CN108997780A - A kind of dye yam natural dye and its application - Google Patents
A kind of dye yam natural dye and its application Download PDFInfo
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- CN108997780A CN108997780A CN201810985129.0A CN201810985129A CN108997780A CN 108997780 A CN108997780 A CN 108997780A CN 201810985129 A CN201810985129 A CN 201810985129A CN 108997780 A CN108997780 A CN 108997780A
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- dye
- dye yam
- yam
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0096—Purification; Precipitation; Filtration
Abstract
The present invention provides a kind of dye yam natural dye and its application, dye yam natural dye is made by the following method: according to parts by weight, it weighs 10-30 parts of dye yam extracting solutions, 0.5-5 parts of acid solutions and stands 3-6h after evenly mixing, obtain red purees, it by the red purees dry solidification, crushes, obtains the dye yam natural dye.Dye yam natural dye of the invention, pigment adsorption capacity is high, and color fastness is strong, and even dyeing, and extraction process is simple, and extraction efficiency is high, and at low cost, market prospects are wide, and there is sterilization and other effects, it is good with ecological environment compatibility, it is biodegradable, it can apply in terms of preventing and treating eupolyphage sece steleophaga disease.
Description
Technical field
The invention belongs to dyestuff manufacture technology fields, and in particular to a kind of dye yam natural dye and its application.
Background technique
The Neolithic Age can be traced back to using natural dye dying, in China, from the root of natural plants, stem, skin, Ye He
The history for spending the pigment of extraction to can be used for the dyeing of yarn and textile can be traced back to before more than 5000 years and be continued up to
In the middle of the 19th century.The invention of artificial synthesized dyestuff has caused the steep cliff formula drop of natural dye.However, using chemical dye to people
Body health and ecological environment cause deep negative effect, vegetable colour with nontoxic, harm, pollution-free, the graceful grace of tone,
Especially its medicine healthy sofa function has been favored by people again.Therefore, at the beginning of 21 century, fashion industry is to using natural dye
The demand of product constantly increase.However, when with natural dye dying, since the color fastness of coloring matter is relatively low,
It must repeatedly dye or dyeing color fastness is improved by using the method for medium.In addition, dye yam is conventional Chinese medicine medicinal material, has and live
Blood hemostasis, regulating qi-flowing for relieving pain, clearing heat and detoxicating effect, have in terms of medicine and have certain effect, it may be considered that in prevention and treatment soil-borne disease
Evil aspect has the effect of certain.
Summary of the invention
For above-mentioned deficiency, it is an object of the invention to provide a kind of pigment adsorption capacity height, color fastness is strong and dyeing is equal
Even dye yam natural dye.
In order to realize the purpose of foregoing invention, the present invention adopts the following technical scheme:
A kind of dye yam natural dye, is made by the following method:
According to parts by weight, 10-30 parts of dye yam extracting solutions, 0.5-5 parts of acid solutions are weighed and stand 3-6h after evenly mixing, are obtained
To red purees, by the red purees dry solidification, crushes, obtain the dye yam natural dye.
In above-mentioned technical proposal, it is preferable that the dye yam extracting solution is made with the following method:
Step 1: it is crushed, is sieved with 100 mesh sieve with high speed disintegrator by being put into after drying box is dried after the clean peeling of fresh dye yam
To dye yam powder, into dye yam powder, addition tealeaves, alkaline solution are uniformly mixed, and obtain dye yam stoste, and heat the potato
Liang stoste；
Step 2: dye yam filtrate is obtained by filtration with filter paper in dye yam stoste heated in step 1, and dye yam filtrate is evaporated
Dye yam concentration filtrate is obtained to the 5% of original volume；
Step 3: the concentration filtrate of dye yam obtained in step 2 is obtained into the dye yam extracting solution with nanofiltration membrane.
In above-mentioned technical proposal, it is further preferred that in step 1, the dye yam powder, tealeaves and alkaline solution
Weight ratio is 30:3:(1-5).
In above-mentioned technical proposal, it is preferable that in step 1, the heating temperature of the dye yam stoste is 40-90 DEG C, heating
Time is 10-30min.
In above-mentioned technical proposal, it is preferable that in step 1, the pH value of the alkaline solution is 8-10.
In above-mentioned technical proposal, it is preferable that the acid solution is one of rice vinegar, dark plum juice, juice of my pomegranate.
The present invention also provides the applications of dye yam natural dye described in any of the above-described technical solution, i.e., in prevention and treatment soil-borne disease
The application of evil aspect when concrete application, regard the plant with tree trunk structure as controlling object, it is natural will to be based on the dye yam
The dyed fabric of dyestuff is wrapped in the overground part tree trunk part of plant, wraps up 1-2 layers of fabric.
