CN104473778A - Quantitative spherical system and preparation method thereof - Google Patents
Quantitative spherical system and preparation method thereof Download PDFInfo
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- CN104473778A CN104473778A CN201410707978.1A CN201410707978A CN104473778A CN 104473778 A CN104473778 A CN 104473778A CN 201410707978 A CN201410707978 A CN 201410707978A CN 104473778 A CN104473778 A CN 104473778A
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Abstract
The invention relates to the field of daily chemicals, particularly a quantitative spherical system and a preparation method thereof. The quantitative spherical system structure is composed of 1-10mm circular microspheres, and comprises a base and an addition body. The base comprises an emulsion system or toothpaste. The addition body comprises agar and/or gellan gum and/or sodium alginate and/or carbomer and/or xanthan gum. The preparation method comprises the following steps: proportioning: preparing the following components in parts by weight: 90-95 parts of emulsion system or toothpaste, and 0.1-2 parts of agar and/or 0.1-2 parts of gellan gum and/or 0.1-2 parts of sodium alginate and/or 0.1-5 parts of carbomer and/or 0.1-5 parts of xanthan gum; heating: adding the 0.1-2 parts of agar and/or 0.1-2 parts of gellan gum and/or 0.1-2 parts of sodium alginate and/or 0.1-5 parts of carbomer and/or 0.1-5 parts of xanthan gum into the emulsion system or toothpaste, and heating to 60-90 DEG C to form a mobile liquid; and pill dropping: dropwisely adding -10-10 DEG C silicon oil, pure water or liquid calcium chloride into the mobile liquid, and preparing the quantitative spherical system with the diameter of 1-10mm. The quantitative spherical system is uniform in formation and convenient and comfortable to use.
Description
Technical field
The present invention relates to household chemicals field, particularly relate to a kind of quantitative spherical system and preparation method thereof.
Background technology
The product forms of current emulsified cosmetics, toothpaste is all homogeneous mastic, uses product, cannot reach effect that is quantitative, health by squeezing tube or with stingy the digging of finger.
CN101240076B (2011-9-14) discloses a kind of macromole and emulsion mackle note alginate polymer micro-sphere, and preparation method is: (1) preparation sodium alginate/ovalbumin complex solution; (2) solution of hydroxyethyl-cellulose deionized water solution with step (1) is mixed; (3) add liquid paraffin and emulsifying agent mixed liquor, stir to obtain emulsion; (4) by emulsion dispersion containing in organic oil phase of dispersant, add polyvinyl pyrrolidone aqueous solution, add calcium chloride water and be cross-linked into microsphere, rinse, microsphere is placed on glutaraldehyde water solution and is cross-linked; Soak with alcoholic solution, ether, obtain with ovalbumin in Tri(Hydroxymethyl) Amino Methane Hydrochloride buffer solution elution microsphere.But the method is shaped complicated, and it is uneven to be shaped.
Summary of the invention
An object of the present invention is to provide a kind of comfortable quantitative spherical system even, easy to use that is shaped.
Two of object of the present invention is to provide a kind of preparation method of the comfortable quantitative spherical system even, easy to use that is shaped.
First technical purpose of the present invention is achieved by the following technical programs:
A kind of quantitative spherical system, structure is the circular microsphere of 1-10mm, comprises matrix and adds body;
Described matrix comprises emulsification system or toothpaste 90-95 part by weight;
Described interpolation body comprises agar 0.1-2 part and/or gellan gum 0.1-2 part and/or sodium alginate 0.1-2 part and/or carbomer 0.1-5 part and/or xanthan gum 0.1-5 part by weight.
Quantitative spherical system of the present invention novelty attractive in appearance, makes product more have market difference degree; In preservation process, can air be completely cut off, keep active enduringly.In use, can be broken smoothly, discharge the active matter in matrix.
As preferably, described emulsification system is Water-In-Oil, oil-in-water or silicon water-in-oil system.
More preferably, described Water-In-Oil comprises oil phase component, water phase components, solid particle and surfactant;
Described oil phase component comprises oils and fats and antioxidant; Described water phase components comprises distilled water and wetting agent;
Described solid particle comprise in titanium dioxide, silicon dioxide or calcium carbonate one or more.
Further preferably, described surfactant is one or more in polyoxyethylene sorbitan sorbic alcohol fatty acid ester, glycerine monofatty ester or sucrose monostearate.
As preferably, described interpolation body also comprises pigment 0.1-0.5 weight portion.
