyeing to fabric, carry out antimicrobial treatment to fabric, bacterium is here streptococcus aureus;
Present invention also offers a kind of leaflet rosewood extractive and preventing and treating the application in anthrax: leaflet rosewood extractive powder is made into the aqueous solution that Solute mass fraction is 8-10%, fruit is sprayed, the good effect of preventing and treating anthrax can be played, or using fruit as controlling object, using being wrapped on described fruit based on leaflet rosewood extractive as the DYED FABRICS of dyestuff, the effect of preventing and treating anthrax can be played.
Beneficial effect of the present invention is: the present invention adopts the method for ethanol-extracted to prepare leaflet rosewood extractive, simple process; Leaflet rosewood extractive is dyeed as natural dyestuff to fabric, avoid the infringement of organic chemistry dyestuff to human body skin, and there is excellent dye uptake and fabulous fastness, and color is very pure after upper dye, and floodlight effect is obvious, the cloth being suitable as high-grade clothing uses, and dyeing adapts to suitability for industrialized production; Antibacterial fabric performance, uvioresistant performance is given after dyeing, and the performance of control fruit anthrax.
Embodiment
Embodiment 1
(1) granular leaflet red sandalwood is cleaned, dries, mechanical disintegration to 30 order, obtain leaflet red sandalwood crushed material, again the leaflet red sandalwood crushed material of gained is joined pH value 7, during concentration of volume percent is 50% aqueous ethanolic solution (volume ratio of ethanol and water is 1:1), the mass ratio of leaflet red sandalwood crushed material and aqueous ethanolic solution is 1: 35, obtains extraction system;
(2) the extraction system obtained in step (1) is warming up to 95 DEG C of refluxing extraction, and is incubated 2h;
(3) system after step (2) refluxing extraction filtered, the filtrate obtained is carried out spraying dry, and inlet temperature is 140 DEG C, and air outlet temperature is 80 DEG C, obtains leaflet rosewood extractive powder, and yield is 19.2%.
Embodiment 2
(1) granular leaflet red sandalwood is cleaned, dries, mechanical disintegration to 30 order, obtain leaflet red sandalwood crushed material, again the leaflet red sandalwood crushed material of gained is joined pH value 8, during concentration of volume percent is 75% aqueous ethanolic solution (volume ratio of ethanol and water is 3:1), the mass ratio of leaflet red sandalwood crushed material and aqueous ethanolic solution is 1: 35, obtains extraction system;
(2) the extraction system obtained in step (1) is warming up to 95 DEG C of refluxing extraction, and is incubated 2h;
(3) system after step (2) refluxing extraction filtered, the filtrate obtained is carried out spraying dry, and inlet temperature is 140 DEG C, and air outlet temperature is 80 DEG C, obtains leaflet rosewood extractive powder, and yield is 22.8%.
Embodiment 3
(1) granular leaflet red sandalwood is cleaned, dries, mechanical disintegration to 30 order, obtain leaflet red sandalwood crushed material, again the leaflet red sandalwood crushed material of gained is joined pH value 7, during concentration of volume percent is 80% aqueous ethanolic solution (volume ratio of ethanol and water is 4:1), the mass ratio of leaflet red sandalwood crushed material and aqueous ethanolic solution is 1: 35, obtains extraction system;
(2) the extraction system obtained in step (1) is warming up to 95 DEG C of refluxing extraction, and is incubated 2h;
(3) system after step (2) refluxing extraction filtered, the filtrate obtained is carried out spraying dry, and inlet temperature is 140 DEG C, and air outlet temperature is 80 DEG C, obtains leaflet rosewood extractive powder, and yield is 18.5%.
Embodiment 4
Adopt conventional " alkaline extraction " method, extract leaflet red sandalwood, concrete steps are:
(1) granular leaflet red sandalwood is cleaned, dries, mechanical disintegration to 30 order, obtains leaflet red sandalwood crushed material, then joins in the sodium carbonate solution of pH value 10 by the leaflet red sandalwood crushed material of gained, the mass ratio of leaflet red sandalwood crushed material and sodium carbonate solution is 1: 35, obtains extraction system;
(2) the extraction system obtained in step (1) is warming up to 95 DEG C of refluxing extraction, and is incubated 2h;
(3) system after step (2) refluxing extraction filtered, the filtrate obtained is carried out spraying dry, and inlet temperature is 140 DEG C, and air outlet temperature is 80 DEG C, obtains leaflet rosewood extractive powder, and yield is 4.4%.
