CN104434675A - Traditional Chinese medicine toothpaste and preparation method thereof - Google Patents

Traditional Chinese medicine toothpaste and preparation method thereof Download PDF

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Publication number
CN104434675A
CN104434675A CN201410726403.4A CN201410726403A CN104434675A CN 104434675 A CN104434675 A CN 104434675A CN 201410726403 A CN201410726403 A CN 201410726403A CN 104434675 A CN104434675 A CN 104434675A
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China
Prior art keywords
parts
chinese medicinal
preparation
formula ratio
antiseptic
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CN201410726403.4A
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Chinese (zh)
Inventor
张一帆
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Chengdu Jinhui Technology Co Ltd
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Chengdu Jinhui Technology Co Ltd
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Priority to CN201410726403.4A priority Critical patent/CN104434675A/en
Publication of CN104434675A publication Critical patent/CN104434675A/en
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Abstract

The invention discloses a piece of traditional Chinese medicine toothpaste and a preparation method thereof. The Chinese traditional medicine toothpaste comprises the following components in parts by weight: 0.01-0.08 part of cogongrass rhizome, 20-40 parts of calcium phosphate, 3-6 parts of lanthanum chloride, 3-6 parts of colloidal silica, 0.5-2 parts of hydroxyethylcellulose, 2-7 parts of pagodatree juvenile branchlet, 0.05-0.2 part of saccharin, 30-60 parts of water, 2-10 parts of mint clove and 0.01-0.08 part of antiseptic. The traditional Chinese medicine toothpaste obtained according to the preparation method not only has good dental plaque removal effect and effectively avoids gum inflammation, but also has light taste of Chinese traditional medicines, the preparation method is simple, and the production cost is low.

