CN104432503B - A kind of slow-release aroma cigarette cored wire and its preparation and application - Google Patents
A kind of slow-release aroma cigarette cored wire and its preparation and application Download PDFInfo
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- CN104432503B CN104432503B CN201310428743.4A CN201310428743A CN104432503B CN 104432503 B CN104432503 B CN 104432503B CN 201310428743 A CN201310428743 A CN 201310428743A CN 104432503 B CN104432503 B CN 104432503B
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- cored wire
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- release
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/08—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent
- A24D3/10—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent of cellulose or cellulose derivatives
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
Abstract
The present invention relates to cigarette material technical fields, and in particular to a kind of slow-release aroma cigarette cored wire and its preparation and application.The preparation method of slow-release aroma cigarette cored wire of the present invention is as follows：1）Alcohol soluble high molecular material is dissolved in ethanol solution, obtains skeleton solution；Edible wine is dissolved in wetting agent, obtains mixing wine liquid；Mixing wine liquid with skeleton solution is mixed, obtains aroma liquid；2）Cored wire is made in short fiber of plant twisting；3）Continue to step 1）Aroma liquid carry out ultrasonic mixing, and by step 2）Cored wire obtained, which is placed in the aroma liquid in ultrasonic mixing, carries out ultrasonic dip-coating；4）By step 3）Cored wire room temperature after ultrasonic dip-coating air-dries, and slow-release aroma cigarette cored wire is made.The had good sustained release effect of the slow-release aroma cigarette cored wire of the present invention, the filter tip containing the cored wire can make consumer's smoking cigarette have apparent aroma mouthfeel, and realize unique odor type style of cigarette.
Description
Technical field
The present invention relates to cigarette material technical fields, and in particular to a kind of slow-release aroma cigarette cored wire and its preparation and should
With.
Background technology
Chinese-style cigarette style characteristic is always the basis that cigarette industry is paid attention to, and so-called Chinese-style cigarette is in satisfaction
State cigarette consumption person currently and potential consumption demand, with peculiar fragrance style and taste profile, the cigarette for possessing core technology,
High fragrance, low tar, less harmful are always the core purpose of cigarette industry.
Chinese-style cigarette has unique aromatic style and taste profile, related with raw material resources, tobacco leaf formulation design, together
When also have inseparable contact with flavoring and casing.And distinct Chinese characteristics natural perfume material it is a large amount of using also make Chinese-style cigarette from
Smell it is fragrant have significant difference to odor characteristic and the cigarette such as English, American, Japanese, consumer can be allowed to divide in the first reaction sucked
It discerns and, and non-burning flavoring and lasting are that a cigarette carries fragrant principal contradiction at present, are especially added again as Maotai
Tool high volatile liquid when, lasting is just particularly important, and slow-release aroma cigarette cored wire of the present invention is by Maotai
Wine and natural porous fiber and alcohol soluble high molecular material reach the abundant combination of Maotai and fiber by ultrasonic dip-coating, and
Cystic structures are formed with alcohol soluble high molecular when dry, each woollen yarn knitting and micropore of cored wire is filled in, aroma is made slowly to discharge, are solved
Perfuming cigarette and lasting contradiction.
The material of countless fine filoplumes and the natural cigarette cored wire of countless micropores is selected during chosen material as natural plant fibre,
By woollen yarn knitting, unwinding, knit again, unwind the step of it is blended, entire cored wire is made to have more small and duct high specific surface area,
The wetting agent that more infiltration has been adsorbed while sorbing liquor essence and has been entered, and Maotai is formed into cryptomere knot in drying
Structure due to infiltrating through fibrous inside using ultrasonic dipping process, aroma essence and the wetting micro- material of agent molecule, has sustained release well
Effect, there is a gas permeability for not influencing entire cored wire, cored wire can be selected in sorbing liquor essence wetting in absorption wetting agent into
Point, make cigarette when discharging Maotai aroma characteristic perfume, increase cigarette moisture feeling, thorn dry sense of the cigarette in suction can be improved, increased
Add comfort level during cigarette smoking, improve the sensory experience of smoker.
