CN104434579A - Smell-eliminating powder containing biological polysaccharide - Google Patents

Smell-eliminating powder containing biological polysaccharide Download PDF

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Publication number
CN104434579A
CN104434579A CN201410758467.2A CN201410758467A CN104434579A CN 104434579 A CN104434579 A CN 104434579A CN 201410758467 A CN201410758467 A CN 201410758467A CN 104434579 A CN104434579 A CN 104434579A
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China
Prior art keywords
taste powder
chitosan
parts
agent
powder
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Pending
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CN201410758467.2A
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Chinese (zh)
Inventor
陈�光
王岩
曹凤杰
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AESTHETIC TECHNOLOGY (BEIJING) Co Ltd
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AESTHETIC TECHNOLOGY (BEIJING) Co Ltd
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Priority to CN201410758467.2A priority Critical patent/CN104434579A/en
Publication of CN104434579A publication Critical patent/CN104434579A/en
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Abstract

The invention relates to smell-eliminating powder containing biological polysaccharide. The smell-eliminating powder comprises the following components in parts by weight: 0.1-20 parts of biological polysaccharide, 0.1-50 parts of a sweat-absorbing agent, 0.2-5 parts of a detention agent, 2-80 parts of a diluent and 0.1-1 part of a flow aid. According to the smell-eliminating powder provided by the invention, the biological polysaccharide is selected as a germicidal ingredient in the smell-eliminating powder, and is further optimized into chitosan; protease and other ingredients in cells are leaked by the chitosan by virtue of interaction of amino with positive charges and negative charges on bacterial cell membranes, and thus the antibacterial and antimicrobial effects are achieved; the safety is high; the effect is significant; meanwhile, biological polysaccharide and derivatives thereof are selected as sweat-absorbing components, so that the smell-eliminating powder has the function of stopping sweating when removing a peculiar smell, and is good in stability and small in thrill to a human body due to synergistic effects of the components of the smell-eliminating powder; and the smell-eliminating powder is very convenient to use, and is easily accepted by consumers.