Description

A kind of Chinese medicinal toothpaste and preparation method thereof
Technical field
The present invention relates to a kind of toothpaste, more particularly, the present invention relates to a kind of Chinese medicinal toothpaste and preparation method thereof.
Background technology
Toothpaste commonly uses in people's daily life, and improved being formed by dentifrice, early stage dentifrice mainly uses calcium carbonate to be surfactant as abrasivus, with soap.Along with developing rapidly of science and technology, toothpaste industry also obtains very large improvement, is the development and application of new abrasivus, wetting agent, thickening agent and surfactant on the one hand, tooth paste product quality is constantly upgraded; On the other hand, toothpaste also from the common function development that cleans the teeth be add medicine become the dental care product preventing and treating odontopathy, the most outstanding is add fluorine toothpaste, and dental caries sickness rate is greatly reduced.The tooth that a bite is firm, pure and fresh implication, everybody wants to have.But enter the manhood, the sickness rate of periodontal rises gradually, and with advancing age, its order of severity is also constantly deepened.Protection gingiva, periodontal tissue, seem more urgent for adult.Part Chinese herbal toothpaste really can play the effect of general protection tooth, gingiva, periodontal tissue.Such as, mica filled polypropylene, it can prevent gingival hemorrhage rapidly, the oral problem such as prevention of gingivitis, periodontitis, gingival atrophy.Certainly, this depends on the active component of YUNNAN BAIYAO in toothpaste, effectively can improve the blood circulation of gingiva, periodontal tissue and oral mucosa, improve the supply of periodontal tissue and oral cavity mucous membrane tissue nutrient, strengthen the resistance against diseases of gingiva, periodontal, tooth and oral mucosa.In addition, after brushing teeth or gargling, suitably gum massage, can make epithelium keratinization strengthen, and strengthens the blood circulation of gingiva tissue, promotes the health of gingiva tissue.Even if toothpaste has so many purposes, but the most people pay attention to or toothpaste to the protection of tooth with in oral hygiene aspect.Due to a lot of people like smoke, so the easy long teeth speckle of tooth, affect teeth whitening attractive in appearance while, also oral hygiene is worked the mischief.Toothpaste is of a great variety on the market, the toothpaste of Chinese herbal medicine also along with its outstanding pharmacological action by people are accepted.But still there is the taste of the uncomfortable Chinese herbal toothpaste of part population.Increasing people likes having fragranced and the good toothpaste of cleaning benefits, especially likes the toothpaste with mint flavored.
Publication number is CN 101467949, and publication date is that the Chinese patent literature of on 07 01st, 2009 discloses a kind of biological product toothpaste, this biological product toothpaste with containing multiple medicinal herb components for feature, multiple Chinese herbal medicine is made through certain technique.Although Chinese herbal toothpaste has heat clearing away drive expectorant, hard masses softening and resolving, effect of eliminating inflammation and expelling toxin, its Chinese herbal medicine flavour of a drug are heavier, and frequent use can cause the discomfort of people to react.
Summary of the invention
In order to overcome the defect of above-mentioned prior art, the invention provides a kind of Chinese medicinal toothpaste and preparation method thereof, Chinese medicinal toothpaste disclosed by the invention not only goes dental plaque effective, effectively can avoid various focusing depths represented, and Chinese medicine is lightly seasoned, its preparation technology is simple, and production cost is low.
In order to realize foregoing invention object, the technical solution used in the present invention is as follows:
A kind of Chinese medicinal toothpaste, is characterized in that: the component comprising following parts by weight:
Rhizoma Imperatae 0.01-0.08 part
Calcium phosphate 20-40 part
Lanthanum chloride 3-6 part
Colloidal silica 3-6 part
Hydroxyethyl-cellulose 0.5-2 part
Rumalus sophorae 2-7 part
Glucide 0.05-0.2 part
Water 30-60 part
Thin Flos Caryophylli 2-10 part
Antiseptic 0.01-0.08 part.
Also comprise foaming agent, blowing agent composition weight number is 0.01-0.08 part.
Described foaming agent is tea saponin.
Described antiseptic is sorbic acid, potassium sorbate or calcium sorbate.
A preparation method for Chinese medicinal toothpaste, is characterized in that: comprise the following steps:
A, the Rhizoma Imperatae of formula ratio and Rumalus sophorae are ground into 50-80 order;
B, the calcium phosphate of formula ratio, lanthanum chloride, colloidal silica and hydroxyethyl-cellulose are fully mixed, stir to obtain mixture;
The water of formula ratio, glucide and thin Flos Caryophylli is added, obtained mixed liquor in C, the mixture that obtains in step B;
The antiseptic of Rhizoma Imperatae powder, Rumalus sophorae powder and formula ratio after step A is pulverized is added in D, the mixed liquor that obtains in step C;
E, D step gained mixture under vacuo degassed stirring get product.
The foaming agent of formula ratio is also added in described D step.
Rhizoma Imperatae of the present invention is the rhizome of grass perennial herb Herba Imperatae, there is cooling blood for hemostasis, the effect of heat-clearing and toxic substances removing, the property of medicine is cold and cool, the blood that operation can be made to overrun replys normal operation, promotes that thrombin is far formed, shortens hemorrhage and clotting time, reduce capillary permeability, hard bleeding rate.
