CN109575634A - A kind of extracting method of narra bronzing vegetable colour - Google Patents
A kind of extracting method of narra bronzing vegetable colour Download PDFInfo
- Publication number
- CN109575634A CN109575634A CN201910006651.4A CN201910006651A CN109575634A CN 109575634 A CN109575634 A CN 109575634A CN 201910006651 A CN201910006651 A CN 201910006651A CN 109575634 A CN109575634 A CN 109575634A
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- China
- Prior art keywords
- narra
- bronzing
- vegetable
- vegetable colour
- extracting method
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/0092—Dyes in solid form
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0096—Purification; Precipitation; Filtration
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Coloring (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of extracting methods of narra bronzing vegetable colour, including pulverizer is first crushed leaflet narra to wood powder；The steaming of high energy steam box is used again；Then the wood powder after softening is added into water and ethyl alcohol and is dissolved, and ultrasonic tank separates；It is standing, after filtering, resin glue is being added into solution, and use boiling water boiling fixation, obtains red ecological vegetable liquid dyes；Finally solid-state is roasted into using plate and frame filter press filters pressing and using the roasting machine of steam；A kind of extracting method of narra bronzing vegetable colour of the present invention, obtaining red dye dry powder amount is five to ten the percent of timber weight itself, the vegetable colour extracted from leaflet red sandalwood is quite high containing haematochrome, can reduce colouring dosage, and tinctorial property is also got well than general vegetable colour；Secondly, making gained vegetable colour finally can also become at dry powder and contain quantity of fluid or solid-state like dyestuff, and be produced according to demand by the baking time of dryer.
Description
Technical field
The present invention relates to technical field of dye, specially a kind of extracting method of narra bronzing vegetable colour.
Background technique
Narra all the time all because it has excellent performance, scarcity of resources due to pursued by people.In some medical books
It mentioned, the substance for the referred to as wooden oxygen that leaflet red sandalwood comes out has the effect of good tranquilization and refreshment, Er Qiechang
The contact of time can also play facilitation to the regeneration of cell, can enough play the cosmetic result of pre- anti-wrinkle, non-to skin
Chang Hao, the red extracted, with the unique fragrance of leaflet narra.According to it is of light color it is deep require, can be with after freely deploying
With fortune on dye close-fitting fabric, daily necessities fabric, full ecological ideas, skin-friendly health.
With the improvement of living standards, the bronzing dyestuff extracted in narra is because class is higher, effect it is prominent and
By wilderness demand, however mode, the means extracted currently on the market more fall behind, and are mostly extracted by artificial mode,
Inefficiency；Also part extracts using mechanical mode, but extraction red dye dry powder amount is generally less, more wastes.
To solve the above-mentioned problems, this case is given birth to therefrom.
Summary of the invention
(1) the technical issues of solving
It is an object of the invention to overcome the deficiencies of the prior art and provide a kind of novel process of mechanization, high efficiency extraction is purple
The extracting method of sandalwood bronzing vegetable colour.
(2) technical solution
In order to achieve the above object, the present invention is achieved by the following technical programs: a kind of narra bronzing vegetable colour
Extracting method includes the following steps:
Step 1, it crushes: taking leaflet narra 1kg, be ground into wood powder with pulverizer；
Step 2, steaming: wood powder is placed in steaming 30-50min in high energy steam box, to soften wood powder；
Step 3, it separates: the wood powder after softening being fitted into 200 mesh stainless steel mesh bags and is put into 2kg boiling water, ethyl alcohol is being added
Afterwards, separation 30-50min is carried out with ultrasonic tank；
Step 4, fixation: after observing water colour from shallow to deep, picking up mesh bag, adds resin glue, and use boiling 20-30min, obtains red
Ecological vegetable liquid dyes；
Step 5, solid-state: the red ecological vegetable liquid dyes of gained in step 4 first with 400 mesh plate compressions, then use steam seasoning
Machine toasts 5-15min, and red ecological vegetable liquid dyes are roasted into dry block, finally smashing into dry powder.
Preferably, the high energy steamer temperature of step 2 is 450-550 DEG C.Steaming process is the content of material pine made in wood powder
Soft, abundant saliva enters certain moisture content, and starts steaming, consequently facilitating later separation goes out color；Certain moisture content is immersed in wood powder,
Self weight ratio increases between percentage 20 to 58.
Preferably, amount of alcohol added is 10-20g in step 3, and ultrasonic tank audio electrical signal is 20Khz ~ 500MHz.
Preferably, the additional amount of rouge glue is 45-55g in step 4, and coolant-temperature gage is at 100-110 DEG C.
Preferably, to the aqueous 20-30% of filter cake, hot air drier baking temperature is 180- for plate and frame filter press filters pressing in step 5
220℃。
(3) beneficial effect
After adopting the above technical scheme, compared with prior art, the present invention having following advantages:
1, the vegetable colour extracted from leaflet red sandalwood is quite high containing haematochrome, can reduce colouring dosage, it is dry that timber obtains red dye
Powder amount is five to ten the percent of wood itself weight, and the dyestuff tinctorial property that gained dry powder is formed is also than general vegetable colour
It is good, it is especially embodied in color fastness, color jail grade is close to 3 grades.
