CN104434569B - A kind of pigment breast and preparation method thereof - Google Patents
A kind of pigment breast and preparation method thereof Download PDFInfo
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- CN104434569B CN104434569B CN201410808474.9A CN201410808474A CN104434569B CN 104434569 B CN104434569 B CN 104434569B CN 201410808474 A CN201410808474 A CN 201410808474A CN 104434569 B CN104434569 B CN 104434569B
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Abstract
The invention provides a kind of pigment breast, by ultra-fine silicon process titanium dioxide dispersion pulp, silicon process nanometer titanium dioxide dispersion pulp, ethylhexyl methoxy cinnamate, silicon process iron oxide yellow dispersion pulp, silicon process iron oxide red dispersion pulp, silicon process iron oxide black dispersion pulp, cyclopenta siloxanes/trimethyl silicane alcoxyl base esters of silicon acis, sorbitan sesquioleate, cyclopenta siloxanes/dimethiconol, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, Magnesiumaluminumsilicate, xanthan gum, polyglutamic acid, propylene glycol, butanediol, phenoxyethanol/Sensiva SC50, ethohexadiol/Sensiva SC50, sodium hydroxide, water forms, pigment breast moistening effect of the present invention is lasting, control oil, anti-antiperspirant is good.
Description
Technical field
The invention belongs to cosmetic field, be specifically related to a kind of pigment breast, and the preparation method of this pigment breast.
Background technology
Traditional BB, CC frost etc. hides the normally common Water-In-Oil (W/O) of flaw product and silicon Water-In-Oil (W/Si) system.These powder body quality are thick and heavy, and poor air permeability, easily blocks pore, and life-time service can accelerate skin ageing; Smear is poor, and adornment sense unnaturally, has the vestige of upper powder excessively and dressing can be made to seem stiff, spreading on face just as one deck mask after using; Smear and just there will be fuel-displaced in the rear short time, floating powder, melts the phenomenon of adornment, and needs to remove ornaments and formal dress with makeup remover.
Summary of the invention
An object of the present invention is the technical problem for solving above, provide that a kind of skinfeel is good, moistening effect is lasting, water-resistance is high, control the good pigment breast of oily anti-antiperspirant.
Another object of the present invention is to provide the preparation method of above-mentioned pigment breast.
For reaching above object, the invention provides a kind of pigment breast, it is made up of the component of following percentage by weight:
Ultra-fine silicon process titanium dioxide dispersion pulp 3 ~ 5%, silicon process nanometer titanium dioxide dispersion pulp 5%, ethylhexyl methoxy cinnamate 3%, silicon process iron oxide yellow dispersion pulp 0.25 ~ 0.35%, silicon process iron oxide red dispersion pulp 0.1 ~ 0.16%, silicon process iron oxide black dispersion pulp 0.06 ~ 0.08%, cyclopenta siloxanes/trimethyl silicane alcoxyl base esters of silicon acis 1 ~ 3.6%, sorbitan sesquioleate 1 ~ 3%, cyclopenta siloxanes/dimethiconol 0.2 ~ 0.5%, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer 0.2 ~ 0.4%, Magnesiumaluminumsilicate 0.1 ~ 0.2%, xanthan gum 0.1 ~ 0.2%, polyglutamic acid 0.02 ~ 0.1%, propylene glycol 2 ~ 3%, butanediol 3 ~ 5%, phenoxyethanol/Sensiva SC50 0.2 ~ 0.3%, ethohexadiol/Sensiva SC50 0.1%, sodium hydroxide 0.075 ~ 0.15%, water surplus.
As one preferred embodiment, pigment breast of the present invention is made up of the component of following percentage by weight:
Ultra-fine silicon process titanium dioxide dispersion pulp 4 ~ 5%, silicon process nanometer titanium dioxide dispersion pulp 5%, ethylhexyl methoxy cinnamate 3%, silicon process iron oxide yellow dispersion pulp 0.30 ~ 0.35%, silicon process iron oxide red dispersion pulp 0.12 ~ 0.16%, silicon process iron oxide black dispersion pulp 0.06 ~ 0.08%, cyclopenta siloxanes/trimethyl silicane alcoxyl base esters of silicon acis 1 ~ 2%, sorbitan sesquioleate 2 ~ 3%, cyclopenta siloxanes/dimethiconol 0.3 ~ 0.5%, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer 0.3 ~ 0.4%, Magnesiumaluminumsilicate 0.15 ~ 0.2%, xanthan gum 0.15 ~ 0.2%, polyglutamic acid 0.05 ~ 0.1%, propylene glycol 2 ~ 3%, butanediol 3%, phenoxyethanol/Sensiva SC50 0.3%, ethohexadiol/Sensiva SC50 0.1%, sodium hydroxide 0.11 ~ 0.15%, water surplus.
