CN104432503A - Sustained-released-type liquor aroma cigarette core line and preparation and application thereof - Google Patents
Sustained-released-type liquor aroma cigarette core line and preparation and application thereof Download PDFInfo
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- CN104432503A CN104432503A CN201310428743.4A CN201310428743A CN104432503A CN 104432503 A CN104432503 A CN 104432503A CN 201310428743 A CN201310428743 A CN 201310428743A CN 104432503 A CN104432503 A CN 104432503A
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- cigarette
- heart yearn
- aroma
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- spacetabs type
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/08—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent
- A24D3/10—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent of cellulose or cellulose derivatives
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention relates to the technical field of cigarette materials, in particular to a sustained-released-type liquor aroma cigarette core line and a preparation method and application thereof. The preparation method of the sustained-released-type liquor aroma cigarette core line comprises the following steps that (1) alcohol-soluble high polymer materials are dissolved in an alcoholic solution to obtain a skeleton solution; edible wine is dissolved in a wetting agent to obtain blending liquid, and the blending liquid and the skeleton solution are mixed to obtain a liquor aroma solution; (2) short plant fibers are twisted to form the core line; (3) ultrasonic mixing is carried out continuously on the liquor aroma solution obtained in the step (1), and the core line obtained in the step (2) is arranged in the liquor aroma solution obtained after the ultrasonic mixing for ultrasonic dip-coating; (4) air drying is carried out on the core line obtained after the ultrasonic dip-coating in the step (3) at normal temperature to obtain the sustained-released-type liquor aroma cigarette core line. The sustained-released-type liquor aroma cigarette core line is good in sustained-released effect, a consumer can taste the obvious liquor aroma when smoking a cigarette through a filter tip containing the core line, and the unique cigarette aroma style is achieved.
Description
Technical field
The present invention relates to cigarette material technical field, be specifically related to a kind of spacetabs type aroma cigarette heart yearn and Synthesis and applications thereof.
Background technology
Chinese-style cigarette style characteristic is the basis that cigarette industry is paid attention to always, so-called Chinese-style cigarette, the cigarette that can meet the current and potential consumption demand of Chinese cigarette consumer exactly, have peculiar fragrance style and taste profile, have core technology, high fragrance, low tar, less harmful are the core objects of cigarette industry always.
Chinese-style cigarette there is unique aromatic style and taste profile, design relevant with raw material resources, tobacco leaf formulation, while also have inseparable contacting with flavoring and casing.And a large amount of uses of distinct Chinese characteristics natural perfume material also make Chinese-style cigarette fragrant to odor characteristic and English from smelling, American, the Japanese cigarette that waits has obvious difference, consumer can be allowed to distinguish in first reaction of sucking, and non-burning perfuming and lasting are that a cigarette carries fragrant principal contradiction at present, when adding the high-volatile liquid of tool as Maotai especially again, lasting just seems particularly important, Maotai and natural porous fiber and alcohol soluble high molecular material are reached the abundant combination of Maotai and fiber by ultrasonic dip-coating by the spacetabs type aroma cigarette heart yearn that the present invention relates to, and when drying and alcohol soluble high molecular form cystic structures, be filled in each woollen yarn knitting and micropore of heart yearn, make aroma slow releasing, solve perfuming cigarette and lasting contradiction.
The material selecting countless fine filoplume and countless micropore natural cigarette heart yearn during chosen material is natural plant fibre, by woollen yarn knitting, unwinding, knit again, the step blending of unwinding, make the more small and duct high specific surface area of whole heart yearn tool, more infiltration has been adsorbed and the wetting agent entered while sorbing liquor essence, and Maotai is formed cystic structures when drying, owing to utilizing ultrasonic dipping process, aroma essence and the micro-material of wetting agent molecule infiltrate through fibrous inside, there is good slow releasing function, there is the gas permeability not affecting whole heart yearn, the moistening ingredients of heart yearn when sorbing liquor essence in meeting adsorption selection wetting agent, make cigarette when discharging Maotai aroma characteristic perfume, increase cigarette moisture feeling, the thorn dry sense of cigarette when aspirating can be improved, add comfort level during cigarette smoking, improve the sensory experience of smoker.