2, by the baking time of dryer in rate-determining steps 5, make gained vegetable colour finally can be at dry powder, it can also be at
For that can be produced according to demand containing quantity of fluid or solid-state like dyestuff.
3, it can be crushed with the waste wood secondary recovery that production red sandalwood furniture is got off, extract, can be utilized with waste product, and
And extraction overall process does not have sewage discharge, adds without any chemicals；Wooden slag in production process simultaneously, can be natural fermented
Biological chemical fertilizer is made, returns the earth, nourishes the earth, nontoxic advantageous plant growth.
Specific embodiment
The present invention will be described in detail in conjunction with the embodiments, but does not do any restriction to claim of the invention.
Embodiment one
A kind of extracting method of narra bronzing vegetable colour, includes the following steps:
Step 1, it crushes: taking leaflet narra 1kg, be ground into wood powder with pulverizer；
Step 2, steaming: wood powder is placed in 450 DEG C of high energy steam boxs and steams 30min, to soften wood powder；
Step 3, separate: the wood powder after softening is fitted into immediately in 200 mesh stainless steel mesh bags, is put into 2kg, in 100 DEG C of water, is added
10g ethyl alcohol carries out separation 30min with 350MHz ultrasonic tank；
Step 4, fixation: after seeing water colour from shallow to deep, picking up mesh bag, add resin glue 40g, still keep 100 DEG C of boiling 20min,
Obtain red ecological vegetable liquid dyes；
Step 5, solid-state: the red ecological vegetable liquid dyes of gained in step 4, first with 400 mesh plate compressions to aqueous 20%, then
5min is toasted with the hot air drier that baking temperature is 180 DEG C, red ecological vegetable liquid dyes are roasted into dry block, are finally crushed
At dry powder.
Bronzing vegetable colour dry powder amount obtained by leaflet red sandalwood timber is 75g, color fastness after the dyestuff colouring that dry powder is formed
About 2-3 grades.
Embodiment two
A kind of extracting method of narra bronzing vegetable colour, includes the following steps:
Step 1, it crushes: taking leaflet narra 1kg, be ground into wood powder with pulverizer；
Step 2, steaming: wood powder is placed in 460 DEG C of high energy steam boxs and steams 35min, to soften wood powder；
Step 3, separate: the wood powder after softening is fitted into immediately in 200 mesh stainless steel mesh bags, is put into 2kg, in 100 DEG C of water, is added
12g ethyl alcohol carries out separation 35min with 380MHz ultrasonic tank；
Step 4, fixation: after seeing water colour from shallow to deep, picking up mesh bag, add resin glue 45g, still keep 100 DEG C of boiling 22min,
Obtain red ecological vegetable liquid dyes；
Step 5, solid-state: the red ecological vegetable liquid dyes of gained in step 4, first with 400 mesh plate compressions to aqueous 23%, then
7min is toasted with the hot air drier that baking temperature is 190 DEG C, red ecological vegetable liquid dyes are roasted into dry block, are finally crushed
At dry powder.
Bronzing vegetable colour dry powder amount obtained by leaflet red sandalwood timber is 87g, color fastness after the dyestuff colouring that dry powder is formed
About 2-3 grades.
Embodiment three
A kind of extracting method of narra bronzing vegetable colour, includes the following steps:
Step 1, it crushes: taking leaflet narra 1kg, be ground into wood powder with pulverizer；
Step 2, steaming: wood powder is placed in 480 DEG C of high energy steam boxs and steams 40min, to soften wood powder；
Step 3, separate: the wood powder after softening is fitted into immediately in 200 mesh stainless steel mesh bags, is put into 2kg, in 100 DEG C of water, is added
15g ethyl alcohol carries out separation 40min with 430MHz ultrasonic tank；
Step 4, fixation: after seeing water colour from shallow to deep, picking up mesh bag, add resin glue 50g, still keep 100 DEG C of boiling 25min,
Obtain red ecological vegetable liquid dyes；
Step 5, solid-state: the red ecological vegetable liquid dyes of gained in step 4, first with 400 mesh plate compressions to aqueous 26%, then
10min is toasted with the hot air drier that baking temperature is 200 DEG C, red ecological vegetable liquid dyes are roasted into dry block, final powder
It is broken into dry powder.
Bronzing vegetable colour dry powder amount obtained by leaflet red sandalwood timber is 92g, color fastness after the dyestuff colouring that dry powder is formed
About 1-2 grades.
Example IV
A kind of extracting method of narra bronzing vegetable colour, includes the following steps:
Step 1, it crushes: taking leaflet narra 1kg, be ground into wood powder with pulverizer；
Step 2, steaming: wood powder is placed in 490 DEG C of high energy steam boxs and steams 45min, to soften wood powder；
Step 3, separate: the wood powder after softening is fitted into immediately in 200 mesh stainless steel mesh bags, is put into 2kg, in 100 DEG C of water, is added
18g ethyl alcohol carries out separation 45min with 470MHz ultrasonic tank；
Step 4, fixation: after seeing water colour from shallow to deep, picking up mesh bag, add resin glue 52g, still keep 100 DEG C of boiling 28min,
Obtain red ecological vegetable liquid dyes；
Step 5, solid-state: the red ecological vegetable liquid dyes of gained in step 4, first with 400 mesh plate compressions to aqueous 28%, then
12min is toasted with the hot air drier that baking temperature is 210 DEG C, red ecological vegetable liquid dyes are roasted into dry block, final powder
It is broken into dry powder.