Description

A kind of taste powder that disappears containing biological polyoses
Technical field
The present invention relates to cosmetic field, be specifically related to a kind of taste powder that disappears containing biological polyoses.
Background technology
Biological polyoses, as the positively charged material of occurring in nature, has antibacterial, antiinflammation, is antipathogenic composition conventional in Wound dressing.In biological polyoses, being most widely used with chitosan, best results.Specifically, the sterilization mechanism of chitosan be rely on positively charged amino can and bacterial cell membrane on the interaction of negative charge, make intracellular protease and the leakage of other compositions, thus reach antibacterial, bactericidal action.In addition, the macromole biological polyoses class materials such as calcium alginate, Chitosan-phospholipid complex, modified starch, have extremely strong water absorption, multiplexly clinically make bleeding-stopping dressing.If calcium alginate Absorbable rod is from 20 times of moisture of height, chitosan/carboxymethyl cellulose resin energy water absorption rate is up to 400 times of own wt.
Tool is reported, in existing cosmetics, sterilization or antipathogenic composition, multiselect chlorhexidine, triclosan etc., as the technical scheme disclosed in patent documentation CN101617995, its antibacterial has just selected the material such as chlorhexidine, triclosan.But these common antipathogenic compositions, exist many problems in preparation compatibility and safety: chlorhexidine and salts substances thereof, be by self-contained positive charge, and be adsorbed in bacterium surface, and then destroy bacterial cytoplasm film, thus play antibacterial or bactericidal action.But chlorhexidine belongs to ingredient, be generally used for medicine or medicine adornment, and have stronger side effect and sensitization, there is incompatibility with anion surfactant in addition, can not be public with soap, alkaloids; Triclosan is a kind of antibacterial of broad-spectrum high efficacy, but as daily chemical products, whether life-time service can bring potential safety hazard, is recently subject to the extensive concern of media and the public.
Therefore, biological polyoses class material is applied in the taste cosmetics that disappear has a good application prospect.
Summary of the invention
Object of the present invention is the defect overcoming prior art, and providing a kind of is main component with biological polyoses, good stability, little and have absorbing sweat concurrently and the powder of the function of odor that disappears to skin irritation.
The invention provides a kind of taste powder that disappears containing biological polyoses, described in the taste powder that disappears comprise the composition of following weight portion: biological polyoses 0.1 ~ 20 part, absorbing sweat agent 0.1 ~ 50 part, is detained agent 0.2 ~ 5 part, diluent 2 ~ 80 parts, fluidizer 0.1 ~ 1 part.
Preferably, the taste powder that disappears described in comprises the composition of following weight portion: biological polyoses 0.5 ~ 5 part, absorbing sweat agent 15 ~ 25 parts, is detained agent 0.5 ~ 2 part, diluent 70 ~ 80 parts, fluidizer 0.2 ~ 0.7 part.
The present invention selects biological polyoses as the major antibacterial composition of the taste powder that disappears, and described biological polyoses is preferably chitosan, and described chitosan is the chitosan of deacetylation 60-99%, is preferably the chitosan of deacetylation 80%.
Described absorbing sweat agent is biological polyoses and derivant thereof, be preferably in calcium alginate, starch sodium octenyl succinate, crosslinked succinic acid starch ester, chitosan/carboxymethyl cellulose resin one or more, the more preferably mixture of calcium alginate, chitosan/carboxymethyl cellulose resin or calcium alginate and chitosan/carboxymethyl cellulose resin.
Described delay agent is polyacrylic resin, is preferably carbomer (Carbomer) series, more preferably carbomer940.
Described diluent is starch, is preferably corn starch.
Described fluidizer be selected from aerosil, Pulvis Talci, magnesium stearate, stearic acid one or more, be preferably aerosil, stearic acid or aerosil and stearic mixture.
Preferably, the composition of taste powder containing following weight portion that disappear of the present invention: chitosan 0.5 ~ 5 part, calcium alginate 10 ~ 15 parts, chitosan/carboxymethyl cellulose resin 0 ~ 15 part, carbomer940 0.5 ~ 2 part, corn starch 70 ~ 80 parts, aerosil 0.1 ~ 0.5 part, stearic acid 0.1 ~ 0.5 part.
Can also comprise adjuvant in the taste powder that disappears of the present invention, described adjuvant comprises emulsifying agent and essence.
The consumption of described emulsifying agent is 0.01 ~ 0.1 part, is preferably 0.05 part; Described emulsifying agent be selected from phospholipid, tween, span, polyoxyethylene castor oil, polyoxyethylene hydrogenated Oleum Ricini, tocofecol succinic acid macrogol ester, spermol, isopropyl palmitate or Polyethylene Glycol coco glycerides one or more, be preferably sorbester p17.
The consumption of described essence is 0.01 ~ 0.2 part, and described essence is preferably vegetable oil, one or more more preferably in Jasmin oil, Oleum Rosae Rugosae, Cananga odorata oil, Oleum Santali albi, tangerine oil or Oleum menthae.