What aroma cigarette heart yearn imparted tobacco product beautiful and comfortable smells perfume (or spice) and obvious characteristic perfume and covering assorted gas, abirritate, and improves in pleasant impression and have great role.Research combined, the not only perfuming of science, can also give prominence to the personalized style of product.
Number of patent application 200810058833.8 discloses a kind of filter tip delay color changing core and preparation method, the method is coating and dyeing on existing natural or chemical fibre material, obtained filter tip delay color changing core, the method is changed by color after the alkali grain in core absorption cigarette flue gas aerosol and oxidation state aerosol particle, forming obvious outward appearance carries out false proof, but at the characteristic perfume of cigarette and suction quality without improvement result.
In prior art, short fiber of plant generally obtains by cutting off, and short fiber of plant is that length range is generally at about 10 ~ 50cm.
Preferably, step 2) specification of described heart yearn is 10 4 strands ~ 40 32 strands.Namely heart yearn of the present invention is that short fiber of plant is spun into single thread through short fibre into yarn system, and then 10 ~ 40 single thread are merged to add be twisted into strand, last again by 4 ~ 32 strands further and close twisting, the second twist strand of preparation is heart yearn of the present invention.The method is prior art, the second twist strand of acquisition and heart yearn.
The line density of heart yearn of the present invention is 160 ~ 260tex, and the twist is 450 ~ 550 number of twists/rice.The heart yearn ultimate strength of preparation is 1300 ~ 2200CN/50cm.
Preferably, ultrasonic hybrid frequency described in step 1) and step 3) is 20 ~ 80KHz.
In step 3), the time of ultrasonic dip-coating is for being no less than 15min.
Preferably, the time of ultrasonic dip-coating described in step 3) is 15 ~ 60min.
Second aspect present invention discloses the spacetabs type aroma cigarette heart yearn adopting preceding method to prepare.
The specification of heart yearn of the present invention is 10 4 strands ~ 40 32 strands.
The present invention also also discloses the application of aforementioned spacetabs type aroma cigarette heart yearn in Cigarette processing field.
Third aspect present invention discloses a kind of spacetabs type aroma cigarette filter, is provided with aforementioned spacetabs type aroma cigarette heart yearn in described spacetabs type aroma cigarette filter.
Fourth aspect present invention discloses the preparation method of aforementioned spacetabs type aroma cigarette filter, for implanting described spacetabs type aroma cigarette heart yearn in the industrialization forming step of cigarette filter rod, cuts, obtained aroma cigarette filter (mouth rod).
Preferably, the shaping shaping specification of described cigarette filter rod industrialization is that 100mm(4 cuts), 120mm(4 cuts), 144mm(6 cuts).
The material with countless fine filoplume and the natural cigarette heart yearn of countless micropore is selected when natural plant fibre of the present invention is drawn materials, by woollen yarn knitting, unwinding, knit again, the step blending of unwinding, make the more small duct of whole heart yearn tool and high specific surface area, while sorbing liquor essence, adsorb more infiltration and the wetting agent that enters, Maotai has been formed cystic structures when drying.Owing to utilizing ultrasonic dipping process, aroma essence and wetting agent molecule infiltration enter fibrous inside, have good slow releasing function, do not affect the gas permeability of whole heart yearn; Heart yearn optionally can adsorb the moistening ingredients in wetting agent when sorbing liquor essence, making cigarette when discharging Maotai aroma characteristic perfume, increasing cigarette moisture feeling, to improve the thorn dry sense of cigarette when aspirating, increase comfort level during cigarette smoking, improve the sensory experience of smoker.