Bronzing vegetable colour dry powder amount obtained by leaflet red sandalwood timber is 83g, color fastness after the dyestuff colouring that dry powder is formed
About 1-2 grades.
Embodiment five
A kind of extracting method of narra bronzing vegetable colour, includes the following steps:
Step 1, it crushes: taking leaflet narra 1kg, be ground into wood powder with pulverizer；
Step 2, steaming: wood powder is placed in 500 DEG C of high energy steam boxs and steams 30-50min, to soften wood powder；
Step 3, separate: the wood powder after softening is fitted into immediately in 200 mesh stainless steel mesh bags, is put into 2kg, in 100 DEG C of water, is added
20g ethyl alcohol carries out separation 50min with 500MHz ultrasonic tank；
Step 4, fixation: after seeing water colour from shallow to deep, picking up mesh bag, add resin glue 55g, still keep 100 DEG C of boiling 30min,
Obtain red ecological vegetable liquid dyes；
Step 5, solid-state: the red ecological vegetable liquid dyes of gained in step 4, first with 400 mesh plate compressions to aqueous 30%, then
15min is toasted with the hot air drier that baking temperature is 220 DEG C, red ecological vegetable liquid dyes are roasted into dry block, final powder
It is broken into dry powder.
Bronzing vegetable colour dry powder amount obtained by leaflet red sandalwood timber is 71g, color fastness after the dyestuff colouring that dry powder is formed
About 1 grade.
Foundation embodiment described above is enlightenment, and through the above description, relevant staff completely can be not
In the range of deviateing this invention thought, various changes and amendments are carried out.The technical scope of this invention is not limited to
In the content on specification, it is necessary to according to scope of the claims come the range of its fixed protection.
Claims (5)
1. a kind of extracting method of narra bronzing vegetable colour, characterized by the following steps:
Step 1, it crushes: taking leaflet narra 1kg, be ground into wood powder with pulverizer；
Step 2, steaming: wood powder is placed in steaming 30-50min in high energy steam box, to soften wood powder；
Step 3, it separates: the wood powder after softening is fitted into immediately in 200 mesh stainless steel mesh bags and is put into 2kg boiling water, is being added
After ethyl alcohol, separation 30-50min is carried out with ultrasonic tank；
Step 4, fixation: after observing water colour from shallow to deep, picking up mesh bag, adds resin glue, and use boiling water boiling 20-30min, obtains red
Color ecological vegetable liquid dyes；
Step 5, solid-state: the red ecological vegetable liquid dyes of gained in step 4 first use 400 mesh plate and frame filter press filters pressings, then with steaming
Gas dryer toasts 5-15min, and red ecological vegetable liquid dyes are roasted into dry block, finally smashing into dry powder.
2. a kind of extracting method of narra bronzing vegetable colour according to claim 1, it is characterised in that: step 2
High energy steamer temperature be 450-550 DEG C.
3. a kind of extracting method of narra bronzing vegetable colour according to claim 1, it is characterised in that: step 3
Middle amount of alcohol added is 10-20g, and ultrasonic tank audio electrical signal is 350-500MHz.
4. a kind of extracting method of narra bronzing vegetable colour according to claim 1, it is characterised in that: step 4
The additional amount of middle rouge glue is 45-55g.
5. a kind of extracting method of narra bronzing vegetable colour according to claim 1, it is characterised in that: step 5
The aqueous 20-30% of filter cake after middle plate and frame filter press filters pressing, hot air drier baking temperature are 180-220 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910006651.4A CN109575634A (en) | 2019-01-04 | 2019-01-04 | A kind of extracting method of narra bronzing vegetable colour |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910006651.4A CN109575634A (en) | 2019-01-04 | 2019-01-04 | A kind of extracting method of narra bronzing vegetable colour |
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| Publication Number | Publication Date |
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| CN109575634A true CN109575634A (en) | 2019-04-05 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201910006651.4A Pending CN109575634A (en) | 2019-01-04 | 2019-01-04 | A kind of extracting method of narra bronzing vegetable colour |
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Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104479398A (en) * | 2014-12-16 | 2015-04-01 | 常州美胜生物材料有限公司 | Pterocarpus santalinus extract and preparation method and application thereof |
-
2019
- 2019-01-04 CN CN201910006651.4A patent/CN109575634A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104479398A (en) * | 2014-12-16 | 2015-04-01 | 常州美胜生物材料有限公司 | Pterocarpus santalinus extract and preparation method and application thereof |
Non-Patent Citations (1)
| Title |
|---|
| M .L .GULRAJANI等: "《紫檀木染料染色的动力学和热力学研究》", 《国外纺织技术》 * |
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Application publication date: 20190405 |
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