CN104418508A - Colored glaze colored drawing pigment and method for preparing same and high temperature curing process of same - Google Patents
Colored glaze colored drawing pigment and method for preparing same and high temperature curing process of same Download PDFInfo
- Publication number
- CN104418508A CN104418508A CN201310375547.5A CN201310375547A CN104418508A CN 104418508 A CN104418508 A CN 104418508A CN 201310375547 A CN201310375547 A CN 201310375547A CN 104418508 A CN104418508 A CN 104418508A
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- Prior art keywords
- coloured
- drawing pigment
- colored
- pigment
- glaze
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/006—Surface treatment of glass, not in the form of fibres or filaments, by coating with materials of composite character
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/20—Materials for coating a single layer on glass
- C03C2217/29—Mixtures
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- Chemical & Material Sciences (AREA)
- Composite Materials (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Glass Compositions (AREA)
- Dental Preparations (AREA)
Abstract
The invention discloses a colored glaze colored drawing pigment, a method for preparing the same, and a high temperature curing process of the same. The pigment comprises the following raw materials by weight: 30%-34% of quartz sand, 30%-28% of alkali powder, 7%-5% of sodium nitrate, 8%-4% of alumina, 10.5%-6.5% of borax, 10%-8% of fluorite, 10%-8% of calcium carbonate, and 0.5%-0.3% of a coloring agent. The method comprises the following steps: mixing the raw materials and water according to a weight ratio of 1:0.3, performing wet-method ball milling for 24 hours; sieving with a 400-mesh sieve after ball milling, drying; adding water into the dried colored glaze colored drawing pigment to adjust into a dressing degree, performing manual dressing decoration of a colored glaze device, and heating the device in a kiln to 650 DEG C. The colored glaze colored drawing pigment of the invention is characterized in that after a colored glaze subjected to colored drawing is cured at a high temperature, the colored drawing pigment is firm in attachment, and bright in color, and never fades, and the colored glaze product is as a perfect integral whole.
Description
Technical field
The present invention relates to pigment preparation and solidification field, specifically the high temperature curing process of a kind of coloured glaze coloured drawing pigment and this pigment method of preparation and this pigment.
Background technology
After the surface engraving of coloured glaze type, former is according to pattern needs, carries out illuminated with oil colour, increases engraving three-dimensional color effect.Because oil colour can not wiping, and the time grown and produced oxidation, cause and fade and come off, can not persistence, this is a large defect.For this defect, we adopt various hard fire colour to carry out illuminated after depiction completes, and apply after illuminated again and add layer of transparent coloured glaze pigment and protect, and increase coloured glaze texture, then carry out high-temperature firing.After high-temperature firing, make depiction combine together with the coloured glaze pigment coated, be in bright colors, solidify, be not afraid of wiping, will never fade.This invention overcomes the defect of original oil colour illuminated, remains engraving original appearance, increases decorative effect and coloured glaze texture, coloured glaze is carved more flawless.
Summary of the invention
The object of this invention is to provide one to be in bright colors, be not afraid of wiping, make coloured glaze and the organic coloured glaze coloured drawing pigment combined together of coloured pigment and prepare the high temperature curing process of this pigment method and this pigment.
The technical solution used in the present invention is, a kind of coloured glaze coloured drawing pigment, is made up of the raw material of following weight part:
Quartz sand 30%-34%, ground caustic 30%-28%, SODIUMNITRATE 7%-5%, aluminum oxide 8%-4%, borax 10.5%-6.5%, fluorite 10%-8%, calcium carbonate 10%-8%, tinting material 0.5%-0.3%;
Above-mentioned coloured glaze coloured drawing pigment, wherein, is made up of the raw material of following weight part: quartz sand 30%, ground caustic 28%, SODIUMNITRATE 7%, aluminum oxide 8%, borax 6.5%, fluorite 10%, calcium carbonate 10%, tinting material 0.5%;
Above-mentioned coloured glaze coloured drawing pigment, wherein, is made up of the raw material of following weight part: quartz sand 32%, ground caustic 30%, SODIUMNITRATE 6%, aluminum oxide 6%, borax 8.6%, fluorite 8%, calcium carbonate 9%, tinting material 0.4%;
The preparation method of above-mentioned coloured glaze coloured drawing pigment, wherein, is made up of the raw material of following weight part: quartz sand 34%, ground caustic 30%, SODIUMNITRATE 5%, aluminum oxide 4.2%, borax 10.5%, fluorite 8%, calcium carbonate 8%, tinting material 0.3%;
Above-mentioned coloured glaze coloured drawing pigment, wherein, described tinting material is cadmium red or cadmium yellow or cobalt oxide or cupric oxide or arsenic potassium or manganese oxide.
The preparation method of above-mentioned coloured glaze coloured drawing pigment, the raw material of weight part: water=1 of weight part: 0.3 mixing, wet ball grinding 24 hours; Cross 400 mesh sieves after ball milling, dry.