The present invention is obtained as follows compared with prior art the utility model has the advantages that dye yam natural dye pigment adsorption capacity of the invention
Height, color fastness is strong, and even dyeing, and extraction process is simple, and extraction efficiency is high, at low cost, wide market；Utilize potato
Liang extracts natural dye, and the dyestuff of available two kinds of colour systems, extract is safe and with sterilization and other effects, with ecological environment
Compatibility is good, biodegradable.
Specific embodiment
By the technology contents of invention are described in detail, construction feature, are reached purpose and efficacy, given below in conjunction with embodiment
To be described in detail.
Embodiment 1:
Step 1: it is crushed, is sieved with 100 mesh sieve with high speed disintegrator by being put into after drying box is dried after the clean peeling of fresh dye yam
To dye yam powder, according to parts by weight, the sodium hydroxide solution that 30 parts of dye yam powder, 3 portions of tealeaves, 1 part of pH value are 9 is weighed, is mixed
It closes uniformly, obtains dye yam stoste, and obtained dye yam stoste is heated into 15min at 40 DEG C；
Step 2: dye yam filtrate is obtained by filtration with filter paper in dye yam stoste heated in step 1, and dye yam filtrate is evaporated
Dye yam concentration filtrate is obtained to the 5% of original volume；
Step 3: the concentration filtrate of dye yam obtained in step 2 is obtained into dye yam extracting solution with nanofiltration membrane；
Step 4: according to parts by weight, 10 parts of dye yam extracting solutions are weighed, 0.5 part of dark plum juice stands 3h after evenly mixing, obtained
Red purees by red purees dry solidification, crushes, obtains dye yam natural dye.
First real silk fabric is impregnated into 2min in water, takes out, wrings out, is spare.The quality of natural dye and real silk fabric
Than 2%, bath raio 1:20 is put into the real silk fabric of above-mentioned processing, disseminates 30min at being 60 DEG C in temperature, uses acidity after taking out fabric
After soaping, washing drying, obtained real silk fabric uniform color, for value of chromatism △ E less than 0.4, dye-uptake reaches 79%, water-fastness
Color fastness reaches 3-4 grades.The washing fastness of all embodiments is according to " GB/T 12490-2007 textile is resistance in the present invention
The measurement of family and commercial laundering color fastness " method.
Embodiment 2:
Step 1: it is crushed, is sieved with 100 mesh sieve with high speed disintegrator by being put into after drying box is dried after the clean peeling of fresh dye yam
To dye yam powder, according to parts by weight, the sodium hydroxide solution that 30 parts of dye yam powder, 3 portions of tealeaves, 2 parts of pH value are 9 is weighed, is mixed
It closes uniformly, obtains dye yam stoste, and obtained dye yam stoste is heated into 18min at 50 DEG C；
Step 2: dye yam filtrate is obtained by filtration with filter paper in dye yam stoste heated in step 1, and dye yam filtrate is evaporated
Dye yam concentration filtrate is obtained to the 5% of original volume；
Step 3: the concentration filtrate of dye yam obtained in step 2 is obtained into dye yam extracting solution with nanofiltration membrane；
Step 4: according to parts by weight, 15 parts of dye yam extracting solutions are weighed, 1.5 parts of dark plum juice stands 3.5h after evenly mixing, obtained
To red purees, by red purees dry solidification, crushes, obtain dye yam natural dye.
First wool yarn is impregnated into 5min in water, takes out, wrings out, is spare.The quality of natural dye and wool yarn
Than 2%, bath raio 1:30 is put into the wool yarn of above-mentioned processing, disseminates 60min at being 80 DEG C in temperature, uses acidity after taking out fabric
After soaping, washing drying, obtained wool yarn uniform color, for value of chromatism △ E less than 0.3, dye-uptake reaches 80%, water-fastness
Color fastness reaches 4 grades.
Embodiment 3:
Step 1: it is crushed, is sieved with 100 mesh sieve with high speed disintegrator by being put into after drying box is dried after the clean peeling of fresh dye yam
To dye yam powder, according to parts by weight, the sodium hydroxide solution that 30 parts of dye yam powder, 3 portions of tealeaves, 2 parts of pH value are 9 is weighed, is mixed
It closes uniformly, obtains dye yam stoste, and obtained dye yam stoste is heated into 20min at 60 DEG C；
Step 2: dye yam filtrate is obtained by filtration with filter paper in dye yam stoste heated in step 1, and dye yam filtrate is evaporated
Dye yam concentration filtrate is obtained to the 5% of original volume；
Step 3: the concentration filtrate of dye yam obtained in step 2 is obtained into dye yam extracting solution with nanofiltration membrane；
Step 4: according to parts by weight, 20 parts of dye yam extracting solutions are weighed, 2.5 parts of dark plum juice stands 4h after evenly mixing, obtained
Red purees by red purees dry solidification, crushes, obtains dye yam natural dye.