Present invention also offers the preparation method of described pigment breast, its step is as follows:
(1) by ultra-fine silicon process titanium dioxide dispersion pulp, silicon process nanometer titanium dioxide dispersion pulp, ethylhexyl methoxy cinnamate, silicon process iron oxide yellow dispersion pulp, silicon process iron oxide red dispersion pulp, silicon process iron oxide black dispersion pulp, cyclopenta siloxanes/trimethyl silicane alcoxyl base esters of silicon acis, sorbitan sesquioleate, cyclopenta siloxanes/dimethiconol mix homogeneously, homogenous disperse is even;
(2) reserved suitable quantity of water, under homogeneous state, the mixture of step (1) is added in the mixture of acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, Magnesiumaluminumsilicate, xanthan gum, polyglutamic acid, propylene glycol, butanediol, phenoxyethanol/Sensiva SC50, ethohexadiol/Sensiva SC50 and remaining water, homogenizing 5 ~ 10min, add the suitable quantity of water and sodium hydroxide that reserve, homogenizing 5 ~ 10min, stirs.
Compared with prior art, pigment breast of the present invention has the following advantages:
1, Gel mile of shape water profit quality, water content, up to more than 75%, has unique salubrious use sense, and moistening effect is lasting, effectively can keep dressing 8 hours de-adornments, and makes adornment sense silk soft thin.Use rear skin more natural, more penetrating;
2, there is splendid smear, slim and graceful, ventilative, gentle, very paste skin, adornment sense nature;
3, waterproof formula, even if hot summer also lasting de-adornment, and can not be infected with medicated clothing after waiting to do;
4, easily clean, do not need to use makeup remover makeup removing, only need with general cleansing milk with regard to energy wash clean, face and health all can use;
5, control oil, anti-antiperspirant excellent performance.
Accompanying drawing explanation
Fig. 1 is organoleptic analysis's assessment result of the embodiment of the present invention 1 ~ 3.
Fig. 2 is the water-resistance assessment result of the embodiment of the present invention 1 ~ 3.
Fig. 3 is the control oil of the embodiment of the present invention 1 ~ 3, anti-antiperspirant assessment result.
Detailed description of the invention
Below in conjunction with the drawings and specific embodiments, technical scheme of the present invention is described in further detail, but protection scope of the present invention is not limited in following examples.
Weigh each component according to following percentage by weight, following component is all bought by commercial channel and is obtained.
Make the pigment breast of embodiment 1 ~ 3, its step is as follows:
(1) by A group component mix homogeneously, homogenous disperse is even;
(2) add in B group component by A group component under homogeneous state, homogenizing 5 ~ 10min, add C group component, homogenizing 5 ~ 10min, stirs;
(3) discharging after outward appearance detection is qualified.
One, Product Safety assessment (human skin patch result)
(1) tested material: cosmetics finished product (the pigment breast of embodiment 1 ~ 3), commercially available common pigment breast is reference examples.
(2) negative control: blank.
(3) experimenter: totally 30 people, male 10 people, female 20 people, at 18 ~ 30 years old age, meets experimenter and volunteers inclusion criteria.
(4) speckle method for testing: select qualified speckle examination device, with closed patch test method, tested material being about 0.02ml ~ 0.025ml is applied in speckle examination device, external special adhesive tape sticks in the bent side of experimenter's forearm, tested material is removed after 24 hours, 30min after removal tested material speckle examination device, observes dermoreaction, by its result of dermoreaction grade scale record in " cosmetics health specification " (version in 2007) after impression disappears.
(5) evaluation of result: according to the form below (skin adverse reaction grade scale) records reaction result.
(6) result of the test sees the following form (cosmetics human skin patch result):
Human skin patch result shows: in formula 1,2,3 (this patent formula), and 30 subjects skin are all negative reaction (grading system: 0 grade).According to " cosmetics health specification " (version in 2007) human body skin class paste test criterion, sample to human body without skin adverse reaction.Reference examples (commercially available domestic famous brand name foundation emulsion) has 2 experimenters to occur 1 order reaction.
Two, organoleptic analysis's assessment
(1) tested material: cosmetics finished product (the pigment breast of embodiment 1 ~ 3), commercially available common pigment breast is reference examples.
2) experimenter: totally 30 people, male 10 people, female 20 people, at 21 ~ 49 years old age, meets experimenter and volunteers inclusion criteria.