Summary of the invention
The object of the invention is to the defect overcoming prior art, a kind of spacetabs type aroma cigarette heart yearn, spacetabs type aroma cigarette filter and Synthesis and applications thereof are provided; Spacetabs type aroma cigarette heart yearn of the present invention and filter tip can prepare the cigarette with aroma characteristic fragrance.
First the present invention discloses a kind of preparation method of spacetabs type aroma cigarette heart yearn, and step is as follows:
1) alcohol soluble high molecular material is dissolved in ethanol, obtains skeleton solution; Edible wine is dissolved in wetting agent, obtains mixing wine liquid; Skeleton solution is mixed with mixing wine liquid, obtains aroma liquid;
2) carbonate plant short fiber is twisted into heart yearn;
3) ultrasonic mixing being carried out, by step 2 while ultrasonic mixing to the aroma liquid of step 1)) obtained heart yearn is placed in described aroma liquid and carries out ultrasonic dip-coating;
4) by air-dry for the heart yearn normal temperature after ultrasonic for step 3) dip-coating, spacetabs type aroma cigarette heart yearn is obtained.
Preferably, alcohol soluble high molecular material described in step 1) is one or more the combination in hydroxypropyl methylcellulose, cellulosic ether (EC), microcrystalline cellulose, PVP.
More excellent, in skeleton solution described in step 1), the content of alcohol soluble high molecular material is 10 ~ 50wt%.
Preferably, edible wine described in step 1) is Maotai.
Preferably, wetting agent described in step 1) is one or more the combination in deionized water, absolute ethyl alcohol, propane diols, glycerine.
More excellent, the weight ratio of edible wine described in step 1) and wetting agent is 1:3 ~ 10.
Preferably, skeleton solution described in step 1) is 2 ~ 10:1 with mixing wine liquid weight ratio.
Preferably, step 2) described short fiber of plant derives from one or more combination in sky silk, ramee, bamboo-carbon fibre, fibre and soya, bamboo pulp fiber and silk fiber.
Accompanying drawing explanation
Fig. 1: the process chart of spacetabs type aroma cigarette heart yearn filter stick
Detailed description of the invention
The present invention is set forth further below in conjunction with embodiment.Should be understood that embodiment only for illustration of the present invention, but not limit the scope of the invention.
Embodiment 1
1. the preparation of spacetabs type aroma cigarette heart yearn
1) be dissolved in ethanolic solution by hydroxypropyl methylcellulose, obtain skeleton solution, in skeleton solution, the mass percent of hydroxypropyl methylcellulose is 10wt%; Maotai is dissolved in deionized water: ethanol weight ratio is in the wetting agent of 1:1, the mass ratio of Maotai and wetting agent is 1:5, obtains mixing wine liquid; In mixing wine liquid, add skeleton solution, skeleton solution and the mass ratio mixing wine liquid are the ultrasonic mixing of 2:1,20kHz, obtain aroma liquid;
2) soybean short fiber and bamboo charcoal staple fiber are spun into single thread through short fibre into yarn system, and then 10 single thread are merged to add are twisted into strand, further again by 20 strands and close twisting, obtain heart yearn finally;
3) continuing to carry out ultrasonic mixing to the aroma liquid of step 1), and by step 2) the obtained heart yearn aroma liquid that is placed in ultrasonic mixing carries out ultrasonic dip-coating 20min;
4) by air-dry for the heart yearn normal temperature after ultrasonic for step 3) dip-coating, obtained spacetabs type aroma cigarette heart yearn.
The spacetabs type aroma cigarette heart yearn that step 4) normal temperature is prepared after drying, the alcohol soluble high molecular material of its inside forms small cystic structures together with the string of porous, Maotai, enhances the slowly-releasing usefulness of heart yearn.