The chemical composition of Rumalus sophorae of the present invention is containing globulariacitrin, and nature and flavor are bitter.
Calcium phosphate of the present invention is white crystal or amorphous powder, relative density 3.14, fusing point 1670 DEG C; Be dissolved in acid, water insoluble and ethanol.
Lanthanum chloride chemical formula of the present invention is blush or gray crystals or block, and chemical formula is LaCl37H2O, fusing point 70 DEG C, can be water-soluble, easy deliquescence; Meet alkali and generate hydroxide or oxychloride precipitation, anhydrous salt is white powder crystallization; Density 3.842, fusing point 860 DEG C, boiling point is 1000-1200 DEG C; Be soluble in soda pop, decompose in hot water; Be soluble in ethanol and pyridine, insoluble in ether and benzene; The strong moisture absorption of anhydrous lanthanum chloride, generation oxychloride is easily decomposed in heating in atmosphere.
Thin Flos Caryophylli of the present invention has the special aroma of Herba Menthae, and taste is just scorching hot rear refrigerant.
Sorbic acid of the present invention is white needles or Powdered crystal, is slightly soluble in water, can be dissolved in multiple organic solvent, and its fusing point is 132-135 DEG C, and boiling point is 228 DEG C.
Potassium sorbate of the present invention is colourless to the crystallization of white flakes shape or crystalline powder, odorless, unstable in atmosphere, can be oxidized painted, and molecular weight 150.22, has hygroscopicity, soluble in water, ethanol.
Calcium sorbate of the present invention is white crystals fine powder, molecular weight 262.32.
The Advantageous Effects that the present invention brings is mainly manifested in the following aspects:
One, the Rhizoma Imperatae in the raw material that the present invention is used is the rhizome of grass perennial herb Herba Imperatae, there is cooling blood for hemostasis, the effect of heat-clearing and toxic substances removing, the property of medicine is cold and cool, the blood that operation can be made to overrun replys normal operation, promotes that thrombin is far formed, shortens hemorrhage and clotting time, reduce capillary permeability, hard bleeding rate.
Two, in the raw material that the present invention is used, decomposability is strong in the hot water for lanthanum chloride, and people's tooth of often smoking is partially yellow, easily produces dental plaque; Lanthanum chloride can be good at dissolving dental plaque.
Three, in the raw material that the present invention is used, calcium phosphate is white crystal or amorphous powder, relative density 3.14, fusing point 1670 DEG C; Be dissolved in acid, water insoluble and ethanol, have good effect to teeth whitening.
Four, in the raw material that the present invention is used, Rumalus sophorae is water white transparency volatile liquid, and dissolubility is strong, most organic solvents such as soluble in water, alcohol, ether, benzene, chloroform.Other compositions in formula are coordinated to can be good at removing dental plaque.
Five, in the raw material that the present invention is used, thin Flos Caryophylli has the special aroma of Herba Menthae, and taste is just scorching hot rear refrigerant, and oral cavity can be made pure and fresh lastingly, and the flavour of a drug of effectively comprehensive Rhizoma Imperatae, make toothpaste taste of Chinese medicine subtract light, be applicable to people's life-time service.
Six, the Rhizoma Imperatae of formula ratio and Rumalus sophorae are ground into 50-80 order, again by the calcium phosphate of formula ratio, lanthanum chloride, colloidal silica and hydroxyethyl-cellulose fully mix, stir to obtain mixture, add the water of formula ratio in the mixture, glucide and thin Flos Caryophylli, obtained mixed liquor, Rhizoma Imperatae powder is added in mixed liquor, the antiseptic of Rumalus sophorae powder and formula ratio, finally by the mixture degassed obtained Chinese medicinal toothpaste that stirs under vacuo, not only go dental plaque effective, effectively can avoid various focusing depths represented, and Chinese medicine is lightly seasoned, its preparation technology is simple, production cost is low.
Detailed description of the invention
Embodiment 1
A kind of Chinese medicinal toothpaste, is characterized in that: the component comprising following parts by weight:
Rhizoma Imperatae 0.01 part
20 parts, calcium phosphate
Lanthanum chloride 3 parts
Colloidal silica 3 parts
Hydroxyethyl-cellulose 0.5 part
Rumalus sophorae 2 parts
0.05 part, glucide
30 parts, water
Thin Flos Caryophylli 2 parts
Antiseptic 0.01 part.
Embodiment 2
A kind of Chinese medicinal toothpaste, is characterized in that: the component comprising following parts by weight:
Rhizoma Imperatae 0.02 part
21 parts, calcium phosphate
Lanthanum chloride 4 parts
Colloidal silica 4 parts
Hydroxyethyl-cellulose 0.6 part
Rumalus sophorae 3 parts
0.06 part, glucide
35 parts, water
Thin Flos Caryophylli 3 parts
Antiseptic 0.02 part
Tea saponin 0.01 part.
Described antiseptic is sorbic acid.
Embodiment 3
A kind of Chinese medicinal toothpaste, is characterized in that: the component comprising following parts by weight:
Rhizoma Imperatae 0.03 part
22 parts, calcium phosphate
Lanthanum chloride 5 parts
Colloidal silica 5 parts
Hydroxyethyl-cellulose 0.7 part
Rumalus sophorae 4 parts
0.07 part, glucide
40 parts, water
Thin Flos Caryophylli 4 parts
Antiseptic 0.03 part
Tea saponin 0.05 part.
Described antiseptic is potassium sorbate.
Embodiment 4
A kind of Chinese medicinal toothpaste, is characterized in that: the component comprising following parts by weight:
Rhizoma Imperatae 0.08 part
40 parts, calcium phosphate
Lanthanum chloride 6 parts
Colloidal silica 6 parts
Hydroxyethyl-cellulose 2 parts
Rumalus sophorae 7 parts
0.2 part, glucide
60 parts, water
Thin Flos Caryophylli 10 parts
Antiseptic 0.08 part
Tea saponin 0.08 part.