What aroma cigarette cored wire imparted tobacco product beautiful and comfortable smells fragrant and apparent characteristic perfume and miscellaneous covering
There is great role in gas, mitigation irritation and improvement pleasant impression.Research is combined, not only the flavoring of science, moreover it is possible to prominent product
Personalized style.
Number of patent application 200810058833.8 discloses a kind of filter tip delay color changing core and preparation method, and this method exists
Coating and dyeing, are made filter tip delay color changing core on existing natural or chemical fibre material, and this method is inhaled by core
Color changes after alkali grain and oxidation state aerosol particle in attached cigarette flue gas aerosol, forms apparent appearance and carries out
It is anti-fake, but cigarette characteristic perfume and suction quality without improvement result.
The content of the invention
The defects of it is an object of the invention to overcome the prior art, provides a kind of slow-release aroma cigarette cored wire, slow-release
Aroma cigarette filter and its preparation and application；The slow-release aroma cigarette cored wire and filter tip of the present invention can prepare special with aroma
The cigarette of color fragrance.
The present invention discloses a kind of preparation method of slow-release aroma cigarette cored wire first, and step is as follows：
1）Alcohol soluble high molecular material is dissolved in ethyl alcohol, obtains skeleton solution；Edible wine is dissolved in wetting agent, is mixed
Close wine liquid；Skeleton solution with mixing wine liquid is uniformly mixed, obtains aroma liquid；
2）Carbonate plant staple fiber is twisted into cored wire；
3）To step 1）Aroma liquid carry out ultrasonic mixing, by step 2 while ultrasonic mixing）Cored wire obtained is placed in
Ultrasonic dip-coating is carried out in the aroma liquid；
4）By step 3）Cored wire room temperature after ultrasonic dip-coating air-dries, and obtains slow-release aroma cigarette cored wire.
Preferably, step 1）The alcohol soluble high molecular material is hydroxypropyl methyl cellulose, cellulosic ether（EC）, crystallite
One or more combinations in cellulose, polyvinylpyrrolidone.
More preferably, step 1）The content of alcohol soluble high molecular material is 10~50wt% in the skeleton solution.
Preferably, step 1）The edible wine is Maotai.
Preferably, step 1）The wetting agent is deionized water, absolute ethyl alcohol, propylene glycol, one kind in glycerine or more
The combination of kind.
More preferably, step 1）The weight ratio of the edible wine and wetting agent is 1：3~10.
Preferably, step 1）The skeleton solution is with mixing wine liquid weight ratio as 2~10：1.
Preferably, step 2）The short fiber of plant is from tencel, ramee, bamboo charcoal fiber, soybean fiber, bamboo pulp
One or more combinations in fiber and silk fiber.
In the prior art, short fiber of plant is generally obtained by cutting off, short fiber of plant for length range generally 10~
50cm or so.
Preferably, step 2）The specification of the cored wire is 10 4 strands~40 32 strands.Cored wire i.e. of the present invention is will to plant
Object staple fiber is spun into single thread by short fibre into yarn system, and 10~40 single thread then are merged twisting again is made strand, most
4~32 strands further and are closed into twisting again afterwards, the second twist strand of preparation is cored wire of the invention.This method is existing skill
Art, second twist strand, that is, cored wire of acquisition.
The line density of cored wire of the present invention is 160~260tex, and the twist is 450~550 number of twists/rice.The core of preparation
Thread breakage strength is 1300~2200CN/50cm.
Preferably, step 1）With step 3）The ultrasonic mixing frequency is 20~80KHz.
Step 3）In, the time of ultrasonic dip-coating is no less than 15min.
Preferably, step 3）The time of the ultrasound dip-coating is 15~60min.
Second aspect of the present invention discloses the slow-release aroma cigarette cored wire prepared using preceding method.