2. the preparation of spacetabs type aroma cigarette heart yearn filter stick:
For implanting aforementioned spacetabs type aroma cigarette heart yearn in the industrialization forming step of cigarette filter rod, obtained aroma cigarette heart yearn mouth rod, shaping specification is that 100mm(4 cuts).Then the cigarette being installed in box mark 12mg is evaluated, and evaluation result is in Table 1-2.
Embodiment 2
1. the preparation of spacetabs type aroma cigarette heart yearn
1) be dissolved in ethanolic solution by hydroxypropyl methylcellulose, obtain skeleton solution, in skeleton solution, the mass percent of hydroxypropyl methylcellulose is 20wt%; Maotai is dissolved in deionized water: propane diols weight ratio is in the wetting agent of 1:2, the mass ratio of Maotai and wetting agent is 1:3, obtains mixing wine liquid; In mixing wine liquid, add skeleton solution, skeleton solution and the mass ratio mixing wine liquid are the ultrasonic mixing of 10:1,60kHz, obtain aroma liquid;
2) ramie short fiber and bamboo charcoal staple fiber are spun into single thread, and then 40 single thread are merged to add are twisted into strand, further again by 4 strands and close twisting, obtain heart yearn finally;
3) continuing to carry out ultrasonic mixing to the aroma liquid of step 1), and by step 2) the obtained heart yearn aroma liquid that is placed in ultrasonic mixing carries out ultrasonic dip-coating 40min;
4) by air-dry for the heart yearn normal temperature after ultrasonic for step 3) dip-coating, obtained spacetabs type aroma cigarette heart yearn.
2. the preparation of spacetabs type aroma cigarette heart yearn filter stick:
For implanting aforementioned spacetabs type aroma cigarette heart yearn in the industrialization forming step of cigarette filter rod, obtained aroma cigarette heart yearn mouth rod, shaping specification is that 100mm(4 cuts).Then the cigarette being installed in box mark 12mg is evaluated, and evaluation result is in Table 1-2.
Embodiment 3
1. the preparation of spacetabs type aroma cigarette heart yearn
1) be dissolved in ethanolic solution by ethyl cellulose, obtain skeleton solution, in skeleton solution, the mass percent of ethyl cellulose is 50wt%; Maotai is dissolved in deionized water: propane diols is in the wetting agent of 1:1, the mass ratio of Maotai and wetting agent is 1:10, obtains mixing wine liquid; In mixing wine liquid, add skeleton solution, skeleton solution and the mass ratio mixing wine liquid are the ultrasonic mixing of 6:1,80kHz, obtain aroma liquid;
2) soybean short fiber and sky wire short fiber are spun into single thread, and then 20 single thread are merged to add are twisted into strand, further again by 32 strands and close twisting, obtain heart yearn finally;
3) continuing to carry out ultrasonic mixing to the aroma liquid of step 1), and by step 2) the obtained heart yearn aroma liquid that is placed in ultrasonic mixing carries out ultrasonic dip-coating 60min;
4) by air-dry for the heart yearn normal temperature after ultrasonic for step 3) dip-coating, obtained spacetabs type aroma cigarette heart yearn.
2. the preparation of spacetabs type aroma cigarette heart yearn filter stick:
For implanting aforementioned spacetabs type aroma cigarette heart yearn in the industrialization forming step of cigarette filter rod, obtained aroma cigarette heart yearn mouth rod, shaping specification is that 100mm(4 cuts).Then the cigarette being installed in box mark 12mg is evaluated, and evaluation result is in Table 1-2.
