CN104470879B - 用于生产甲基丁炔醇的方法 - Google Patents
用于生产甲基丁炔醇的方法 Download PDFInfo
- Publication number
- CN104470879B CN104470879B CN201380037175.3A CN201380037175A CN104470879B CN 104470879 B CN104470879 B CN 104470879B CN 201380037175 A CN201380037175 A CN 201380037175A CN 104470879 B CN104470879 B CN 104470879B
- Authority
- CN
- China
- Prior art keywords
- water
- feed composition
- methyl butynol
- pervaporation
- acetone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/36—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring increasing the number of carbon atoms by reactions with formation of hydroxy groups, which may occur via intermediates being derivatives of hydroxy, e.g. O-metal
- C07C29/38—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring increasing the number of carbon atoms by reactions with formation of hydroxy groups, which may occur via intermediates being derivatives of hydroxy, e.g. O-metal by reaction with aldehydes or ketones
- C07C29/42—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring increasing the number of carbon atoms by reactions with formation of hydroxy groups, which may occur via intermediates being derivatives of hydroxy, e.g. O-metal by reaction with aldehydes or ketones with compounds containing triple carbon-to-carbon bonds, e.g. with metal-alkynes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/36—Pervaporation; Membrane distillation; Liquid permeation
- B01D61/362—Pervaporation
- B01D61/3621—Pervaporation comprising multiple pervaporation steps
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
- C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C33/00—Unsaturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
- C07C33/04—Acyclic alcohols with carbon-to-carbon triple bonds
- C07C33/042—Acyclic alcohols with carbon-to-carbon triple bonds with only one triple bond
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2311/00—Details relating to membrane separation process operations and control
- B01D2311/26—Further operations combined with membrane separation processes
- B01D2311/2669—Distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2311/00—Details relating to membrane separation process operations and control
- B01D2311/26—Further operations combined with membrane separation processes
- B01D2311/2673—Evaporation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Water Supply & Treatment (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP12175996.3 | 2012-07-11 | ||
| EP12175996 | 2012-07-11 | ||
| PCT/EP2013/064651 WO2014009452A1 (en) | 2012-07-11 | 2013-07-11 | Process for the production of methylbutinol |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104470879A CN104470879A (zh) | 2015-03-25 |
| CN104470879B true CN104470879B (zh) | 2017-03-22 |
Family
ID=48782332
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201380037175.3A Active CN104470879B (zh) | 2012-07-11 | 2013-07-11 | 用于生产甲基丁炔醇的方法 |
Country Status (14)
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107827711B (zh) * | 2017-10-31 | 2023-09-29 | 西南化工研究设计院有限公司 | 一种联产甲基丁炔醇和二甲基己炔二醇的系统及工艺 |
| CN108299161B (zh) * | 2018-03-30 | 2020-05-19 | 西南化工研究设计院有限公司 | 一种脱除2-甲基-3-丁炔-2-醇中水的方法及夹带剂 |
| EP3908395B1 (en) * | 2019-01-09 | 2024-10-30 | SABIC Global Technologies B.V. | Dehydration of a mixture containing a diol with high water content using optimized pervaporation process |
| CN110317124A (zh) * | 2019-06-20 | 2019-10-11 | 袁玮 | 环保处理生产炔醇类产品产生的工业残渣和废焦油的工艺 |
| WO2022016317A1 (zh) * | 2020-07-20 | 2022-01-27 | 万华化学集团股份有限公司 | 一种2-甲基-3-丁炔-2-醇的分离方法 |
| CN111807929B (zh) * | 2020-07-20 | 2022-08-05 | 万华化学集团股份有限公司 | 一种2-甲基-3-丁炔-2-醇的分离方法 |
| CN114456039B (zh) * | 2021-12-10 | 2024-04-26 | 浙江天采云集科技股份有限公司 | 一种隔壁塔式异丙醇溶液分子筛膜精馏分离与净化方法 |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1023856A (en) * | 1962-09-04 | 1966-03-30 | Snam Spa | Method for purifying aqueous solutions of methylbutynol |