The specification of cored wire of the present invention is 10 4 strands~40 32 strands.
The present invention also also discloses application of the foregoing slow-release aroma cigarette cored wire in Cigarette processing field.
Third aspect present invention discloses a kind of slow-release aroma cigarette filter, is set in the slow-release aroma cigarette filter
There is foregoing slow-release aroma cigarette cored wire.
Fourth aspect present invention discloses the preparation method of foregoing slow-release aroma cigarette filter, is the work in cigarette filter rod
The slow-release aroma cigarette cored wire is implanted into industry forming step, is cut, aroma cigarette filter is made（Mouth stick）.
Preferably, the molding shaping specification of cigarette filter rod industrialization is 100mm（4 cuttings）, 120mm（4 cuttings）,
144mm（6 cuttings）.
It is selected during the natural plant fibre materials of the present invention with countless fine filoplumes and the natural cigarette cored wire of countless micropores
Material, by woollen yarn knitting, unwinding, knit again, unwind the step of it is blended, entire cored wire is made to have more small duct and higher ratio
Surface area, the wetting agent that more infiltration has been adsorbed while sorbing liquor essence and has been entered, capsule is formed by Maotai in drying
Shape structure.Since using ultrasonic dipping process, aroma essence and wetting agent molecule infiltration enter fibrous inside, there is sustained release well
Effect does not influence the gas permeability of entire cored wire；Wetting of the cored wire in sorbing liquor essence in the absorption wetting agent of meeting selectivity
Ingredient makes cigarette when discharging Maotai aroma characteristic perfume, increases cigarette moisture feeling, to improve thorn dry sense of the cigarette in suction,
Increase comfort level during cigarette smoking, improve the sensory experience of smoker.
Description of the drawings
Fig. 1：The process flow chart of slow-release aroma cigarette cored wire filter stick
Specific embodiment
With reference to embodiment, the present invention is further explained.It is to be understood that embodiment is merely to illustrate the present invention, and it is unrestricted
The scope of the present invention.
Embodiment 1
1. the preparation of slow-release aroma cigarette cored wire
1）Hydroxypropyl methyl cellulose is dissolved in ethanol solution, acquisition skeleton solution, hydroxypropyl methyl in skeleton solution
The mass percent of cellulose is 10wt%；Maotai is dissolved in deionized water：Ethyl alcohol weight ratio is 1:In 1 wetting agent, Maotai
The mass ratio of wine and wetting agent is 1:5, obtain mixing wine liquid；Skeleton solution is added in into mixing wine liquid, skeleton solution is with mixing
The mass ratio of wine liquid is 2:1,20kHz ultrasonic mixing obtains aroma liquid；
2）Soybean staple fiber and bamboo charcoal staple fiber are spun into single thread by short fibre into yarn system, then again by 10 lists
Yarn merge twisting strand is made, finally again by 20 strands further and close twisting, obtain cored wire；
3）Continue to step 1）Aroma liquid carry out ultrasonic mixing, and by step 2）Cored wire obtained is placed in ultrasonic mixing
Aroma liquid in carry out ultrasonic dip-coating 20min；
4）By step 3）Cored wire room temperature after ultrasonic dip-coating air-dries, and slow-release aroma cigarette cored wire is made.
Step 4）The slow-release aroma cigarette cored wire for preparing after room temperature drying, internal alcohol soluble high molecular material with it is porous
Plant fiber, Maotai form small cystic structures together, enhance the sustained release efficiency of cored wire.
2. the preparation of slow-release aroma cigarette cored wire filter stick：
To be implanted into foregoing slow-release aroma cigarette cored wire in the industrialization forming step of cigarette filter rod, aroma cigarette is made
Cored wire mouth stick, shaping specification are 100mm（4 cuttings）.Then it is installed on the cigarette of box mark 12mg and is evaluated, evaluation result is shown in
Table 1-2.