Further preferably, the composition of taste powder containing following weight portion that disappear of the present invention: chitosan 0.5 ~ 5 part, calcium alginate 10 ~ 15 parts, chitosan/carboxymethyl cellulose resin 0 ~ 15 part, carbomer940 0.5 ~ 2 part, corn starch 70 ~ 80 parts, aerosil 0.1 ~ 0.5 part, stearic acid 0.1 ~ 0.5 part, sorbester p17 0.01 ~ 0.1 part, vegetable oil 0.01 ~ 0.2 part.
As most preferably scheme, the composition of taste powder containing following weight portion that disappear of the present invention: chitosan 3 parts, calcium alginate 12 parts, chitosan/carboxymethyl cellulose resin 10 parts, carbomer940 1 part, corn starch 75 parts, aerosil 0.3 part, stearic acid 0.3 part, sorbester p17 0.05 part, vegetable oil 0.1 part.
Disappear described in invention further provides the preparation method of taste powder, said method comprising the steps of:
(1) by after biological polyoses, absorbing sweat agent, delay agent and diluent grinding, 200 mesh sieves are crossed, mix and blend 10-20min;
(2) in step (1) products therefrom, add fluidizer, mix and blend 5-10min, must disappear taste powder.
When containing adjuvant in described powder, adjuvant adds with fluidizer in step (2) simultaneously.
Disappear described in the present invention protects further the application of taste powder, described in the taste powder that disappears can be used for the deodorization of human body.
The present invention selects chitosan as the sterilization component disappeared in taste powder, selects biological polyoses and derivant thereof to be absorbing sweat composition, while removal abnormal flavour, have hidroschesis function concurrently; And the taste powder preparation stability that disappears provided by the invention is good, little to the zest of human body, be easily esthetically acceptable to the consumers, have a good application prospect.
Detailed description of the invention
Following examples for illustration of the present invention, but are not used for limiting the scope of the invention.
The chitosan used in various embodiments of the present invention is the chitosan of deacetylation 80%.
Embodiment 1
1, disappear the raw material of taste powder: chitosan 3g, calcium alginate 12g, chitosan/carboxymethyl cellulose resin 10g, carbomer940 1g, corn starch 75g, aerosil 0.3g, stearic acid 0.3g, sorbester p17 0.05g, Jasmin oil 0.1g.
2, prepare according to following steps the taste powder that disappears:
(1) by after chitosan, calcium alginate, chitosan/carboxymethyl cellulose resin, carbomer940 and corn starch ground, 200 mesh sieves are crossed, mix and blend 15min;
(2) in step (1) products therefrom, add sorbester p17, Jasmin oil, aerosil and stearic acid, mix and blend 10min, must disappear taste powder.
Embodiment 2
1, disappear the raw material of taste powder: chitosan 0.5g, calcium alginate 10g, chitosan/carboxymethyl cellulose resin 15g, carbomer940 0.8g, corn starch 72g, aerosil 0.2g;
2, prepare according to following steps the taste powder that disappears:
(1) by after chitosan, calcium alginate, chitosan/carboxymethyl cellulose resin, carbomer940 and corn starch ground, 200 mesh sieves are crossed, mix and blend 20min;
(2) in step (1) products therefrom, add aerosil, mix and blend 5min, must disappear taste powder.
Embodiment 3
1, disappear the raw material of taste powder: chitosan 5g, calcium alginate 15g, carbomer940 1g, corn starch 76.5g, aerosil 0.5g;
2, prepare according to following steps the taste powder that disappears:
(1) by after chitosan, calcium alginate, carbomer940 and corn starch ground, 200 mesh sieves are crossed, mix and blend 10min;
(2) in step (1) products therefrom, add aerosil, mix and blend 10min, must disappear taste powder.
Embodiment 4
1, disappear the raw material of taste powder: chitosan 1.5g, calcium alginate 15g, carbomer940 1g, corn starch 79.75g, aerosil 0.5g, stearic acid 0.5g, sorbester p17 0.05g, Oleum Rosae Rugosae 0.2g;
2, prepare according to following steps the taste powder that disappears:
(1) by after chitosan, calcium alginate, carbomer940 and corn starch ground, 200 mesh sieves are crossed, mix and blend 20min;
(2) in step (1) products therefrom, add sorbester p17, Oleum Rosae Rugosae, aerosil and stearic acid, mix and blend 5min, must disappear taste powder.
Comparative example 1
Compared with embodiment 1, difference is only: replace chitosan with triclosan.
Comparative example 2
Compared with embodiment 1, difference is only: replace calcium alginate and chitosan/carboxymethyl cellulose resin with sodium stearate.
Comparative example 3
Compared with embodiment 1, difference is only: replace carbomer with Polyethylene Glycol.
Comparative example 4
Compared with embodiment 1, difference is only, prepares the taste powder that disappears: according to following steps after chitosan, calcium alginate, chitosan/carboxymethyl cellulose resin, carbomer940 and corn starch ground, crosses 200 mesh sieves; By all raw material mix and blend 25min, must disappear taste powder.
Experimental example 1: stability test
The taste powder that embodiment 1 ~ 4 and comparative example 1 ~ 4 gained disappeared is transferred at 37 DEG C, often wet condition respectively and is set to 0 .5 month, 1 month and 3 months, and basis of microscopic observation detects sample and whether occurs adhesion or caking.Test result is in table 1.