3) appraisal procedure: the sample of 70ul is applied to the back of the hand, mildly circle round with another and smear 8 times, then in the mode (0 ~ 10 point of marking, mark is higher, represents the water moisture feeling of this product, spreadability, subsides skin, naturally naked adornment sense, better by rear comfort) evaluate successively sample water moisture feeling, spreadability, subsides skin, naturally naked adornment sense, use rear comfort.
Assessment result: be coated with and add up with rear comprehensive experimenter's scoring, result as shown in Figure 1.Result shows, texture, water moisture feeling, spreadability, subsides skin, the naturally naked adornment sense of the pigment breast of the embodiment of the present invention 1 ~ 3 and be all obviously better than reference examples by rear comfort.
Three, moistening effect assessment
(1) tested material: cosmetics finished product (the pigment breast of embodiment 1 ~ 3), commercially available common pigment breast is reference examples.
(2) experimenter: totally 11 people, male 2 people, female 9 people, at 21 ~ 49 years old age, meets experimenter and volunteers inclusion criteria.
(3) appraisal procedure: experimenter left and right face smears embodiment 1,2,3 and reference examples (commercially available common foundation emulsion) respectively, with skin moisture tester measure skin use embodiment 1,2,3 and commercially available common foundation emulsion before, use the moisture value of skin after 2 hours, 4 hours, 8 hours, test result is as shown in the table:
| Test sample | Initial water score value | Use rear moisture value | Moisture value after 2 hours | Moisture value after 4 hours | Moisture value after 8 hours |
| Blank | 33.5 | / | 33.2 | 33.4 | 33.3 |
| Embodiment 1 | 32.6 | 52.5 | 52.3 | 50.2 | 51.4 |
| Embodiment 2 | 33.4 | 53.4 | 52.2 | 51.8 | 52.0 |
| Embodiment 3 | 33.8 | 55.2 | 55.1 | 53.6 | 52.5 |
| Reference examples | 33.9 | 55.6 | 42.3 | 40.2 | 37.6 |
As can be seen from the above table, embodiment 1,2,3 is compared with reference examples (commercially available common foundation emulsion), and the moistening effect of embodiment 1,2,3 is better.
Four, water-resistance assessment
Embodiment 1,2,3 and the sunscreen containing identical type and same amount, the common foundation emulsion of SPF8 is indicated for commercially available, by 11 professional test personnel according to the COLIPA way of recommendation, painting is measured with water-bath the SPF drawn after using and is carried out statistical before water-bath after 20 minutes, as shown in Figure 2.Diagram shows, the water-resistance of embodiment 1,2,3 is significantly higher than reference examples (commercially available indicate the common foundation emulsion of SPF8).
Five, control oil, the assessment of anti-antiperspirant
Look for 11 volunteers, embodiment 1,2,3 and reference examples (commercially available common foundation emulsion) 70ul is smeared respectively at left face and right face, sucked the unnecessary oils and fats of skin surface every 2 hours with oil-Absorbing Sheets in 8 hours and observe dressing, then with the mode of marking (0 ~ 10 point, mark is higher, represent that dressing is more lasting, in contrast, mark is lower, represents that the oil quantity that oil-Absorbing Sheets absorb is fewer, control oily effect better), assess.Be coated with and add up with rear comprehensive experimenter's scoring, as shown in Figure 3, embodiment 1,2,3 is more effective than reference examples (commercially available common foundation emulsion) control oil, anti-antiperspirant for result.
Claims (3)
1. a pigment breast, is characterized in that being made up of the component of following percentage by weight:
Ultra-fine silicon process titanium dioxide dispersion pulp 3 ~ 5%, silicon process nanometer titanium dioxide dispersion pulp 5%, ethylhexyl methoxy cinnamate 3%, silicon process iron oxide yellow dispersion pulp 0.25 ~ 0.35%, silicon process iron oxide red dispersion pulp 0.1 ~ 0.16%, silicon process iron oxide black dispersion pulp 0.06 ~ 0.08%, cyclopenta siloxanes/trimethyl silicane alcoxyl base esters of silicon acis 1 ~ 3.6%, sorbitan sesquioleate 1 ~ 3%, cyclopenta siloxanes/dimethiconol 0.2 ~ 0.5%, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer 0.2 ~ 0.4%, Magnesiumaluminumsilicate 0.1 ~ 0.2%, xanthan gum 0.1 ~ 0.2%, polyglutamic acid 0.02 ~ 0.1%, propylene glycol 2 ~ 3%, butanediol 3 ~ 5%, phenoxyethanol/Sensiva SC50 0.2 ~ 0.3%, ethohexadiol/Sensiva SC50 0.1%, sodium hydroxide 0.075 ~ 0.15%, water surplus.