Rhizoma Imperatae of the present invention is the rhizome of grass perennial herb Herba Imperatae, there is cooling blood for hemostasis, the effect of heat-clearing and toxic substances removing, the property of medicine is cold and cool, the blood that operation can be made to overrun replys normal operation, promotes that thrombin is far formed, shortens hemorrhage and clotting time, reduce capillary permeability, hard bleeding rate.
The chemical composition of Rumalus sophorae of the present invention is containing globulariacitrin, and nature and flavor are bitter.
Calcium phosphate of the present invention is white crystal or amorphous powder, relative density 3.14, fusing point 1670 DEG C; Be dissolved in acid, water insoluble and ethanol.
Lanthanum chloride chemical formula of the present invention is blush or gray crystals or block, and chemical formula is LaCl37H2O, fusing point 70 DEG C, can be water-soluble, easy deliquescence; Meet alkali and generate hydroxide or oxychloride precipitation, anhydrous salt is white powder crystallization; Density 3.842, fusing point 860 DEG C, boiling point is 1000-1200 DEG C; Be soluble in soda pop, decompose in hot water; Be soluble in ethanol and pyridine, insoluble in ether and benzene; The strong moisture absorption of anhydrous lanthanum chloride, generation oxychloride is easily decomposed in heating in atmosphere.
Thin Flos Caryophylli of the present invention has the special aroma of Herba Menthae, and taste is just scorching hot rear refrigerant.
Sorbic acid of the present invention is white needles or Powdered crystal, is slightly soluble in water, can be dissolved in multiple organic solvent, and its fusing point is 132-135 DEG C, and boiling point is 228 DEG C.
Potassium sorbate of the present invention is colourless to the crystallization of white flakes shape or crystalline powder, odorless, unstable in atmosphere, can be oxidized painted, and molecular weight 150.22, has hygroscopicity, soluble in water, ethanol.
Embodiment 5
A preparation method for Chinese medicinal toothpaste, is characterized in that: comprise the following steps:
A, 0.01 part of Rhizoma Imperatae and 2 parts of Rumalus sophorae are ground into 50 orders;
B, 20 parts of calcium phosphate, 3 parts of lanthanum chloride, 3 parts of colloidal silicas and 0.5 part of hydroxyethyl-cellulose are fully mixed, stir to obtain mixture;
C, in the mixture that step B is obtained, add 30 parts of water, 0.05 part of glucide and 2 parts of thin Flos Caryophyllis, obtained mixed liquor;
Rhizoma Imperatae powder, Rumalus sophorae powder and 0.01 portion of antiseptic after step A is pulverized is added in D, the mixed liquor that obtains in step C;
E, D step gained mixture under vacuo degassed stirring get product.
Embodiment 6
A preparation method for Chinese medicinal toothpaste, is characterized in that: comprise the following steps:
A, 0.02 part of Rhizoma Imperatae and 3 parts of Rumalus sophorae are ground into 60 orders;
B, 21 parts of calcium phosphate, 4 parts of lanthanum chloride, 4 parts of colloidal silicas and 0.6 part of hydroxyethyl-cellulose are fully mixed, stir to obtain mixture;
C, in the mixture that step B is obtained, add 35 parts of water, 0.06 part of glucide and 3 parts of thin Flos Caryophyllis, obtained mixed liquor;
Rhizoma Imperatae powder, Rumalus sophorae powder and 0.02 portion of antiseptic after step A is pulverized is added in D, the mixed liquor that obtains in step C;
E, D step gained mixture under vacuo degassed stirring get product.
The foaming agent of 0.01 part is also added in described D step.
Embodiment 7
A preparation method for Chinese medicinal toothpaste, is characterized in that: comprise the following steps:
A, 0.03 part of Rhizoma Imperatae and 4 parts of Rumalus sophorae are ground into 70 orders;
B, 22 parts of calcium phosphate, 5 parts of lanthanum chloride, 5 parts of colloidal silicas and 0.7 part of hydroxyethyl-cellulose are fully mixed, stir to obtain mixture;
C, in the mixture that step B is obtained, add 40 parts of water, 0.07 part of glucide and 4 parts of thin Flos Caryophyllis, obtained mixed liquor;
Rhizoma Imperatae powder, Rumalus sophorae powder and 0.03 portion of antiseptic after step A is pulverized is added in D, the mixed liquor that obtains in step C;
E, D step gained mixture under vacuo degassed stirring get product.
The foaming agent of 0.05 part is also added in described D step.
Embodiment 8
A preparation method for Chinese medicinal toothpaste, is characterized in that: comprise the following steps:
A, 0.08 part of Rhizoma Imperatae and 7 parts of Rumalus sophorae are ground into 80 orders;
B, 40 parts of calcium phosphate, 6 parts of lanthanum chloride, 6 parts of colloidal silicas and 2 parts of hydroxyethyl-celluloses are fully mixed, stir to obtain mixture;
C, in the mixture that step B is obtained, add 60 parts of water, 0.2 part of glucide and 10 parts of thin Flos Caryophyllis, obtained mixed liquor;
Rhizoma Imperatae powder, Rumalus sophorae powder and 0.08 portion of antiseptic after step A is pulverized is added in D, the mixed liquor that obtains in step C;
E, D step gained mixture under vacuo degassed stirring get product.
The foaming agent of 0.08 part is also added in described D step.
The Rhizoma Imperatae of formula ratio and Rumalus sophorae are ground into 80 orders, again the calcium phosphate of formula ratio, lanthanum chloride, colloidal silica and hydroxyethyl-cellulose are fully mixed, stir to obtain mixture, add the water of formula ratio, glucide and thin Flos Caryophylli in the mixture, obtained mixed liquor, the antiseptic of Rhizoma Imperatae powder, Rumalus sophorae powder and formula ratio is added in mixed liquor, finally by the mixture degassed obtained Chinese medicinal toothpaste that stirs under vacuo, not only go dental plaque effective, effectively can avoid various focusing depths represented, and Chinese medicine is lightly seasoned, its preparation technology is simple, and production cost is low.