Embodiment 5
Adopt conventional " acid extraction " method, extract leaflet red sandalwood, concrete steps are:
(1) granular leaflet red sandalwood is cleaned, dries, mechanical disintegration to 30 order, obtains leaflet red sandalwood crushed material, then joins in the acidic solution of pH value 4 by the leaflet red sandalwood crushed material of gained, the mass ratio of leaflet red sandalwood crushed material and acidic solution is 1: 35, obtains extraction system;
(2) the extraction system obtained in step (1) is warming up to 95 DEG C of refluxing extraction, and is incubated 2h;
(3) system after step (2) refluxing extraction filtered, the filtrate obtained is carried out spraying dry, and inlet temperature is 140 DEG C, and air outlet temperature is 80 DEG C, obtains leaflet rosewood extractive powder, and yield is 2.9%.
Embodiment 6
Adopt conventional " neutral water extraction " method, extract leaflet red sandalwood, concrete steps are:
(1) granular leaflet red sandalwood is cleaned, dries, mechanical disintegration to 30 order, obtain leaflet red sandalwood crushed material, again the leaflet red sandalwood crushed material of gained is joined in the neutral deionized water of pH value 7, the mass ratio of leaflet red sandalwood crushed material and neutral deionized water is 1: 35, obtains extraction system;
(2) the extraction system obtained in step (1) is warming up to 95 DEG C of refluxing extraction, and is incubated 2h;
(3) system after step (2) refluxing extraction filtered, the filtrate obtained is carried out spraying dry, and inlet temperature is 140 DEG C, and air outlet temperature is 80 DEG C, obtains leaflet rosewood extractive powder, and yield is 2.6%.
Embodiment 7-12:
Leaflet rosewood extractive, as natural dyestuff, carries out the application of upper dye to fabric:
Adopt the leaflet rosewood extractive powder of preparation in embodiment 1-6 as natural dyestuff respectively, the technique dyeed to silk fabric is as follows:
Respectively the leaflet rosewood extractive powder of preparation in embodiment 1-6 is dissolved in ethanol, every 5g leaflet rosewood extractive powder dissolution is in 2ml ethanol, add deionized water dispersion again, obtain uniform diluent, and to control the mass concentration of leaflet rosewood extractive in diluent be 1.2%, and the pH value of diluent is regulated to be 5; Be immersed in by fabric in the diluent of gained, dye to fabric, controlling dyeing condition is that bath raio is 1:20, and dyeing temperature is 95 DEG C, and dyeing time is 60 minutes, washes and dry after dyeing, obtains DYED FABRICS.
After upper dye, performance is as shown in table 1.
Embodiment 13:
Adopt the leaflet rosewood extractive powder of preparation in embodiment 2 as natural dyestuff, dye to silk fabric, compared with the technique in embodiment 7-12, upper dye temperature is reduced to 60 DEG C, and all the other processing parameters are constant.After upper dye, performance is as shown in table 1.
Table 1: in embodiment 7-13 after dyeing, the dyeing ability of fabric
Colour fastness to rubbing presses GB/T3920-2008 " textile color stability test colour fastness to rubbing " test;
Fastness to soaping presses GB/T3921-2008 " textile color stability test fastness to soaping " test;
Colour fastness to light presses GB/T 8426-1998 " textile color stability test colour fastness to light " test;
The mensuration of color depth (K/S value): by DYED FABRICS folding twice (four layers), adopt Datacolor SF60OX Computer color testing color matching instrument to measure the K/S value of DYED FABRICS at λ max place, each sample is surveyed four times and is averaged;
Color type passes through visual inspection.