First cotton fabric is boiled into 5min in boiling water, takes out, wrings out, is spare.The mass ratio of natural dye and cotton fabric
2%, bath raio 1:15 are put into the cotton fabric of above-mentioned processing, disseminate 60min at being 50 DEG C in temperature, are soaped after taking out fabric with acidity
Afterwards, washing drying, obtained cotton fabric uniform color, value of chromatism △ E is less than 0.5, and dye-uptake reaches 80%, washing color fastness
Reach 3-4 grades.
Embodiment 4:
Step 1: it is crushed, is sieved with 100 mesh sieve with high speed disintegrator by being put into after drying box is dried after the clean peeling of fresh dye yam
To dye yam powder, according to parts by weight, the sodium hydroxide solution that 30 parts of dye yam powder, 3 portions of tealeaves, 3 parts of pH value are 8 is weighed, is mixed
It closes uniformly, obtains dye yam stoste, and obtained dye yam stoste is heated into 25min at 70 DEG C；
Step 2: dye yam filtrate is obtained by filtration with filter paper in dye yam stoste heated in step 1, and dye yam filtrate is evaporated
Dye yam concentration filtrate is obtained to the 5% of original volume；
Step 3: the concentration filtrate of dye yam obtained in step 2 is obtained into dye yam extracting solution with nanofiltration membrane；
Step 4: according to parts by weight, 25 parts of dye yam extracting solutions are weighed, 4 parts of dark plum juice stands 5h after evenly mixing, obtained red
Color purees by red purees dry solidification, crushes, obtains dye yam natural dye.
First linen thread and yarn is boiled into 4min in boiling water, takes out, wrings out, is spare.The matter of natural dye and linen thread and yarn
Ratio 3% is measured, bath raio 1:15 is put into the linen thread and yarn of above-mentioned processing, disseminates 60min at being 70 DEG C in temperature, uses acid after taking out fabric
Property soap after, washing drying, obtained linen thread and yarn line uniform color, for value of chromatism △ E less than 0.4, dye-uptake reaches 80%, resistance to
Washing reaches 3-4 grades.
Embodiment 5:
Step 1: it is crushed, is sieved with 100 mesh sieve with high speed disintegrator by being put into after drying box is dried after the clean peeling of fresh dye yam
To dye yam powder, according to parts by weight, the sodium hydroxide solution that 30 parts of dye yam powder, 3 portions of tealeaves, 4 parts of pH value are 8 is weighed, is mixed
It closes uniformly, obtains dye yam stoste, and obtained dye yam stoste is heated into 30min at 80 DEG C；
Step 2: dye yam filtrate is obtained by filtration with filter paper in dye yam stoste heated in step 1, and dye yam filtrate is evaporated
Dye yam concentration filtrate is obtained to the 5% of original volume；
Step 3: the concentration filtrate of dye yam obtained in step 2 is obtained into dye yam extracting solution with nanofiltration membrane；
Step 4: according to parts by weight, 30 parts of dye yam extracting solutions are weighed, 5 parts of dark plum juice stands 6h after evenly mixing, obtained red
Color purees by red purees dry solidification, crushes, obtains dye yam natural dye.
First wool/cotton blended yarn is boiled into 4min in boiling water, takes out, wrings out, is spare.Natural dye is blended with velvet apple
The mass ratio 2% of yarn, bath raio 1:15 are put into the wool/cotton blended yarn of above-mentioned processing, disseminate 40min at being 60 DEG C in temperature, take
After being soaped after fabric with acidity out, washing drying, obtained wool/cotton blended yarn uniform color, value of chromatism △ E less than 0.5, on
Dye rate reaches 78%, and washing color fastness reaches 3-4 grades.
1- embodiment 5 through the foregoing embodiment, it can be seen that dye yam natural dye pigment adsorption capacity of the present invention is high, color is firm
Spend strong and even dyeing.
Soil-borne disease experiment:
Select that one piece of soil shape is consistent, fertility is uniformly medium, and the cotton field with certain cotton wilt incidence trend, and should
Cotton tree in cotton field has all grown the tree trunk structure for having had certain length.