Table 1: stability test result
Sample Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Comparative example 1 Comparative example 2 Comparative example 3 Comparative example 4
0.5 month Without caking Without caking Without caking Without caking Without caking Without caking Without caking Without caking
1 month Without caking Without caking Without caking Without caking Without caking Without caking A small amount of caking Without caking
3 months Without caking Without caking Without caking Without caking A small amount of caking A small amount of caking A large amount of caking A small amount of caking
From above result, the good stability of the taste powder that disappears provided by the invention, still there will not be caking after long-time placement, is better than each comparative example.
Experimental example 2: deodorizing effect is tested
Testing example 1 ~ 4 and comparative example 1 ~ 4 gained disappear the deodorizing effect of taste powder.
Detection method is: collect 10ml profuse sweating in the armpit, getting 9 test tubes and being numbered by test tube is 1 ~ No. 9, often pipe loads 1ml profuse sweating in the armpit liquid, wherein a test tube does not add any sample as blank, embodiment 1 ~ 4 and comparative example 1 ~ 4 gained sample are added in all the other eight corresponding test tubes respectively, the addition of each sample is 0.5g, each test tube silica gel plug is sealed, 6h is cultivated at 37 DEG C, after cultivation terminates, culture in each test tube is equally divided into 8 parts, seals and under placing 4 DEG C of conditions, for subsequent use;
Double-blind method intersection sensory test is adopted to evaluate the deodorizing effect of different sample, concrete operations are: choose 8 olfactory sensation healthy premenopausal volunteers, and everyone is assigned to each portion of culture in 1 ~ No. 9 test tube, hears above-mentioned culture taste with olfactory sensation, and experience separately with the five-grade marking system record, average.Standards of grading are: 0 is divided into abnormal smells from the patient normal, without uncomfortable taste; 5 are divided into stench, are difficult to stand, and remaining fraction degree is between 0 ~ 5.Before each news sample, experimenter has a breath of fresh air in outdoor at least 10min.Test result is in table 2.
Table 2: deodorizing effect evaluation
From above result, the deodorizing effect disappearing taste powder provided by the invention is better than each comparative example, and the deodorizing effect of embodiment 1 is best.
Experimental example 3: soaking effect is tested
Testing example 1 ~ 4 and comparative example 1 ~ 4 gained disappear the soaking effect of taste powder.
Detection method is: each 0.5g of sample thief, is placed on glass cotton respectively, is placed in the hermetic container containing excess water, places 24 hours under 37 DEG C of conditions.Of poor quality by calculating glass cotton loading product water suction front and back, the final water absorption rate obtaining sample, the computing formula of water absorption rate is: example weight × 100% before water absorption rate=(after water suction the front example weight of example weight-water suction)/water suction.Test result is in table 3.
Table 3: water absorption rate test result
Sample Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Comparative example 1 Comparative example 2 Comparative example 3 Comparative example 4
Water absorption rate 680% 525% 560% 610% 520% 400% 410% 480%
From above result, the soaking effect disappearing taste powder provided by the invention is better than each comparative example, and the soaking effect of embodiment 1 is best.
Experimental example 4: skin irritation is tested
Adopt double-blind method to intersect sensory test evaluation to disappear the zest of taste powder to skin.Concrete operations are: choose 20 normal healthy premenopausal volunteers of sense of touch, everyone be assigned to 8 groups of each 0.1g of sample and uniform application to hard of hearing portion, smear a kind of sample at every turn, clean by clean water immediately after each daubing product, interval at least 10min between smearing for each time.Experience separately with the five-grade marking system record, average.Standards of grading are: 0 is divided into without sensation of pricking; 5 are divided into sensation of pricking very strong, and remaining fraction degree is between 0 ~ 5.Test result is in table 4.
Table 4: skin irritation evaluation
Sample Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Comparative example 1 Comparative example 2 Comparative example 3 Comparative example 4
Scoring 2.15 3.01 2.09 2.67 4.02 4.38 4.57 3.91
From above result, the skin irritation of the taste powder that disappears provided by the invention is all significantly smaller than each comparative example.
Although above with general explanation, detailed description of the invention and test, the present invention is described in detail, and on basis of the present invention, can make some modifications or improvements it, this will be apparent to those skilled in the art.Therefore, these modifications or improvements without departing from theon the basis of the spirit of the present invention, all belong to the scope of protection of present invention.