Embodiment 14
To the DYED FABRICS obtained in embodiment 7 (utilizing the extract of preparation in embodiment 1 to form as dye on dyestuff), carry out the detection of uvioresistant performance before and after dyeing:
Test by GB/T18830-2009 " evaluation of textiles UV resistance performance ", before dyeing, the UPF value of fabric is 8.62, and the UPF value of the fabric obtained after dyeing in embodiment 7 is 75.06.
Embodiment 15
To the DYED FABRICS obtained in embodiment 8 (utilizing the extract of preparation in embodiment 2 to form as dye on dyestuff), carry out the detection of uvioresistant performance before and after dyeing:
Test by GB/T18830-2009 " evaluation of textiles UV resistance performance ", before dyeing, the UPF value of fabric is 9.14, and the UPF value of the fabric obtained after dyeing in embodiment 8 is 78.31.
Embodiment 16
To the DYED FABRICS obtained in embodiment 9 (utilizing the extract of preparation in embodiment 3 to form as dye on dyestuff), carry out the detection of anti-microbial property before and after dyeing:
The DYED FABRICS obtained in embodiment 9 is cut into the circle that diameter is 2cm, the silk fabric of undyed same size is also cut into as blank sample the circle that diameter is 2cm, for subsequent use,
Then GB/T 20944.2 is pressed---2007 agar plate diffusion processs, by the Solid nutritional base for preparing at 121 DEG C of high-temperature sterilization 20min, pour in watch-glass while hot and cool, gold coated staphylococcus aureus after condensation, silk fabric after dyeing and blank sample are tightly attached on Solid nutritional base, 18h is cultivated in incubator, observing the DYED FABRICS obtained in embodiment 9 is 81% to the antibiotic rate of streptococcus aureus, and the bacteriostasis rate of silk fabric blank sample to streptococcus aureus is only 15%.
Embodiment 17:
Controlling object: citrus anthracnose
Means of prevention: the leaflet rosewood extractive powder of preparation in embodiment 1 is made into the aqueous solution that Solute mass fraction is 8%, after adopting 500ml this leaflet rosewood extractive aqueous solution evenly to spray 100kg citrusfruit, naturally ventilatedly to dry;
Again by 10 4the anthrax bacteria spore suspension 500ml of cfu/ml evenly sprays in the oranges and tangerines surface through above-mentioned process, and under being placed in room temperature, (25 DEG C) storage is observed.
In contrast, replace the leaflet rosewood extractive aqueous solution in the present embodiment to spray citrusfruit with distilled water, all the other experimental procedures are constant.
Observation through 15 days: in the oranges and tangerines of leaflet rosewood extractive aqueous solution process, sickness rate is 8%, and the citrusfruit contrasted in item is all fallen ill, and what its scab exceeded fruit surface area 1/3rd accounts for 56%.
Embodiment 18:
Controlling object: bitter rot or anthracnose of grape
Means of prevention: the leaflet rosewood extractive powder of preparation in embodiment 2 is made into the aqueous solution that Solute mass fraction is 9%, after adopting 500ml this leaflet rosewood extractive aqueous solution evenly to spray 100kg grape fruit, naturally ventilatedly to dry;
Again by 10 4the anthrax bacteria spore suspension 500ml of cfu/ml evenly sprays in the grape surface through above-mentioned process, and under being placed in room temperature, (25 DEG C) storage is observed.
In contrast, replace the leaflet rosewood extractive aqueous solution in the present embodiment to spray grape fruit with distilled water, all the other experimental procedures are constant.
Observation through 15 days: in the grape of leaflet rosewood extractive aqueous solution process, sickness rate is 11%, and the grape fruit contrasted in item is all fallen ill, and what its scab exceeded fruit surface area 1/3rd accounts for 72%.