Embodiment 4
1. the preparation of spacetabs type aroma cigarette heart yearn
1) be dissolved in ethanolic solution by ethyl cellulose, obtain skeleton solution, in skeleton solution, the mass percent of ethyl cellulose is 40wt%; Be dissolved in by Maotai in deionized water, the mass ratio of Maotai and deionized water is 1:7, obtains mixing wine liquid; In mixing wine liquid, add skeleton solution, skeleton solution and the mass ratio mixing wine liquid are the ultrasonic mixing of 2:1,50kHz, obtain aroma liquid;
2) bamboo charcoal staple fiber and sky wire short fiber are spun into single thread, and then 10 single thread are merged to add are twisted into strand, further again by 10 strands and close twisting, obtain heart yearn finally;
3) continuing to carry out ultrasonic mixing to the aroma liquid of step 1), and by step 2) the obtained heart yearn aroma liquid that is placed in ultrasonic mixing carries out ultrasonic dip-coating 60min;
4) by air-dry for the heart yearn normal temperature after ultrasonic for step 3) dip-coating, obtained spacetabs type aroma cigarette heart yearn.
2. the preparation of spacetabs type aroma cigarette heart yearn filter stick:
For implanting aforementioned spacetabs type aroma cigarette heart yearn in the industrialization forming step of cigarette filter rod, obtained aroma cigarette heart yearn mouth rod, shaping specification is that 100mm(4 cuts).Then the cigarette being installed in box mark 12mg is evaluated, and evaluation result is in Table 1-2.
Embodiment 5
1. the preparation of spacetabs type aroma cigarette heart yearn
1) be dissolved in ethanolic solution by microcrystalline cellulose, obtain skeleton solution, in skeleton solution, the mass percent of microcrystalline cellulose is 15wt%; Maotai is water-soluble: ethanol is in the wetting agent of 3:1, the mass ratio of Maotai and wetting agent is 1:9, obtains mixing wine liquid; In mixing wine liquid, add skeleton solution, skeleton solution and the mass ratio mixing wine liquid are the ultrasonic mixing of 7.5:1,35kHz, obtain aroma liquid;
2) ramie short fiber is spun into single thread, and then 30 single thread are merged to add is twisted into strand, further again by 4 strands and close twisting, obtain heart yearn finally;
3) continuing to carry out ultrasonic mixing to the aroma liquid of step 1), and by step 2) the obtained heart yearn aroma liquid that is placed in ultrasonic mixing carries out ultrasonic dip-coating 20min;
4) by air-dry for the heart yearn normal temperature after ultrasonic for step 3) dip-coating, obtained spacetabs type aroma cigarette heart yearn.
2. the preparation of spacetabs type aroma cigarette heart yearn filter stick:
For implanting aforementioned spacetabs type aroma cigarette heart yearn in the industrialization forming step of cigarette filter rod, obtained aroma cigarette heart yearn mouth rod, shaping specification is that 100mm(4 cuts).Then the cigarette being installed in box mark 12mg is evaluated, and evaluation result is in Table 1-2.
Embodiment 6
1. the preparation of spacetabs type aroma cigarette heart yearn
1) be dissolved in ethanolic solution by vinylpyrrolidone and ethyl cellulose, obtain skeleton solution, in skeleton solution, the mass percent of ethyl cellulose is 25wt%; Be dissolved in by Maotai in deionized water, the mass ratio of Maotai and deionized water is 1:5, obtains mixing wine liquid; In mixing wine liquid, add skeleton solution, skeleton solution and the mass ratio mixing wine liquid are the ultrasonic mixing of 10:1,20kHz, obtain aroma liquid;
2) bamboo charcoal staple fiber, short silk fiber and sky wire short fiber are spun into single thread, and then 12 single thread are merged to add are twisted into strand, further again by 20 strands and close twisting, obtain heart yearn finally;
3) continue step, 1) aroma liquid carry out ultrasonic mixing, and by step 2) the obtained heart yearn aroma liquid that is placed in ultrasonic mixing carries out ultrasonic dip-coating 15min;
4) by air-dry for the heart yearn normal temperature after ultrasonic for step 3) dip-coating, obtained spacetabs type aroma cigarette heart yearn.