Second technical purpose of the present invention is achieved by the following technical programs:
A preparation method for quantitative spherical system, comprises the following steps successively:
(1) prepare burden: prepare emulsification system or toothpaste 90-95 part by weight; Agar 0.1-2 part and/or gellan gum 0.1-2 part and/or sodium alginate 0.1-2 part and/or carbomer 0.1-5 part and/or xanthan gum 0.1-5 part;
(2) heat: in described emulsification system or toothpaste, add described agar 0.1-2 part and/or gellan gum 0.1-2 part and/or sodium alginate 0.1-2 part and/or carbomer 0.1-5 part and/or xanthan gum 0.1-5 part; Be heated to 60-90 DEG C to forming mobility liquid;
(3) drop pill: instill the silicone oil of-10-10 DEG C, pure water or liquid calcium chloride in described mobility liquid, then obtain the quantitative spherical system of uniform diameter 1-10mm with solid drop pill machine.
The present invention selects the material post-heating adding certain content in described emulsification system or toothpaste, then instills predetermined substance, makes the quantitative spherical system of homogeneous diameter, make product more have market difference degree, environmentally-friendly sanitary; In preservation process, can air be completely cut off, keep active enduringly.In use, can be broken smoothly, discharge the active matter in matrix.
As preferably, the calcium chloride content in described liquid calcium chloride is 0.1-2wt%.
As preferably, the mass ratio of the silicone oil, pure water or the liquid calcium chloride that instill during described step (3) drop pill and described mobility liquid is 1-2.
As preferably, in described step (2) heating process, add 0.5-0.8 part anion powder; Described anion powder is made up of following components in mass portion: gull rock 15-20 part; Tourmaline 5-10 part; Opal 30-35 part; Serpentine 2-6 part; Maifanitum 4-6 part; Rare ice stone 4-6 part; Hokutolite 1-2 part; Doctor Wang Shi 5-7 part; Shell 1-3 part; Kieselguhr 12-18 part; Zirconium oxide 5-8 part; Zirconium phosphate 4-6 part.
Anion powder of the present invention has good electronegative ion, completely cuts off air for improving again it in spherical system further and keeps activity, in use smooth fragmentation enduringly and discharge base activated performance in preservation process.
More preferably, the preparation of described anion powder is by described gull rock, tourmaline, opal, serpentine, Maifanitum, rare ice stone, hokutolite, doctor Wang Shi, shell, kieselguhr, zirconium oxide and zirconium phosphate mix homogeneously, superfine grinding to grain diameter is 15-30nm, sieve, microwave treatment, microwave frequency is 500 ~ 650MHz, and microwave treatment time is 1 ~ 3min.
In sum, the present invention has following beneficial effect: the present invention selects the material post-heating adding certain content in described emulsification system or toothpaste, then instills predetermined substance, makes the quantitative spherical system of homogeneous diameter, product is made more to have market difference degree, environmentally-friendly sanitary; In preservation process, can air be completely cut off, keep active enduringly.In use, can be broken smoothly, discharge the active matter in matrix.
Detailed description of the invention
Embodiment one
Batching: prepare emulsification system or 90 parts, toothpaste by weight; 0.1 part, agar;
Heating: add agar in emulsification system; Be heated to 60 DEG C to forming mobility liquid;
Emulsification system is water-in-oil system.Water-in-oil system comprises oil phase component, water phase components, solid particle and surfactant; Oil phase component comprises oils and fats and antioxidant; Water phase components comprises distilled water and wetting agent; Solid particle comprise in titanium dioxide, silicon dioxide or calcium carbonate one or more.Surfactant is one or more in polyoxyethylene sorbitan sorbic alcohol fatty acid ester, glycerine monofatty ester or sucrose monostearate.
Drop pill: the silicone oil instilling-10 DEG C in mobility liquid, then obtains the quantitative spherical system of uniform diameter 1mm with solid drop pill machine.The mass ratio of the silicone oil instilled during drop pill, pure water or liquid calcium chloride and mobility liquid is 1.
Embodiment two
Batching: prepare emulsification system or 95 parts, toothpaste by weight; 2 parts, agar and gellan gum 2 parts and sodium alginate 0.1 part;
Heating: add agar, gellan gum and sodium alginate in emulsification system; Be heated to 90 DEG C to forming mobility liquid; Emulsification system is oil-in-water system;
0.5 part of anion powder is added in heating process;
The preparation method of anion powder is by gull rock 18 parts; Tourmaline 8 parts; 32 parts, opal; Serpentine 4 parts; Maifanitum 5 parts; Rare ice stone 5 parts; Hokutolite 1.2 parts; Doctor Wang Shi 6 parts; 2 parts, shell; 16 parts, kieselguhr; Zirconium oxide 7 parts; Zirconium phosphate 5 parts of mix homogeneously, superfine grinding is 20nm to grain diameter, sieves, microwave treatment, and microwave frequency is 550MHz, and microwave treatment time is 2min.