Embodiment 19
Get the citrusfruit of 100kg maturation, be divided into two parts that quality is equal at random, the DYED FABRICS obtained in embodiment 8 is adopted to wrap up (first according to the size of citrusfruit to each oranges and tangerines in a copy of it, DYED FABRICS is cut into suitable size, respectively each citrusfruit is wrapped up again, each block fabric that control cutting is got off can realize two-layer parcel to citrusfruit just), and make upper mark;
And for each oranges and tangerines in another part, then adopt the silk fabric of undyed same size to carry out wrapping up (being two-layer parcel equally), as blank,
By 10 4the anthrax bacteria spore suspension 500ml of cfu/ml evenly sprays on the mature orange fruit that is wrapped in above-mentioned 100kg, and (25 DEG C) storage is observed under these fruits are placed in room temperature, observation through 15 days: in the citrusfruit that dyeing and weaving thing wraps up in leaflet rosewood extractive, sickness rate is 9%, and the citrusfruit contrasted in item is all fallen ill, what its scab exceeded fruit surface area 1/3rd accounts for 65%.
Embodiment 20
Get the cucumber fruits of 100kg maturation, be divided into two parts that quality is equal at random, the DYED FABRICS obtained in embodiment 9 is adopted to wrap up (first according to the size of cucumber fruits to each cucumber in a copy of it, DYED FABRICS is cut into suitable size, respectively each cucumber fruits is wrapped up again, each block fabric that control cutting is got off can realize two-layer parcel to cucumber fruits just), and make upper mark;
And for each cucumber in another part, then adopt the silk fabric of undyed same size to carry out wrapping up (being two-layer parcel equally), as blank,
By 10 4the anthrax bacteria spore suspension 500ml of cfu/ml evenly sprays in the ripe cucumber fruits that is wrapped in above-mentioned 100kg, and (25 DEG C) storage is observed under these fruits are placed in room temperature, observation through 15 days: in the cucumber fruits that dyeing and weaving thing wraps up in leaflet rosewood extractive, sickness rate is 10%, and the cucumber fruits 90% contrasted in item is fallen ill, what its scab exceeded fruit surface area 1/3rd accounts for 58%.

Claims (8)

1. a preparation method for leaflet rosewood extractive, is characterized in that: described preparation method is,
(1) granular leaflet red sandalwood is cleaned, dries, mechanical disintegration to 20-50 order, obtain leaflet red sandalwood crushed material, more described leaflet red sandalwood crushed material is joined pH value 7-9, concentration of volume percent is in 50-85% aqueous ethanolic solution, obtains extraction system;
(2) the extraction system obtained in step (1) is warming up to 95 DEG C of refluxing extraction, and is incubated 2h;
(3) system after step (2) refluxing extraction is filtered, the filtrate obtained is carried out spraying dry, obtains leaflet rosewood extractive powder.
2. the preparation method of leaflet rosewood extractive as claimed in claim 1, is characterized in that: the pH value of the aqueous ethanolic solution described in step (1) is regulated by sodium bicarbonate or sodium carbonate.
3. the preparation method of leaflet rosewood extractive as claimed in claim 1, is characterized in that: the mass ratio of the leaflet red sandalwood crushed material described in step (1) and aqueous ethanolic solution is 1: 35.
4. the preparation method of leaflet rosewood extractive as claimed in claim 1, it is characterized in that: the spray-dired inlet temperature described in step (3) is 140 DEG C, air outlet temperature is 80 DEG C.
5. leaflet rosewood extractive as claimed in claim 1 is as the dyeing of natural dyestuff to fabric, it is characterized in that: described dyeing is,
Described leaflet rosewood extractive powder is dissolved in ethanol, every 5g leaflet rosewood extractive powder dissolution is in 1 ~ 2ml ethanol, add deionized water dispersion again, obtain uniform diluent, and to control the mass concentration of leaflet rosewood extractive in diluent be 0.8-1.6%, and the pH value of diluent is regulated to be 4-6; Be immersed in by fabric in the diluent of gained, dye to fabric, controlling dyeing condition is that bath raio is 1:10-30, and dyeing temperature is 95 DEG C, and dyeing time is 20-40 minutes, washes and dry after dyeing, obtains DYED FABRICS.
6. the application of leaflet rosewood extractive as claimed in claim 1, it is characterized in that: described is applied as, leaflet rosewood extractive as the application of UV light absorber, described leaflet rosewood extractive as natural dyestuff, to giving fabric uvioresistant performance after textile dyeing.