2. pigment breast according to claim 1, is characterized in that being made up of the component of following percentage by weight:
Ultra-fine silicon process titanium dioxide dispersion pulp 4 ~ 5%, silicon process nanometer titanium dioxide dispersion pulp 5%, ethylhexyl methoxy cinnamate 3%, silicon process iron oxide yellow dispersion pulp 0.30 ~ 0.35%, silicon process iron oxide red dispersion pulp 0.12 ~ 0.16%, silicon process iron oxide black dispersion pulp 0.06 ~ 0.08%, cyclopenta siloxanes/trimethyl silicane alcoxyl base esters of silicon acis 1 ~ 2%, sorbitan sesquioleate 2 ~ 3%, cyclopenta siloxanes/dimethiconol 0.3 ~ 0.5%, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer 0.3 ~ 0.4%, Magnesiumaluminumsilicate 0.15 ~ 0.2%, xanthan gum 0.15 ~ 0.2%, polyglutamic acid 0.05 ~ 0.1%, propylene glycol 2 ~ 3%, butanediol 3%, phenoxyethanol/Sensiva SC50 0.3%, ethohexadiol/Sensiva SC50 0.1%, sodium hydroxide 0.11 ~ 0.15%, water surplus.
3. the preparation method of pigment breast described in claim 1 or 2, its step is as follows:
(1) by ultra-fine silicon process titanium dioxide dispersion pulp, silicon process nanometer titanium dioxide dispersion pulp, ethylhexyl methoxy cinnamate, silicon process iron oxide yellow dispersion pulp, silicon process iron oxide red dispersion pulp, silicon process iron oxide black dispersion pulp, cyclopenta siloxanes/trimethyl silicane alcoxyl base esters of silicon acis, sorbitan sesquioleate, cyclopenta siloxanes/dimethiconol mix homogeneously, homogenous disperse is even;
(2) reserved suitable quantity of water, under homogeneous state, the mixture of step (1) is added in the mixture of acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, Magnesiumaluminumsilicate, xanthan gum, polyglutamic acid, propylene glycol, butanediol, phenoxyethanol/Sensiva SC50, ethohexadiol/Sensiva SC50 and remaining water, homogenizing 5 ~ 10min, add the suitable quantity of water and sodium hydroxide that reserve, homogenizing 5 ~ 10min, stirs.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410808474.9A CN104434569B (en) | 2014-12-19 | 2014-12-19 | A kind of pigment breast and preparation method thereof |
| JP2015142893A JP6067069B2 (en) | 2014-12-19 | 2015-07-17 | Cream foundation and method for preparing the same |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410808474.9A CN104434569B (en) | 2014-12-19 | 2014-12-19 | A kind of pigment breast and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104434569A CN104434569A (en) | 2015-03-25 |
| CN104434569B true CN104434569B (en) | 2015-12-09 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410808474.9A Active CN104434569B (en) | 2014-12-19 | 2014-12-19 | A kind of pigment breast and preparation method thereof |
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| JP (1) | JP6067069B2 (en) |
| CN (1) | CN104434569B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104825371A (en) * | 2015-05-26 | 2015-08-12 | 广州智媛生物科技有限公司 | Makeup-free face cream containing enriched emulsion and preparation method of makeup-free face cream |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006249049A (en) * | 2005-03-14 | 2006-09-21 | Shiseido Co Ltd | Skin care composition |
| CN103919693A (en) * | 2014-03-26 | 2014-07-16 | 上海得高实业有限公司 | Water dispersible powder syrup for oleophylic treatment and product applying powder syrup |
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- 2014-12-19 CN CN201410808474.9A patent/CN104434569B/en active Active
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| Publication number | Publication date |
|---|---|
| JP2016117704A (en) | 2016-06-30 |
| JP6067069B2 (en) | 2017-01-25 |
| CN104434569A (en) | 2015-03-25 |
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Effective date of registration: 20210420 Address after: Room 2213, 2215, 2218, 2220, 2222, 22 / F, Wuyang Dongcheng Plaza, 111-115 siyouxin Road, Yuexiu District, Guangzhou, Guangdong 510000 Patentee after: Guangzhou ganfei Biotechnology Co.,Ltd. Address before: 18, 510000, 111-115, 20 and 22 rooms, 22 floor, Wuyang East Square, right new road, Yuexiu District temple, Guangzhou, Guangdong Patentee before: GUANGZHOU SHEENCOLOR COSMETICS Co.,Ltd. |