CN104470882B - 生产氟代芳族化合物的方法 - Google Patents

生产氟代芳族化合物的方法 Download PDF

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Publication number
CN104470882B
CN104470882B CN201380036738.7A CN201380036738A CN104470882B CN 104470882 B CN104470882 B CN 104470882B CN 201380036738 A CN201380036738 A CN 201380036738A CN 104470882 B CN104470882 B CN 104470882B
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China
Prior art keywords
amino
formula
methyl
ethyl
process according
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Expired - Fee Related
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CN201380036738.7A
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English (en)
Chinese (zh)
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CN104470882A (zh
Inventor
M·拉克
M·多奇纳赫勒
V·迈瓦尔德
B·沃尔夫
J·格布哈特
T·弗拉塞托
U·J·福格尔巴赫
R·格策
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/62—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by introduction of halogen; by substitution of halogen atoms by other halogen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/35—Preparation of halogenated hydrocarbons by reactions not affecting the number of carbon or of halogen atoms in the reaction
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/68—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton
    • C07C209/74—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton by halogenation, hydrohalogenation, dehalogenation, or dehydrohalogenation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C245/00—Compounds containing chains of at least two nitrogen atoms with at least one nitrogen-to-nitrogen multiple bond
    • C07C245/20—Diazonium compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
    • C07C37/74—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C07C37/76—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by distillation by steam distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/18—Preparation of ethers by reactions not forming ether-oxygen bonds
    • C07C41/22—Preparation of ethers by reactions not forming ether-oxygen bonds by introduction of halogens; by substitution of halogen atoms by other halogen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/347—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups
    • C07C51/363—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups by introduction of halogen; by substitution of halogen atoms by other halogen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/72—Nitrogen atoms
    • C07D213/73—Unsubstituted amino or imino radicals

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN201380036738.7A 2012-07-18 2013-07-08 生产氟代芳族化合物的方法 Expired - Fee Related CN104470882B (zh)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US201261672787P 2012-07-18 2012-07-18
EP12176859 2012-07-18
US61/672,787 2012-07-18
EP12176859.2 2012-07-18
PCT/EP2013/064361 WO2014012811A1 (en) 2012-07-18 2013-07-08 Process for manufacturing fluoroaromatics

Publications (2)

Publication Number Publication Date
CN104470882A CN104470882A (zh) 2015-03-25
CN104470882B true CN104470882B (zh) 2017-03-29

Family

ID=49948309

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CN201380036738.7A Expired - Fee Related CN104470882B (zh) 2012-07-18 2013-07-08 生产氟代芳族化合物的方法

Country Status (5)

Country Link
US (1) US9126905B2 (enExample)
CN (1) CN104470882B (enExample)
AR (1) AR091828A1 (enExample)
IN (1) IN2015DN00714A (enExample)
WO (1) WO2014012811A1 (enExample)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20160105815A (ko) 2013-12-18 2016-09-07 바스프 아그로 비.브이. 치환 페녹시페닐 케톤의 제조 방법
CN106232604A (zh) 2014-04-17 2016-12-14 巴斯夫欧洲公司 具有除草活性的取代吡啶化合物
US10053436B2 (en) 2014-07-08 2018-08-21 BASF Agro B.V. Process for the preparation of substituted oxiranes and triazoles
CN105753631B (zh) * 2014-12-15 2018-11-02 沈阳化工研究院有限公司 一种含氟芳香族化合物的合成方法
DK3294700T3 (da) 2015-05-08 2020-04-14 Basf Agro Bv Fremgangsmåde til fremstilling af limonen-4-ol
WO2016180642A1 (en) 2015-05-08 2016-11-17 BASF Agro B.V. A process for the preparation of terpinolene epoxide
MX2018015764A (es) 2016-06-15 2019-08-29 Basf Agro Bv Proceso para la epoxidacion de un alqueno tetrasustituido.
AU2017284971B2 (en) 2016-06-15 2021-01-21 BASF Agro B.V. Process for the epoxidation of a tetrasubstituted alkene
CN112110790B (zh) * 2020-09-28 2023-06-23 台州臻挚生物科技有限公司 一种3,5-二卤三氟甲苯及3`-氯-5`-(三氟甲基)苯基三氟乙酮的制备方法
CN116751103A (zh) * 2022-09-16 2023-09-15 山东东岳高分子材料有限公司 一种制备电子级氟苯的方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1832906A (zh) * 2003-06-07 2006-09-13 艾夫西亚药品有限公司 芳基重氮盐的制备方法及其与亲核体的反应

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2563796A (en) 1948-05-26 1951-08-07 Harshaw Chem Corp Manufacture of aromatic diazonium fluorides and corresponding aromatic fluorides
FR1310192A (enExample) 1960-12-23 1963-03-06
DE3577704D1 (de) * 1984-10-10 1990-06-21 Ciba Geigy Ag Verfahren zur herstellung von fluorierten pyridin-derivaten.
GB8619375D0 (en) * 1986-08-08 1986-09-17 Ici Plc Chemical process
US4886920A (en) * 1987-04-06 1989-12-12 Mallinckrodt, Inc. Process for preparing aromatic fluorides
US4912268A (en) * 1988-02-26 1990-03-27 E. I. Du Pont De Nemours And Company Process for manufacture of fluoroaromatics
US5107046A (en) * 1990-05-23 1992-04-21 Mallinckrodt Specialty Chemicals Co., Inc. Process for preparing aromatic fluorides
GB9609154D0 (en) * 1996-05-01 1996-07-03 Rhone Poulenc Chemicals Process for the preparation of fluoro compounds from the corresponding amines

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1832906A (zh) * 2003-06-07 2006-09-13 艾夫西亚药品有限公司 芳基重氮盐的制备方法及其与亲核体的反应

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
Facile Preparation of Aromatic Fluorides by Deaminative Fluorination of Aminoarenes Using Hydrogen Fluoride Combined with Bases;Norihiko Yoneda，et al.;《Tetrahedron》;19961231;第52卷(第1期);第23-36页 *
芳香族氟化合物的合成研究;姜小明;《中国优秀硕士学位论文全文数据库 工程科技I辑》;20040915(第3期);第28页 *

Also Published As

Publication number Publication date
CN104470882A (zh) 2015-03-25
IN2015DN00714A (enExample) 2015-07-10
AR091828A1 (es) 2015-03-04
US9126905B2 (en) 2015-09-08
WO2014012811A1 (en) 2014-01-23
US20150166446A1 (en) 2015-06-18

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