| EP0610775A1 (de) * | 1993-02-06 | 1994-08-17 | BASF Aktiengesellschaft | Verfahren zur Trennung von Flüssigkeitsgemischen mit azeotropem Siedeverhalten durch Verschaltung von Pervaporation und Destillation |
| CN1247181A (zh) * | 1999-08-25 | 2000-03-15 | 成都惟精防水材料研究所 | 2,5－二甲基－2,5－己二醇一步合成法 |
| DE102005037430A1 (de) * | 2005-08-04 | 2007-02-08 | Basf Ag | Enzymatische Herstellung von (Meth)acrylsäureestern |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1193496B (de) | 1962-09-04 | 1965-05-26 | Snam Spa | Verfahren zur Reinigung waessriger Loesungen von Methylbutinol, die durch Aceton ver-unreinigt sind |
| BE636431A (fr) * | 1962-09-04 | 1964-02-21 | Snam Spa | Procédé pour purifier les solutions aqueuses de méthylbutinol par élimination de l'acétone qu'elles contiennent |
| DE1768877B1 (de) * | 1968-07-10 | 1971-08-26 | Basf Ag | Verfahren zur kontinuierlichen Herstellung von Acetylenalkoholen |
| KR100277722B1 (ko) * | 1998-08-26 | 2001-02-01 | 남창우 | 연속 공정을 이용한 아세틸렌 알코올 화합물의 제조방법 |
| JP2009275019A (ja) * | 2008-05-16 | 2009-11-26 | Nippon Shokubai Co Ltd | 水−アルコール組成物の精製方法 |
-
2013
- 2013-07-11 EA EA201500116A patent/EA026542B1/ru not_active IP Right Cessation
- 2013-07-11 IN IN10741DEN2014 patent/IN2014DN10741A/en unknown
- 2013-07-11 EP EP13735284.5A patent/EP2872473B1/en active Active
- 2013-07-11 SG SG11201408260RA patent/SG11201408260RA/en unknown
- 2013-07-11 US US14/407,144 patent/US9284243B2/en active Active
- 2013-07-11 CN CN201380037175.3A patent/CN104470879B/zh active Active
- 2013-07-11 WO PCT/EP2013/064651 patent/WO2014009452A1/en active Application Filing
- 2013-07-11 CA CA2876281A patent/CA2876281C/en active Active
- 2013-07-11 MX MX2015000401A patent/MX2015000401A/es unknown
- 2013-07-11 KR KR20157003589A patent/KR20150036530A/ko not_active Withdrawn
- 2013-07-11 JP JP2015520985A patent/JP6284933B2/ja active Active
- 2013-07-11 AU AU2013288761A patent/AU2013288761B2/en not_active Ceased
- 2013-07-11 BR BR112015000322A patent/BR112015000322A2/pt not_active IP Right Cessation
-
2014
- 2014-12-10 IL IL236159A patent/IL236159A/en not_active IP Right Cessation
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1023856A (en) * | 1962-09-04 | 1966-03-30 | Snam Spa | Method for purifying aqueous solutions of methylbutynol |
| EP0610775A1 (de) * | 1993-02-06 | 1994-08-17 | BASF Aktiengesellschaft | Verfahren zur Trennung von Flüssigkeitsgemischen mit azeotropem Siedeverhalten durch Verschaltung von Pervaporation und Destillation |
| CN1247181A (zh) * | 1999-08-25 | 2000-03-15 | 成都惟精防水材料研究所 | 2,5－二甲基－2,5－己二醇一步合成法 |
| DE102005037430A1 (de) * | 2005-08-04 | 2007-02-08 | Basf Ag | Enzymatische Herstellung von (Meth)acrylsäureestern |
Also Published As
| Publication number | Publication date |
|---|---|
| JP6284933B2 (ja) | 2018-02-28 |
| EP2872473A1 (en) | 2015-05-20 |
| EA201500116A1 (ru) | 2015-06-30 |
| US9284243B2 (en) | 2016-03-15 |
| HK1205097A1 (en) | 2015-12-11 |
| US20150141709A1 (en) | 2015-05-21 |
| EA026542B1 (ru) | 2017-04-28 |
| BR112015000322A2 (pt) | 2017-06-27 |
| EP2872473B1 (en) | 2017-03-01 |
| AU2013288761B2 (en) | 2017-08-31 |
| KR20150036530A (ko) | 2015-04-07 |
| IL236159A0 (en) | 2015-02-01 |
| SG11201408260RA (en) | 2015-01-29 |
| WO2014009452A1 (en) | 2014-01-16 |
| AU2013288761A1 (en) | 2015-01-22 |
| CA2876281A1 (en) | 2014-01-16 |
| IN2014DN10741A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 2015-09-04 |
| CN104470879A (zh) | 2015-03-25 |
| JP2015528800A (ja) | 2015-10-01 |
| MX2015000401A (es) | 2015-03-12 |
| IL236159A (en) | 2017-03-30 |
| CA2876281C (en) | 2020-07-21 |
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Effective date of registration: 20200810 Address after: Swiss Fisp Patentee after: Longsha solutions Inc Address before: Swiss Fisp Patentee before: LONZA Ltd. |
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| CP01 | Change in the name or title of a patent holder | ||
| CP01 | Change in the name or title of a patent holder |
Address after: Swiss Fisp Patentee after: Alsada AG Address before: Swiss Fisp Patentee before: Longsha solutions Inc. |