Drop pill: the pure water dripping 2 DEG C in mobility liquid, then obtains the quantitative spherical system of uniform diameter 10mm with solid drop pill machine.The mass ratio of the silicone oil instilled during drop pill, pure water or liquid calcium chloride and mobility liquid is 2.
Embodiment three
Batching: prepare 90 parts, toothpaste by weight; Xanthan gum 5 parts;
Heating: add xanthan gum in toothpaste; Be heated to 80 DEG C to forming mobility liquid;
0.8 part of anion powder is added in heating process;
The preparation method of anion powder is by gull rock 15 parts; Tourmaline 5 parts; 30 parts, opal; Serpentine 2 parts; Maifanitum 4 parts; Rare ice stone 4 parts; Hokutolite 1 part; Doctor Wang Shi 5 parts; 1 part, shell; 12 parts, kieselguhr; Zirconium oxide 5 parts; Zirconium phosphate 6 parts of mix homogeneously, superfine grinding is 15nm to grain diameter, sieves, microwave treatment, and microwave frequency is 500MHz, and microwave treatment time is 1min.
Drop pill: the liquid calcium chloride instilling-10 DEG C in mobility liquid, then obtains the quantitative spherical system of uniform diameter 6mm with solid drop pill machine.The mass ratio of the liquid calcium chloride instilled during drop pill and mobility liquid is 1.5, and the calcium chloride content in liquid calcium chloride is 0.1wt%.
Embodiment four
With embodiment one, unlike batching: prepare emulsification system 92 parts by weight; 2 parts, agar and gellan gum 0.1 part and sodium alginate 0.1 part and carbomer 0.1 part and xanthan gum 0.1 part.Emulsification system is oil-in-water system.
0.7 part of anion powder and pigment 0.1-0.5 weight portion is added in heating process;
The preparation method of anion powder is by gull rock 20 parts; Tourmaline 10 parts; 35 parts, opal; Serpentine 6 parts; Maifanitum 6 parts; Rare ice stone 6 parts; Hokutolite 2 parts; Doctor Wang Shi 7 parts; 3 parts, shell; 18 parts, kieselguhr; Zirconium oxide 8 parts; Zirconium phosphate 4 parts of mix homogeneously, superfine grinding is 30nm to grain diameter, sieves, microwave treatment, and microwave frequency is 650MHz, and microwave treatment time is 3min.
Drop pill: the liquid calcium chloride instilling 10 DEG C in mobility liquid, the calcium chloride content in liquid calcium chloride is 2wt%.Then the quantitative spherical system of uniform diameter 10mm is obtained with solid drop pill machine.
Comparative example one
With embodiment one, only comprise matrix emulsification system or toothpaste unlike batching, do not comprise any one of adding in body agar or gellan gum or sodium alginate or carbomer or xanthan gum.
Comparative example two
With embodiment two, be starch or dextrin unlike the interpolation body in batching; Heating-up temperature is 50 DEG C.
Comparative example three
With embodiment three, be the magnesium chloride liquid of 20 DEG C unlike what instill in drop pill process.
Table 1 embodiment and comparative example's properties of product evaluating and test experience
This specific embodiment is only explanation of the invention; it is not limitation of the present invention; those skilled in the art can make to the present embodiment the amendment not having creative contribution as required after reading this description, as long as but be all subject to the protection of Patent Law in right of the present invention.
Claims (10)
1. a quantitative spherical system, is characterized in that: structure is the circular microsphere of 1-10mm, comprises matrix and adds body;
Described matrix comprises emulsification system or toothpaste 90-95 part by weight;
Described interpolation body comprises agar 0.1-2 part and/or gellan gum 0.1-2 part and/or sodium alginate 0.1-2 part and/or carbomer 0.1-5 part and/or xanthan gum 0.1-5 part by weight.
2. the quantitative spherical system of one according to claim 1, is characterized in that: a kind of quantitative spherical system, is characterized in that: described emulsification system is Water-In-Oil, oil-in-water or silicon water-in-oil system.
3. the quantitative spherical system of one according to claim 2, is characterized in that: described Water-In-Oil comprises oil phase component, water phase components, solid particle and surfactant;
Described oil phase component comprises oils and fats and antioxidant; Described water phase components comprises distilled water and wetting agent;
Described solid particle comprise in titanium dioxide, silicon dioxide or calcium carbonate one or more.
4. the quantitative spherical system of one according to claim 3, is characterized in that: described surfactant is one or more in polyoxyethylene sorbitan sorbic alcohol fatty acid ester, glycerine monofatty ester or sucrose monostearate.