The high temperature curing process of above-mentioned coloured glaze coloured drawing pigment,
Step 1, coloured glaze coloured drawing pigment being added water is adjusted to can dressing degree,
Step 2, to the manual dressing decoration of coloured glaze type, then apply and add layer of transparent coloured glaze colorant
650 DEG C are warming up in step 3, placement kiln.
Beneficial effect of the present invention: coloured glaze coloured drawing pigment and preparation method and high-temperature firing technique skill are provided, make the coloured glaze type after colored drawing after hot setting, coloured drawing pigment adhere firmly, be in bright colors, will never fade, make whole coloured glaze works one integrated mass, perfection is to attaining.
Embodiment
Below in conjunction with embodiment, the present invention is described in further detail.
A kind of coloured glaze coloured drawing pigment of the present invention, is made up of the raw material of following weight part: quartz sand 30%-34%, ground caustic 30%-28%, SODIUMNITRATE 7%-5%, aluminum oxide 8%-4%, borax 10.5%-6.5%, fluorite 10%-8%, calcium carbonate 10%-8%, tinting material 0.5%-0.3%.
The preparation method of above-mentioned coloured glaze coloured drawing pigment, the raw material of weight part: water=1 of weight part: 0.3 mixing, wet ball grinding 24 hours; Cross 400 mesh sieves after ball milling, dry.
The high temperature curing process of above-mentioned coloured glaze coloured drawing pigment,
Step 1, coloured glaze coloured drawing pigment being added water is adjusted to can dressing degree,
Step 2, to the manual dressing decoration of coloured glaze type, then apply and add layer of transparent coloured glaze colorant
650 DEG C are warming up in step 3, placement kiln.
Embodiment one
The raw material of weight part: quartz sand 30%, ground caustic 28%, SODIUMNITRATE 7%, aluminum oxide 8%, borax 6.5%, fluorite 10%, calcium carbonate 10%, tinting material 0.5%;
Again by the raw material of weight part: water=1 of weight part: 0.3 mixing, wet ball grinding 24 hours; Cross 400 mesh sieves after ball milling, dry.
Then the coloured glaze coloured drawing pigment of oven dry being added that water is adjusted to can dressing degree, to the manual dressing decoration of coloured glaze type, can apply again and add layer of transparent coloured glaze colorant, be warming up to 650 DEG C in placement kiln.
Embodiment two,
The raw material of weight part: quartz sand 32%, ground caustic 30%, SODIUMNITRATE 6%, aluminum oxide 6%, borax 8.6%, fluorite 8%, calcium carbonate 9%, tinting material 0.4%;
Again by the raw material of weight part: the water=1:0.3 mixing of weight part, wet ball grinding 24 hours; Cross 400 mesh sieves after ball milling, dry.
Then the coloured glaze coloured drawing pigment of oven dry being added that water is adjusted to can dressing degree, to the manual dressing decoration of coloured glaze type, can apply again and add layer of transparent coloured glaze colorant, be warming up to 650 DEG C in placement kiln.
Embodiment three,
The raw material of weight part: quartz sand 34%, ground caustic 30%, SODIUMNITRATE 5%, aluminum oxide 4.2%, borax 10.5%, fluorite 8%, calcium carbonate 8%, tinting material 0.3%;
Again by the raw material of weight part: water=1 of weight part: 0.3 mixing, wet ball grinding 24 hours; Cross 400 mesh sieves after ball milling, dry.
Then the coloured glaze coloured drawing pigment of oven dry being added that water is adjusted to can dressing degree, to the manual dressing decoration of coloured glaze type, can apply again and add layer of transparent coloured glaze colorant, be warming up to 650 DEG C in placement kiln.
Certainly; the present invention also can have other various embodiments; when not deviating from the present invention's spirit and essence thereof; those of ordinary skill in the art are when making various corresponding change and distortion according to the present invention, but these change accordingly and are out of shape the protection domain that all should belong to the claim appended by the present invention.
Claims (7)
1. a coloured glaze coloured drawing pigment, is characterized in that, is made up of the raw material of following weight part: quartz sand 30%-34%, ground caustic 30%-28%, SODIUMNITRATE 7%-5%, aluminum oxide 8%-4%, borax 10.5%-6.5%, fluorite 10%-8%, calcium carbonate 10%-8%, tinting material 0.5%-0.3%.
2. coloured glaze coloured drawing pigment as claimed in claim 1, is characterized in that, be made up of the raw material of following weight part: quartz sand 30%, ground caustic 28%, SODIUMNITRATE 7%, aluminum oxide 8%, borax 6.5%, fluorite 10%, calcium carbonate 10%, tinting material 0.5%.
3. coloured glaze coloured drawing pigment as claimed in claim 1, is characterized in that, be made up of the raw material of following weight part: quartz sand 32%, ground caustic 30%, SODIUMNITRATE 6%, aluminum oxide 6%, borax 8.6%, fluorite 8%, calcium carbonate 9%, tinting material 0.4%.
4. coloured glaze coloured drawing pigment as claimed in claim 1, is characterized in that, be made up of the raw material of following weight part: quartz sand 34%, ground caustic 30%, SODIUMNITRATE 5%, aluminum oxide 4.2%, borax 10.5%, fluorite 8%, calcium carbonate 8%, tinting material 0.3%.