Embodiment 2
1. the preparation of slow-release aroma cigarette cored wire
1）Hydroxypropyl methyl cellulose is dissolved in ethanol solution, acquisition skeleton solution, hydroxypropyl methyl in skeleton solution
The mass percent of cellulose is 20wt%；Maotai is dissolved in deionized water：Propylene glycol weight ratio is 1:In 2 wetting agent, thatch
The mass ratio of platform wine and wetting agent is 1:3, obtain mixing wine liquid；Skeleton solution is added in into mixing wine liquid, skeleton solution is with mixing
The mass ratio for closing wine liquid is 10:1,60kHz ultrasonic mixing obtains aroma liquid；
2）Ramie staple fiber and bamboo charcoal staple fiber are spun into single thread, 40 single thread then are merged twisting again is made stock
Line, finally again by 4 strands further and close twisting, obtain cored wire；
3）Continue to step 1）Aroma liquid carry out ultrasonic mixing, and by step 2）Cored wire obtained is placed in ultrasonic mixing
Aroma liquid in carry out ultrasonic dip-coating 40min；
4）By step 3）Cored wire room temperature after ultrasonic dip-coating air-dries, and slow-release aroma cigarette cored wire is made.
2. the preparation of slow-release aroma cigarette cored wire filter stick：
To be implanted into foregoing slow-release aroma cigarette cored wire in the industrialization forming step of cigarette filter rod, aroma cigarette is made
Cored wire mouth stick, shaping specification are 100mm（4 cuttings）.Then it is installed on the cigarette of box mark 12mg and is evaluated, evaluation result is shown in
Table 1-2.
Embodiment 3
1. the preparation of slow-release aroma cigarette cored wire
1）Ethyl cellulose is dissolved in ethanol solution, acquisition skeleton solution, the quality of ethyl cellulose in skeleton solution
Percentage is 50wt%；Maotai is dissolved in deionized water：Propylene glycol is 1:In 1 wetting agent, the quality of Maotai and wetting agent
Than for 1:10, obtain mixing wine liquid；Skeleton solution is added in into mixing wine liquid, skeleton solution is 6 with the mass ratio for mixing wine liquid:
1,80kHz ultrasonic mixing obtains aroma liquid；
2）Soybean staple fiber and day wire short fiber are spun into single thread, 20 single thread then are merged twisting again is made stock
Line, finally again by 32 strands further and close twisting, obtain cored wire；
3）Continue to step 1）Aroma liquid carry out ultrasonic mixing, and by step 2）Cored wire obtained is placed in ultrasonic mixing
Aroma liquid in carry out ultrasonic dip-coating 60min；
4）By step 3）Cored wire room temperature after ultrasonic dip-coating air-dries, and slow-release aroma cigarette cored wire is made.
2. the preparation of slow-release aroma cigarette cored wire filter stick：
To be implanted into foregoing slow-release aroma cigarette cored wire in the industrialization forming step of cigarette filter rod, aroma cigarette is made
Cored wire mouth stick, shaping specification are 100mm（4 cuttings）.Then it is installed on the cigarette of box mark 12mg and is evaluated, evaluation result is shown in
Table 1-2.
Embodiment 4
1. the preparation of slow-release aroma cigarette cored wire
1）Ethyl cellulose is dissolved in ethanol solution, acquisition skeleton solution, the quality of ethyl cellulose in skeleton solution
Percentage is 40wt%；Maotai is dissolved in deionized water, the mass ratio of Maotai and deionized water is 1:7, obtain mixing wine
Liquid；Skeleton solution is added in into mixing wine liquid, skeleton solution is 2 with the mass ratio for mixing wine liquid:1,50kHz ultrasonic mixing, is obtained
Obtain aroma liquid；
2）Bamboo charcoal staple fiber and day wire short fiber are spun into single thread, 10 single thread then are merged twisting again is made strand,
Finally again by 10 strands further and close twisting, obtain cored wire；
3）Continue to step 1）Aroma liquid carry out ultrasonic mixing, and by step 2）Cored wire obtained is placed in ultrasonic mixing
Aroma liquid in carry out ultrasonic dip-coating 60min；
4）By step 3）Cored wire room temperature after ultrasonic dip-coating air-dries, and slow-release aroma cigarette cored wire is made.