5. the quantitative spherical system of one according to claim 4, is characterized in that: described interpolation body also comprises pigment 0.1-0.5 weight portion.
6. a preparation method for quantitative spherical system, is characterized in that comprising the following steps successively:
(1) prepare burden: prepare emulsification system or toothpaste 90-95 part by weight; Agar 0.1-2 part and/or gellan gum 0.1-2 part and/or sodium alginate 0.1-2 part and/or carbomer 0.1-5 part and/or xanthan gum 0.1-5 part;
(2) heat: in described emulsification system or toothpaste, add described agar 0.1-2 part and/or gellan gum 0.1-2 part and/or sodium alginate 0.1-2 part and/or carbomer 0.1-5 part and/or xanthan gum 0.1-5 part; Be heated to 60-90 DEG C to forming mobility liquid;
(3) drop pill: instill the silicone oil of-10-10 DEG C, pure water or liquid calcium chloride in described mobility liquid, then obtain the quantitative spherical system of uniform diameter 1-10mm with solid drop pill machine.
7. the preparation method of a kind of quantitative spherical system according to claim 6, is characterized in that: the calcium chloride content in described liquid calcium chloride is 0.1-2wt%.
8. the preparation method of a kind of quantitative spherical system according to claim 7, is characterized in that: the mass ratio of the silicone oil, pure water or the liquid calcium chloride that instill during described step (3) drop pill and described mobility liquid is 1-2.
9. the preparation method of a kind of quantitative spherical system according to claim 8, is characterized in that: add 0.5-0.8 part anion powder in described step (2) heating process; Described anion powder is made up of following components in mass portion: gull rock 15-20 part; Tourmaline 5-10 part; Opal 30-35 part; Serpentine 2-6 part; Maifanitum 4-6 part; Rare ice stone 4-6 part; Hokutolite 1-2 part; Doctor Wang Shi 5-7 part; Shell 1-3 part; Kieselguhr 12-18 part; Zirconium oxide 5-8 part; Zirconium phosphate 4-6 part.
10. the preparation method of a kind of quantitative spherical system according to claim 9, it is characterized in that: the preparation of described anion powder is by described gull rock, tourmaline, opal, serpentine, Maifanitum, rare ice stone, hokutolite, doctor Wang Shi, shell, kieselguhr, zirconium oxide and zirconium phosphate mix homogeneously, superfine grinding to grain diameter is 15-30nm, sieve, microwave treatment, microwave frequency is 500 ~ 650MHz, and microwave treatment time is 1 ~ 3min.
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| CN201410707978.1A CN104473778A (en) | 2014-12-01 | 2014-12-01 | Quantitative spherical system and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105456041A (en) * | 2015-12-11 | 2016-04-06 | 广州薇美姿实业有限公司 | Toothpaste containing particles and transparent viscous substance |
| CN108066165A (en) * | 2017-12-22 | 2018-05-25 | 江山 | A kind of toothpaste particle and preparation method thereof and the application in toothpaste |
| CN113069405A (en) * | 2021-04-27 | 2021-07-06 | 广州优妥生物科技有限公司 | Antibacterial toothpaste for relieving oral ulcer and preparation method thereof |
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| US20100272834A1 (en) * | 2009-04-22 | 2010-10-28 | Dr. Suwelack Skin & Health Care Ag | Freeze-Dried Molded Article Containing Magnesium Ascorbyl Phosphate |
| CN104056017A (en) * | 2014-06-16 | 2014-09-24 | 万伦 | Traditional Chinese medicine composition for treating rheumatism and preparation method thereof |
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2014
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|---|---|---|---|---|
| US20100272834A1 (en) * | 2009-04-22 | 2010-10-28 | Dr. Suwelack Skin & Health Care Ag | Freeze-Dried Molded Article Containing Magnesium Ascorbyl Phosphate |
| CN104056017A (en) * | 2014-06-16 | 2014-09-24 | 万伦 | Traditional Chinese medicine composition for treating rheumatism and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105456041A (en) * | 2015-12-11 | 2016-04-06 | 广州薇美姿实业有限公司 | Toothpaste containing particles and transparent viscous substance |
| CN105456041B (en) * | 2015-12-11 | 2021-01-15 | 广州舒客实业有限公司 | Toothpaste containing particles and transparent viscous object |
| CN108066165A (en) * | 2017-12-22 | 2018-05-25 | 江山 | A kind of toothpaste particle and preparation method thereof and the application in toothpaste |
| CN113069405A (en) * | 2021-04-27 | 2021-07-06 | 广州优妥生物科技有限公司 | Antibacterial toothpaste for relieving oral ulcer and preparation method thereof |
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