5. the coloured glaze coloured drawing pigment as described in as arbitrary in Claims 1-4, is characterized in that, described tinting material is cadmium red or cadmium yellow or cobalt oxide or cupric oxide or arsenic potassium or manganese oxide.
6. the preparation method of coloured glaze coloured drawing pigment as claimed in claim 1, is characterized in that, the raw material of weight part: water=1 of weight part: 0.3 mixing, and wet ball grinding 24 hours, crosses 400 mesh sieves after ball milling, dries.
7. the high temperature curing process of coloured glaze coloured drawing pigment as claimed in claim 1, is characterized in that,
Step 1, coloured glaze coloured drawing pigment being added water is adjusted to can dressing degree;
Step 2, to the manual dressing decoration of coloured glaze type;
650 DEG C are warming up in step 3, placement kiln.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310375547.5A CN104418508B (en) | 2013-08-27 | 2013-08-27 | Colored glaze colored drawing pigment and method for preparing same and high temperature curing process of same |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310375547.5A CN104418508B (en) | 2013-08-27 | 2013-08-27 | Colored glaze colored drawing pigment and method for preparing same and high temperature curing process of same |
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| Publication Number | Publication Date |
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| CN104418508A true CN104418508A (en) | 2015-03-18 |
| CN104418508B CN104418508B (en) | 2017-04-12 |
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| CN201310375547.5A Active CN104418508B (en) | 2013-08-27 | 2013-08-27 | Colored glaze colored drawing pigment and method for preparing same and high temperature curing process of same |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105504934A (en) * | 2016-01-30 | 2016-04-20 | 淄博市淄川振华玻璃制品有限公司 | Pigment for colored glaze with Chinese painting and application method of pigment |
| CN105778596A (en) * | 2016-01-30 | 2016-07-20 | 淄博市淄川振华玻璃制品有限公司 | Golden red pigment for colored glaze and application method thereof |
| CN108545957A (en) * | 2018-05-08 | 2018-09-18 | 孙云浩 | A kind of coloured glaze type and its method for cooking |
| CN108585951A (en) * | 2018-05-08 | 2018-09-28 | 孙云浩 | A kind of coloured glaze type and its method for cooking |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU1164218A1 (en) * | 1983-05-13 | 1985-06-30 | Днепропетровский химико-технологический институт им.Ф.Э.Дзержинского | Frit for colour enamel coating |
| CN1040570A (en) * | 1988-08-19 | 1990-03-21 | 北京市建筑材料科学研究所 | The preparation method of lead-free gluzed enamel |
| RO102388A2 (en) * | 1988-09-05 | 1991-12-02 | Intreprinderea De Vase Emailate, Focsani, Ro | Process for manufacturing a coloured enamel for steel plate, with direct application |
| CN102503134A (en) * | 2011-10-14 | 2012-06-20 | 关润明 | Application technology for colorful glass grains and powder colored glazes in glass crafts |
| CN103183527A (en) * | 2011-12-29 | 2013-07-03 | 湖南省明丰达陶瓷琉璃瓦业有限公司 | Blue gray glaze for glazed tiles and its firing method |
-
2013
- 2013-08-27 CN CN201310375547.5A patent/CN104418508B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU1164218A1 (en) * | 1983-05-13 | 1985-06-30 | Днепропетровский химико-технологический институт им.Ф.Э.Дзержинского | Frit for colour enamel coating |
| CN1040570A (en) * | 1988-08-19 | 1990-03-21 | 北京市建筑材料科学研究所 | The preparation method of lead-free gluzed enamel |
| RO102388A2 (en) * | 1988-09-05 | 1991-12-02 | Intreprinderea De Vase Emailate, Focsani, Ro | Process for manufacturing a coloured enamel for steel plate, with direct application |
| CN102503134A (en) * | 2011-10-14 | 2012-06-20 | 关润明 | Application technology for colorful glass grains and powder colored glazes in glass crafts |
| CN103183527A (en) * | 2011-12-29 | 2013-07-03 | 湖南省明丰达陶瓷琉璃瓦业有限公司 | Blue gray glaze for glazed tiles and its firing method |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105504934A (en) * | 2016-01-30 | 2016-04-20 | 淄博市淄川振华玻璃制品有限公司 | Pigment for colored glaze with Chinese painting and application method of pigment |
| CN105778596A (en) * | 2016-01-30 | 2016-07-20 | 淄博市淄川振华玻璃制品有限公司 | Golden red pigment for colored glaze and application method thereof |
| CN108545957A (en) * | 2018-05-08 | 2018-09-18 | 孙云浩 | A kind of coloured glaze type and its method for cooking |
| CN108585951A (en) * | 2018-05-08 | 2018-09-28 | 孙云浩 | A kind of coloured glaze type and its method for cooking |
Also Published As
| Publication number | Publication date |
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| CN104418508B (en) | 2017-04-12 |
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