2. the preparation of slow-release aroma cigarette cored wire filter stick：
To be implanted into foregoing slow-release aroma cigarette cored wire in the industrialization forming step of cigarette filter rod, aroma cigarette is made
Cored wire mouth stick, shaping specification are 100mm（4 cuttings）.Then it is installed on the cigarette of box mark 12mg and is evaluated, evaluation result is shown in
Table 1-2.
Embodiment 5
1. the preparation of slow-release aroma cigarette cored wire
1）Microcrystalline cellulose is dissolved in ethanol solution, acquisition skeleton solution, the quality of microcrystalline cellulose in skeleton solution
Percentage is 15wt%；Maotai is dissolved in water：Ethyl alcohol is 3:In 1 wetting agent, the mass ratio of Maotai and wetting agent is 1:9,
Obtain mixing wine liquid；Skeleton solution is added in into mixing wine liquid, skeleton solution is 7.5 with the mass ratio for mixing wine liquid:1,35kHz
Ultrasonic mixing obtains aroma liquid；
2）Ramie staple fiber is spun into single thread, 30 single thread then are merged twisting again is made strand, finally again by 4
Strand is further and closes twisting, obtains cored wire；
3）Continue to step 1）Aroma liquid carry out ultrasonic mixing, and by step 2）Cored wire obtained is placed in ultrasonic mixing
Aroma liquid in carry out ultrasonic dip-coating 20min；
4）By step 3）Cored wire room temperature after ultrasonic dip-coating air-dries, and slow-release aroma cigarette cored wire is made.
2. the preparation of slow-release aroma cigarette cored wire filter stick：
To be implanted into foregoing slow-release aroma cigarette cored wire in the industrialization forming step of cigarette filter rod, aroma cigarette is made
Cored wire mouth stick, shaping specification are 100mm（4 cuttings）.Then it is installed on the cigarette of box mark 12mg and is evaluated, evaluation result is shown in
Table 1-2.
Embodiment 6
1. the preparation of slow-release aroma cigarette cored wire
1）Vinylpyrrolidone and ethyl cellulose are dissolved in ethanol solution, acquisition skeleton solution, second in skeleton solution
The mass percent of base cellulose is 25wt%；Maotai is dissolved in deionized water, the mass ratio of Maotai and deionized water is
1:5, obtain mixing wine liquid；Skeleton solution is added in into mixing wine liquid, skeleton solution is 10 with the mass ratio for mixing wine liquid:1,
20kHz ultrasonic mixings obtain aroma liquid；
2）Bamboo charcoal staple fiber, short silk fiber and day wire short fiber are spun into single thread, then again merge 12 single thread
Twisting strand is made, finally again by 20 strands further and close twisting, obtain cored wire；
3）Continue to step, 1）Aroma liquid carry out ultrasonic mixing, and by step 2）Cored wire obtained is placed in ultrasonic mixing
In aroma liquid in carry out ultrasonic dip-coating 15min；
4）By step 3）Cored wire room temperature after ultrasonic dip-coating air-dries, and slow-release aroma cigarette cored wire is made.
2. the preparation of slow-release aroma cigarette cored wire filter stick：
To be implanted into foregoing slow-release aroma cigarette cored wire in the industrialization forming step of cigarette filter rod, aroma cigarette is made
Cored wire mouth stick, shaping specification are 100mm（4 cuttings）.Then it is installed on the cigarette of box mark 12mg and is evaluated, evaluation result is shown in
Table 1-2.