Claims (10)

1., containing the taste powder that disappears of biological polyoses, it is characterized in that, described in the taste powder that disappears comprise the composition of following weight portion: biological polyoses 0.1 ~ 20 part, absorbing sweat agent 0.1 ~ 50 part, is detained agent 0.2 ~ 5 part, diluent 2 ~ 80 parts, fluidizer 0.1 ~ 1 part.
2. the taste powder that disappears according to claim 1, is characterized in that, described in the taste powder that disappears comprise the composition of following weight portion: biological polyoses 0.5 ~ 5 part, absorbing sweat agent 15 ~ 25 parts, is detained agent 0.5 ~ 2 part, diluent 70 ~ 80 parts, fluidizer 0.2 ~ 0.7 part.
3. the taste powder that disappears according to claim 1, is characterized in that, described biological polyoses is the chitosan of deacetylation 60 ~ 99%.
4. the taste powder that disappears according to claim 1, it is characterized in that, described absorbing sweat agent is biological polyoses and derivant thereof, is preferably one or more in calcium alginate, starch sodium octenyl succinate, crosslinked succinic acid starch ester, chitosan/carboxymethyl cellulose resin.
5. the taste powder that disappears according to claim 1, is characterized in that, described delay agent is polyacrylic resin; Described diluent is starch; Described fluidizer be selected from aerosil, Pulvis Talci, magnesium stearate, stearic acid one or more.
6. the taste powder that disappears according to claim 1, it is characterized in that, the described taste powder that disappears comprises the composition of following weight portion: chitosan 0.5 ~ 5 part, calcium alginate 10 ~ 15 parts, chitosan/carboxymethyl cellulose resin 0 ~ 15 part, carbomer940 0.5 ~ 2 part, corn starch 70 ~ 80 parts, aerosil 0.1 ~ 0.5 part, stearic acid 0.1 ~ 0.5 part.
7. the taste powder that disappears according to claim 1 ~ 6 any one, is characterized in that, described in disappear in taste powder and also comprise emulsifying agent 0.01 ~ 0.1 part and 0.01 ~ 0.2 part, essence.
8. the taste powder that disappears according to claim 1, it is characterized in that, the described composition of taste powder containing following weight portion that disappear: chitosan 0.5 ~ 5 part, calcium alginate 10 ~ 15 parts, chitosan/carboxymethyl cellulose resin 0 ~ 15 part, carbomer940 0.5 ~ 2 part, corn starch 70 ~ 80 parts, aerosil 0.1 ~ 0.5 part, stearic acid 0.1 ~ 0.5 part, sorbester p17 0.01 ~ 0.1 part, vegetable oil 0.01 ~ 0.2 part.
9. prepare the method for the taste powder that to disappear described in claim 1 ~ 6 any one, it is characterized in that, comprise the following steps:
(1) by after biological polyoses, absorbing sweat agent, delay agent and diluent grinding, 200 mesh sieves are crossed, mix and blend 10-20min;
(2) in step (1) products therefrom, add fluidizer, mix and blend 5-10min, must disappear taste powder.
10. prepare the method for the taste powder that to disappear described in claim 7 or 8, it is characterized in that, comprise the following steps:
(1) by after biological polyoses, absorbing sweat agent, delay agent and diluent grinding, 200 mesh sieves are crossed, mix and blend 10-20min;
(2) in step (1) products therefrom, add emulsifying agent, essence and fluidizer, mix and blend 5-10min, must disappear taste powder.
CN201410758467.2A 2014-12-10 2014-12-10 Smell-eliminating powder containing biological polysaccharide Pending CN104434579A (en)

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CN111632013A (en) * 2020-06-09 2020-09-08 广州市科能化妆品科研有限公司 Soothing and repairing composition, soothing and repairing powder preparation and preparation method thereof

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110016085A (en) * 2018-01-10 2019-07-16 烟台绿叶动物保健品有限公司 A kind of preparation method of astragalus polyose
CN111632013A (en) * 2020-06-09 2020-09-08 广州市科能化妆品科研有限公司 Soothing and repairing composition, soothing and repairing powder preparation and preparation method thereof

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Application publication date: 20150325