2. the preparation of spacetabs type aroma cigarette heart yearn filter stick:
For implanting aforementioned spacetabs type aroma cigarette heart yearn in the industrialization forming step of cigarette filter rod, obtained aroma cigarette heart yearn mouth rod, shaping specification is that 100mm(4 cuts).Then the cigarette being installed in box mark 12mg is evaluated, and evaluation result is in Table 1-2.
Embodiment 7
1. the preparation of spacetabs type aroma cigarette heart yearn
1) be dissolved in ethanolic solution by microcrystalline cellulose, obtain skeleton solution, in skeleton solution, the mass percent of microcrystalline cellulose is 30wt%; Maotai is dissolved in deionized water: ethanol: propane diols is in the wetting agent of 1:1:1, obtains mixing wine liquid; In mixing wine liquid, add skeleton solution, skeleton solution and the mass ratio mixing wine liquid are the ultrasonic mixing of 3:1,40kHz, obtain aroma liquid;
2) bamboo pulp short fiber is spun into single thread, and then 10 single thread are merged to add is twisted into strand, further again by 32 strands and close twisting, obtain heart yearn finally;
3) continuing to carry out ultrasonic mixing to the aroma liquid of step 1), and by step 2) the obtained heart yearn aroma liquid that is placed in ultrasonic mixing carries out ultrasonic dip-coating 60min;
4) by air-dry for the heart yearn normal temperature after ultrasonic for step 3) dip-coating, obtained spacetabs type aroma cigarette heart yearn.
2. the preparation of spacetabs type aroma cigarette heart yearn filter stick:
For implanting aforementioned spacetabs type aroma cigarette heart yearn in the industrialization forming step of cigarette filter rod, obtained aroma cigarette heart yearn mouth rod, shaping specification is that 100mm(4 cuts).Then the cigarette being installed in box mark 12mg is evaluated, and evaluation result is in Table 1-2.
Embodiment 8
1. the preparation of spacetabs type aroma cigarette heart yearn
1) be dissolved in ethanolic solution by hydroxypropyl methylcellulose, obtain skeleton solution, in skeleton solution, the mass percent of hydroxypropyl methylcellulose is 15wt%; Maotai is dissolved in deionized water: ethanol is in the wetting agent of 1:3, the mass ratio of Maotai and wetting agent is 1:8, obtains mixing wine liquid; In mixing wine liquid, add skeleton solution, skeleton solution and the mass ratio mixing wine liquid are the ultrasonic mixing of 2:1,20kHz, obtain aroma liquid;
2) bamboo charcoal staple fiber and bamboo pulp short fiber are spun into single thread, and then 20 single thread are merged to add are twisted into strand, further again by 20 strands and close twisting, obtain heart yearn finally;
3) continuing to carry out ultrasonic mixing to the aroma liquid of step 1), and by step 2) the obtained heart yearn aroma liquid that is placed in ultrasonic mixing carries out ultrasonic dip-coating 90min;
4) by air-dry for the heart yearn normal temperature after ultrasonic for step 3) dip-coating, obtained spacetabs type aroma cigarette heart yearn.
2. the preparation of spacetabs type aroma cigarette heart yearn filter stick:
For implanting aforementioned spacetabs type aroma cigarette heart yearn in the industrialization forming step of cigarette filter rod, obtained aroma cigarette heart yearn mouth rod, shaping specification is that 100mm(4 cuts).Then the cigarette being installed in box mark 12mg is evaluated, and evaluation result is in Table 1-2.