Embodiment 7
1. the preparation of slow-release aroma cigarette cored wire
1）Microcrystalline cellulose is dissolved in ethanol solution, acquisition skeleton solution, the quality of microcrystalline cellulose in skeleton solution
Percentage is 30wt%；Maotai is dissolved in deionized water：Ethyl alcohol：Propylene glycol is 1:1:In 1 wetting agent, mixing wine liquid is obtained；
Skeleton solution is added in into mixing wine liquid, skeleton solution is 3 with the mass ratio for mixing wine liquid:Isosorbide-5-Nitrae 0kHz ultrasonic mixings obtain wine
Fragrant liquid；
2）Bamboo pulp staple fiber is spun into single thread, 10 single thread then are merged twisting again is made strand, finally again by 32
Root strand is further and closes twisting, obtains cored wire；
3）Continue to step 1）Aroma liquid carry out ultrasonic mixing, and by step 2）Cored wire obtained is placed in ultrasonic mixing
Aroma liquid in carry out ultrasonic dip-coating 60min；
4）By step 3）Cored wire room temperature after ultrasonic dip-coating air-dries, and slow-release aroma cigarette cored wire is made.
2. the preparation of slow-release aroma cigarette cored wire filter stick：
To be implanted into foregoing slow-release aroma cigarette cored wire in the industrialization forming step of cigarette filter rod, aroma cigarette is made
Cored wire mouth stick, shaping specification are 100mm（4 cuttings）.Then it is installed on the cigarette of box mark 12mg and is evaluated, evaluation result is shown in
Table 1-2.
Embodiment 8
1. the preparation of slow-release aroma cigarette cored wire
1）Hydroxypropyl methyl cellulose is dissolved in ethanol solution, acquisition skeleton solution, hydroxypropyl methyl in skeleton solution
The mass percent of cellulose is 15wt%；Maotai is dissolved in deionized water：Ethyl alcohol is 1:In 3 wetting agent, Maotai and profit
The mass ratio of humectant is 1:8, obtain mixing wine liquid；Skeleton solution is added in into mixing wine liquid, skeleton solution is with mixing wine liquid
Mass ratio is 2:1,20kHz ultrasonic mixing obtains aroma liquid；
2）Bamboo charcoal staple fiber and bamboo pulp staple fiber are spun into single thread, 20 single thread then are merged twisting again is made stock
Line, finally again by 20 strands further and close twisting, obtain cored wire；
3）Continue to step 1）Aroma liquid carry out ultrasonic mixing, and by step 2）Cored wire obtained is placed in ultrasonic mixing
Aroma liquid in carry out ultrasonic dip-coating 90min；
4）By step 3）Cored wire room temperature after ultrasonic dip-coating air-dries, and slow-release aroma cigarette cored wire is made.
2. the preparation of slow-release aroma cigarette cored wire filter stick：
To be implanted into foregoing slow-release aroma cigarette cored wire in the industrialization forming step of cigarette filter rod, aroma cigarette is made
Cored wire mouth stick, shaping specification are 100mm（4 cuttings）.Then it is installed on the cigarette of box mark 12mg and is evaluated, evaluation result is shown in
Table 1-2.
Embodiment 9
1. the preparation of slow-release aroma cigarette cored wire
1）Ethyl cellulose is dissolved in ethanol solution, acquisition skeleton solution, the quality of ethyl cellulose in skeleton solution
Percentage is 10wt%；Maotai is dissolved in deionized water：Ethyl alcohol：Glycerine is 1:1:In 1 wetting agent, mixing wine liquid is obtained；
Skeleton solution is added in into mixing wine liquid, skeleton solution is 2.5 with the mass ratio for mixing wine liquid:1,30kHz ultrasonic mixing obtains
Aroma liquid；
2）Day wire short fiber and short silk fiber are spun into single thread, 40 single thread then are merged twisting again is made stock
Line, finally again by 5 strands further and close twisting, obtain cored wire；
3）Continue to step 1）Aroma liquid carry out ultrasonic mixing, and by step 2）Cored wire obtained is placed in ultrasonic mixing
Aroma liquid in carry out ultrasonic dip-coating 30min；
4）By step 3）Cored wire room temperature after ultrasonic dip-coating air-dries, and slow-release aroma cigarette cored wire is made.