The total amount of cotton tree in above-mentioned cotton field is checked, and randomly selects the cotton tree of 1/2 quantity, using in embodiment 4
Linen sheet after the dye yam natural dye dying of preparation be cut into it is suitably sized, as wrapping up cotton tree overground part tree
The fabric material of bar part wraps up the overground part tree trunk part of the cotton tree of this 1/2 quantity, wraps up two layers, is denoted as sample
Product 1；
For the cotton tree of 1/2 quantity remaining in above-mentioned cotton field, using with specification same in embodiment 4 but without
The blank linen sheet of upper dye is as the fabric material for wrapping up cotton tree overground part tree trunk part, to the cotton of this 1/2 quantity
The overground part tree trunk of Hua Shu is wrapped up, and is wrapped up two layers, is denoted as sample 2.
The incidence of the cotton wilt of the above sample 1 and sample 2 is observed, specific statistical conditions are as shown in table 1:
Table 1:
| Investigate strain tree | Cotton wilt disease incidence | |
| Sample 1 | 100 | 2% |
| Sample 2 | 100 | 70% |
(disease incidence (%)=morbidity strain tree/investigates total strain number × 100)
From table 1 it follows that dye yam dyestuff has the function of good prevention and treatment soil-borne disease.
The above embodiments merely illustrate the technical concept and features of the present invention, and its object is to allow person skilled in the art
Scholar cans understand the content of the present invention and implement it accordingly, and it is not intended to limit the scope of the present invention.It is all according to the present invention
Equivalent change or modification made by spirit, should be covered by the protection scope of the present invention.
Claims (7)
1. a kind of dye yam natural dye, which is characterized in that be made by the following method:
According to parts by weight, 10-30 parts of dye yam extracting solutions, 0.5-5 parts of acid solutions are weighed and stand 3-6h after evenly mixing, are obtained
To red purees, by the red purees dry solidification, crushes, obtain the dye yam natural dye.
2. dye yam natural dye according to claim 1, which is characterized in that the dye yam extracting solution is with the following method
It is made:
Step 1: it is crushed, is sieved with 100 mesh sieve with high speed disintegrator by being put into after drying box is dried after the clean peeling of fresh dye yam
To dye yam powder, into dye yam powder, addition tealeaves, alkaline solution are uniformly mixed, and obtain dye yam stoste, and heat the potato
Liang stoste；
Step 2: dye yam filtrate is obtained by filtration with filter paper in dye yam stoste heated in step 1, and dye yam filtrate is evaporated
Dye yam concentration filtrate is obtained to the 5% of original volume；
Step 3: the concentration filtrate of dye yam obtained in step 2 is obtained into the dye yam extracting solution with nanofiltration membrane.
3. dye yam natural dye according to claim 2, which is characterized in that in step 1, the dye yam powder, tealeaves with
And the weight ratio of alkaline solution is 30:3:(1-5).
4. dye yam natural dye according to claim 2, which is characterized in that in step 1, the dye yam stoste adds
Hot temperature is 40-90 DEG C, heating time 10-30min.
5. dye yam natural dye according to claim 2, which is characterized in that in step 1, the pH value of the alkaline solution
For 8-10.
6. dye yam natural dye according to claim 1, which is characterized in that the acid solution be rice vinegar, dark plum juice,
One of juice of my pomegranate.
7. dye yam natural dye the answering in terms of preventing and treating soil-borne disease as described in any one of claim 1-6 claim
With.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810985129.0A CN108997780A (en) | 2018-08-28 | 2018-08-28 | A kind of dye yam natural dye and its application |
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| CN201810985129.0A CN108997780A (en) | 2018-08-28 | 2018-08-28 | A kind of dye yam natural dye and its application |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109098013A (en) * | 2018-08-28 | 2018-12-28 | 苏州典传创意科技有限公司 | A kind of natural dye for Nature Fibre Textile product |
| CN109295757A (en) * | 2018-08-28 | 2019-02-01 | 苏州典传创意科技有限公司 | A kind of natural dye dying method of regenerated fiber fabric |
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| CN109098013A (en) * | 2018-08-28 | 2018-12-28 | 苏州典传创意科技有限公司 | A kind of natural dye for Nature Fibre Textile product |
| CN109295757A (en) * | 2018-08-28 | 2019-02-01 | 苏州典传创意科技有限公司 | A kind of natural dye dying method of regenerated fiber fabric |
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- 2018-08-28 CN CN201810985129.0A patent/CN108997780A/en active Pending
Patent Citations (6)
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| CN101046067A (en) * | 2007-04-12 | 2007-10-03 | 苏州大学 | Process of dyeing silk with dye yam extract |
| WO2012033536A2 (en) * | 2010-09-09 | 2012-03-15 | Kalamazoo Holdings, Inc. | Red radish and rosemary compositions with enhanced color stability and use of same in foods, beverages, cosmetics and pharmaceuticals |
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| Publication number | Priority date | Publication date | Assignee | Title |
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