7. the application of leaflet rosewood extractive as claimed in claim 1, it is characterized in that: described is applied as, leaflet rosewood extractive as natural antibacterial staining agent, while fabric is dyeed, carry out antimicrobial treatment to fabric, described bacterium is streptococcus aureus.
8. the application of leaflet rosewood extractive as claimed in claim 1, it is characterized in that: described is applied as, leaflet rosewood extractive is preventing and treating the application in anthrax.
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105019231A (en) * 2015-08-18 2015-11-04 肇庆涞馨美体内衣有限公司 Production technology of antibacterial and health care fabric
CN106349740A (en) * 2016-08-24 2017-01-25 张永成 Method for extracting dye with residual branch saw dust and application
CN107266933A (en) * 2017-08-25 2017-10-20 中山市中广测协同创新中心 Dyeing method on a kind of red sandalwood dyestuff and fabric
CN107501993A (en) * 2017-08-25 2017-12-22 中山市中广测协同创新中心 Dyeing method on a kind of Burma padauk dyestuff and fabric
CN109575634A (en) * 2019-01-04 2019-04-05 红河贝叶五经生物科技有限公司 A kind of extracting method of narra bronzing vegetable colour

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2483228A1 (en) * 1980-05-28 1981-12-04 Fabre Sa Pierre Natural colourant prepd. by solvent extn. of leguminous plants - of specified Pterocarpus and Dalbergia species, used as hair dyes
WO2006008917A1 (en) * 2004-07-15 2006-01-26 Lion Corporation Deodorant agent, deodorant preparation and method of deodorant treatment for fiber
CN101322738A (en) * 2007-06-11 2008-12-17 陈丽华 Preparation of red sandalwood extract for treating diabetic and uses thereof
CN101530450B (en) * 2008-03-11 2013-04-24 北京富华安德生物医药科技开发有限公司 Method for preparing pterocarpus indicus ethanol extract used for endothelium-dependent vasodilation agent and applications of method
CN103981736A (en) * 2014-03-25 2014-08-13 嘉兴学院 Dyeing method of non-woven fabrics by employing prodigiosin

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2483228A1 (en) * 1980-05-28 1981-12-04 Fabre Sa Pierre Natural colourant prepd. by solvent extn. of leguminous plants - of specified Pterocarpus and Dalbergia species, used as hair dyes
WO2006008917A1 (en) * 2004-07-15 2006-01-26 Lion Corporation Deodorant agent, deodorant preparation and method of deodorant treatment for fiber
CN101322738A (en) * 2007-06-11 2008-12-17 陈丽华 Preparation of red sandalwood extract for treating diabetic and uses thereof
CN101530450B (en) * 2008-03-11 2013-04-24 北京富华安德生物医药科技开发有限公司 Method for preparing pterocarpus indicus ethanol extract used for endothelium-dependent vasodilation agent and applications of method
CN103981736A (en) * 2014-03-25 2014-08-13 嘉兴学院 Dyeing method of non-woven fabrics by employing prodigiosin

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
M.L.GULRAJANI等: "紫檀木染料染色的动力学和热力学研究", 《国外纺织技术》 *
王立永: "新疆大学硕士学位论文", 《一种抗紫外线萘醌染料的仿生合成及修饰研究》 *
董书池: "苏州大学硕士学位论文", 《天然染料分子结构对抗紫外性的影响》 *

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105019231A (en) * 2015-08-18 2015-11-04 肇庆涞馨美体内衣有限公司 Production technology of antibacterial and health care fabric
CN106349740A (en) * 2016-08-24 2017-01-25 张永成 Method for extracting dye with residual branch saw dust and application
CN107266933A (en) * 2017-08-25 2017-10-20 中山市中广测协同创新中心 Dyeing method on a kind of red sandalwood dyestuff and fabric
CN107501993A (en) * 2017-08-25 2017-12-22 中山市中广测协同创新中心 Dyeing method on a kind of Burma padauk dyestuff and fabric
CN109575634A (en) * 2019-01-04 2019-04-05 红河贝叶五经生物科技有限公司 A kind of extracting method of narra bronzing vegetable colour

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