Embodiment 9
1. the preparation of spacetabs type aroma cigarette heart yearn
1) be dissolved in ethanolic solution by ethyl cellulose, obtain skeleton solution, in skeleton solution, the mass percent of ethyl cellulose is 10wt%; Maotai is dissolved in deionized water: ethanol: glycerine is in the wetting agent of 1:1:1, obtains mixing wine liquid; In mixing wine liquid, add skeleton solution, skeleton solution and the mass ratio mixing wine liquid are the ultrasonic mixing of 2.5:1,30kHz, obtain aroma liquid;
2) sky wire short fiber and short silk fiber are spun into single thread, and then 40 single thread are merged to add are twisted into strand, further again by 5 strands and close twisting, obtain heart yearn finally;
3) continuing to carry out ultrasonic mixing to the aroma liquid of step 1), and by step 2) the obtained heart yearn aroma liquid that is placed in ultrasonic mixing carries out ultrasonic dip-coating 30min;
4) by air-dry for the heart yearn normal temperature after ultrasonic for step 3) dip-coating, obtained spacetabs type aroma cigarette heart yearn.
2. the preparation of spacetabs type aroma cigarette heart yearn filter stick:
For implanting aforementioned spacetabs type aroma cigarette heart yearn in the industrialization forming step of cigarette filter rod, obtained aroma cigarette heart yearn mouth rod, shaping specification is that 100mm(4 cuts).Then the cigarette being installed in box mark 12mg is evaluated, and evaluation result is in Table 1-2.
Embodiment 10
Spacetabs type aroma cigarette heart yearn filter stick prepared by embodiment 1-9 is carried out to fume indication and inhales the detection of taste description, and the evaluation criterion of inhaling taste description is GB5006.4-2005, and experimental result is in Table 1-2.
Table 1 fume indication
Table 2 is inhaled taste and is described
Claims (10)
1. a preparation method for spacetabs type aroma cigarette heart yearn, step is as follows:
1) alcohol soluble high molecular material is dissolved in ethanol, obtains skeleton solution; Edible wine is dissolved in wetting agent, obtains mixing wine liquid; Skeleton solution is mixed with mixing wine liquid, obtains aroma liquid;
2) carbonate plant short fiber is twisted into heart yearn;
3) ultrasonic mixing being carried out, by step 2 while ultrasonic mixing to the aroma liquid of step 1)) obtained heart yearn is placed in described aroma liquid and carries out ultrasonic dip-coating;
4) by air-dry for the heart yearn normal temperature after ultrasonic for step 3) dip-coating, spacetabs type aroma cigarette heart yearn is obtained.
2. preparation method as claimed in claim 1, it is characterized in that, alcohol soluble high molecular material described in step 1) is one or more the combination in hydroxypropyl methylcellulose, cellulosic ether, microcrystalline cellulose, PVP; Described wetting agent is one or more the combination in deionized water, absolute ethyl alcohol, propane diols, glycerine.
3. preparation method as claimed in claim 1, it is characterized in that, in skeleton solution described in step 1), the content of alcohol soluble high molecular material is 10 ~ 50wt%; The weight ratio of described edible wine and wetting agent is 1:3 ~ 10.
4. preparation method as claimed in claim 1, it is characterized in that, skeleton solution described in step 1) is 2 ~ 10:1 with mixing wine liquid weight ratio.
5. preparation method as claimed in claim 1, is characterized in that, step 2) described short fiber of plant derives from one or more combination in sky silk, ramee, bamboo-carbon fibre, fibre and soya, bamboo pulp fiber and silk fiber.
6. preparation method as claimed in claim 5, is characterized in that, step 2) specification of described heart yearn is 10 4 strands ~ 40 32 strands.
7. preparation method as claimed in claim 1, it is characterized in that, ultrasonic hybrid frequency described in step 3) is 20 ~ 80KHz.
8. a spacetabs type aroma cigarette heart yearn, adopts method described in the arbitrary claim of claim 1-7 to prepare.
9. a spacetabs type aroma cigarette filter, is characterized in that, described spacetabs type aroma cigarette filter includes spacetabs type aroma cigarette heart yearn described in requirement 8 of having the right.
10. the preparation method of spacetabs type aroma cigarette filter described in claim 9, for implanting spacetabs type aroma cigarette heart yearn described in claim 8 in the industrialization forming step of cigarette filter rod, cuts, obtained spacetabs type aroma cigarette filter.