Claims (6)

1. a Chinese medicinal toothpaste, is characterized in that: the component comprising following parts by weight:
Rhizoma Imperatae 0.01-0.08 part
Calcium phosphate 20-40 part
Lanthanum chloride 3-6 part
Colloidal silica 3-6 part
Hydroxyethyl-cellulose 0.5-2 part
Rumalus sophorae 2-7 part
Glucide 0.05-0.2 part
Water 30-60 part
Thin Flos Caryophylli 2-10 part
Antiseptic 0.01-0.08 part.
2. a kind of Chinese medicinal toothpaste according to claim 1, it is characterized in that: also comprise foaming agent, blowing agent composition weight number is 0.01-0.08 part.
3. a kind of Chinese medicinal toothpaste according to claim 2, is characterized in that: described foaming agent is tea saponin.
4. a kind of Chinese medicinal toothpaste according to claim 1 or 2, is characterized in that: described antiseptic is sorbic acid, potassium sorbate or calcium sorbate.
5. a preparation method for Chinese medicinal toothpaste, is characterized in that: comprise the following steps:
A, the Rhizoma Imperatae of formula ratio and Rumalus sophorae are ground into 50-80 order;
B, the calcium phosphate of formula ratio, lanthanum chloride, colloidal silica and hydroxyethyl-cellulose are fully mixed, stir to obtain mixture;
The water of formula ratio, glucide and thin Flos Caryophylli is added, obtained mixed liquor in C, the mixture that obtains in step B;
The antiseptic of Rhizoma Imperatae powder, Rumalus sophorae powder and formula ratio after step A is pulverized is added in D, the mixed liquor that obtains in step C;
E, D step gained mixture under vacuo degassed stirring get product.
6. the preparation method of a kind of Chinese medicinal toothpaste according to claim 5, is characterized in that: the foaming agent also adding formula ratio in described D step.
CN201410726403.4A 2014-12-04 2014-12-04 Traditional Chinese medicine toothpaste and preparation method thereof Pending CN104434675A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105168026A (en) * 2015-10-29 2015-12-23 成都顺发消洗科技有限公司 Tooth whitening paste
CN105726417A (en) * 2016-04-11 2016-07-06 福建海山茶业有限公司 Oolong toothpaste and preparation method thereof
CN106214600A (en) * 2016-08-08 2016-12-14 雷春生 A kind of preparation method of child edible toothpaste
CN106727152A (en) * 2017-01-11 2017-05-31 安徽科技学院 A kind of common rabdosia leaf health-care toothpaste and its production method