2. the preparation of slow-release aroma cigarette cored wire filter stick：
To be implanted into foregoing slow-release aroma cigarette cored wire in the industrialization forming step of cigarette filter rod, aroma cigarette is made
Cored wire mouth stick, shaping specification are 100mm（4 cuttings）.Then it is installed on the cigarette of box mark 12mg and is evaluated, evaluation result is shown in
Table 1-2.
Embodiment 10
Fume indication is carried out to slow-release aroma cigarette cored wire filter stick prepared by embodiment 1-9 and inhales the detection of taste description,
The evaluation criterion for inhaling taste description is GB5006.4-2005, and experimental result is shown in Table 1-2.
1 fume indication of table
Table 2 inhales taste description
Claims (5)
1. a kind of preparation method of slow-release aroma cigarette cored wire, step are as follows：
1) alcohol soluble high molecular material is dissolved in ethyl alcohol, obtains skeleton solution；Edible wine is dissolved in wetting agent, obtains mixing wine
Liquid；Skeleton solution with mixing wine liquid is uniformly mixed, obtains aroma liquid；
2) carbonate plant staple fiber is twisted into cored wire；
3) ultrasonic mixing is carried out to the aroma liquid of step 1), be placed in cored wire made from step 2) while ultrasonic mixing described
Ultrasonic dip-coating is carried out in aroma liquid；
4) the cored wire room temperature after the ultrasonic dip-coating of step 3) is air-dried, obtains slow-release aroma cigarette cored wire；
Step 1) the alcohol soluble high molecular material is hydroxypropyl methyl cellulose, cellulosic ether, microcrystalline cellulose, polyvinyl
One or more combinations in pyrrolidones；The wetting agent is deionized water, in absolute ethyl alcohol, propylene glycol, glycerine
One or more combinations；
The content of alcohol soluble high molecular material is 10~50wt% in step 1) the skeleton solution；The edible wine and wetting agent
Weight ratio is 1：3~10；
Step 1) the skeleton solution is with mixing wine liquid weight ratio as 2~10：1；
Step 2) the short fiber of plant derives from tencel, ramee, bamboo charcoal fiber, soybean fiber, bamboo pulp fiber and silk
One or more combinations in fiber；
The specification of the step 2) cored wire is 10 4 strands~40 32 strands；The line density of the cored wire is 160~260tex, is twisted with the fingers
It spends for 450~550 number of twists/rice.
2. preparation method as described in claim 1, which is characterized in that step 3) the ultrasonic mixing frequency is 20~80KHz.
3. a kind of slow-release aroma cigarette cored wire is prepared using claim 1-2 any claim the methods.
4. a kind of slow-release aroma cigarette filter, which is characterized in that the slow-release aroma cigarette filter includes requirement 3 of having the right
The slow-release aroma cigarette cored wire.
5. the preparation method of slow-release aroma cigarette filter described in claim 4 is the industrialization forming step in cigarette filter rod
Slow-release aroma cigarette filter is made in slow-release aroma cigarette cored wire described in middle implantation claim 3, cutting.
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| CN106387994A (en) * | 2016-08-31 | 2017-02-15 | 刘迎春 | Cigarette filter stick containing controlled-release spice core wire |
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| CN109875113B (en) * | 2019-04-17 | 2021-08-03 | 云南中烟工业有限责任公司 | Graphene-based cigarette core line and preparation method and application thereof |
| CN110574958A (en) * | 2019-10-12 | 2019-12-17 | 湖北中烟工业有限责任公司 | Process for improving spreading rate of reconstituted tobacco |
| CN111808767B (en) * | 2020-05-28 | 2023-02-28 | 重庆中烟工业有限责任公司 | Microbial preparation for improving tobacco leaf quality |
| CN115039914A (en) * | 2022-07-07 | 2022-09-13 | 天津工业大学 | Cooling belt-shaped fabric and preparation method and application thereof |
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