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| CN106868942A (en) * | 2017-03-06 | 2017-06-20 | 云南芯韵科技开发有限公司 | A kind of filter stick functionalization papery heart yearn and preparation method thereof |
| CN109875113A (en) * | 2019-04-17 | 2019-06-14 | 云南中烟工业有限责任公司 | A kind of graphene-based cigarette core wire and its preparation method and application |
| CN110574958A (en) * | 2019-10-12 | 2019-12-17 | 湖北中烟工业有限责任公司 | Process for improving spreading rate of reconstituted tobacco |
| CN111808767A (en) * | 2020-05-28 | 2020-10-23 | 重庆中烟工业有限责任公司 | Microbial preparation for improving tobacco leaf quality |
| CN115039914A (en) * | 2022-07-07 | 2022-09-13 | 天津工业大学 | Cooling belt-shaped fabric and preparation method and application thereof |
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| CN105533795A (en) * | 2016-01-15 | 2016-05-04 | 红云红河烟草(集团)有限责任公司 | Method for preparing honey-fragrant cigarette fragrance line through citrus nectar |
| CN105533794A (en) * | 2016-01-15 | 2016-05-04 | 红云红河烟草(集团)有限责任公司 | Method for preparing honey-fragrant cigarette fragrance line through longan nectar |
| CN105533796A (en) * | 2016-01-15 | 2016-05-04 | 红云红河烟草(集团)有限责任公司 | Method for preparing honey-fragrant cigarette fragrance line through rape nectar |
| CN105595415A (en) * | 2016-01-15 | 2016-05-25 | 红云红河烟草(集团)有限责任公司 | Method for preparing honey fragrance cigarette incense thread by means of litchi nectar |
| CN105595416A (en) * | 2016-01-15 | 2016-05-25 | 红云红河烟草(集团)有限责任公司 | Method for preparing honey fragrance cigarette incense thread by means of loquat nectar |
| CN105661628A (en) * | 2016-01-15 | 2016-06-15 | 红云红河烟草(集团)有限责任公司 | Method for preparing honey aroma cigarette fragrance lines through osmanthus honey |
| CN105686050A (en) * | 2016-01-15 | 2016-06-22 | 红云红河烟草(集团)有限责任公司 | Method using Chinese date honey to prepare honey aroma cigarette fragrant filament |
| CN106387994A (en) * | 2016-08-31 | 2017-02-15 | 刘迎春 | Cigarette filter stick containing controlled-release spice core wire |
| CN106868942A (en) * | 2017-03-06 | 2017-06-20 | 云南芯韵科技开发有限公司 | A kind of filter stick functionalization papery heart yearn and preparation method thereof |
| CN106868942B (en) * | 2017-03-06 | 2021-02-26 | 云南芯韵科技开发有限公司 | Functional paper core wire for filter stick and preparation method thereof |
| CN109875113A (en) * | 2019-04-17 | 2019-06-14 | 云南中烟工业有限责任公司 | A kind of graphene-based cigarette core wire and its preparation method and application |
| CN109875113B (en) * | 2019-04-17 | 2021-08-03 | 云南中烟工业有限责任公司 | Graphene-based cigarette core line and preparation method and application thereof |
| CN110574958A (en) * | 2019-10-12 | 2019-12-17 | 湖北中烟工业有限责任公司 | Process for improving spreading rate of reconstituted tobacco |
| CN111808767A (en) * | 2020-05-28 | 2020-10-23 | 重庆中烟工业有限责任公司 | Microbial preparation for improving tobacco leaf quality |
| CN111808767B (en) * | 2020-05-28 | 2023-02-28 | 重庆中烟工业有限责任公司 | Microbial preparation for improving tobacco leaf quality |
| CN115039914A (en) * | 2022-07-07 | 2022-09-13 | 天津工业大学 | Cooling belt-shaped fabric and preparation method and application thereof |
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