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1969811A (en) * 2006-11-30 2007-05-30 广州立白企业集团有限公司 Application of natural plant cogongras rhizome extract in oral care product
KR20110135678A (en) * 2010-06-11 2011-12-19 (주)네오메디컬 Functional toothpaste composition
CN103054742A (en) * 2011-10-21 2013-04-24 汤治强 Aromatic tooth-cleaning toothpaste
CN103385828A (en) * 2013-07-17 2013-11-13 广州立白企业集团有限公司 Salty toothpaste having the function of preventing oral cavity fire ascending

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1969811A (en) * 2006-11-30 2007-05-30 广州立白企业集团有限公司 Application of natural plant cogongras rhizome extract in oral care product
KR20110135678A (en) * 2010-06-11 2011-12-19 (주)네오메디컬 Functional toothpaste composition
CN103054742A (en) * 2011-10-21 2013-04-24 汤治强 Aromatic tooth-cleaning toothpaste
CN103385828A (en) * 2013-07-17 2013-11-13 广州立白企业集团有限公司 Salty toothpaste having the function of preventing oral cavity fire ascending

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105168026A (en) * 2015-10-29 2015-12-23 成都顺发消洗科技有限公司 Tooth whitening paste
CN105726417A (en) * 2016-04-11 2016-07-06 福建海山茶业有限公司 Oolong toothpaste and preparation method thereof
CN106214600A (en) * 2016-08-08 2016-12-14 雷春生 A kind of preparation method of child edible toothpaste
CN106727152A (en) * 2017-01-11 2017-05-31 安徽科技学院 A kind of common rabdosia leaf health-care toothpaste and its production method

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Application publication date: 20150325