CN1044112C - High-energy organic fertilizer - Google Patents
High-energy organic fertilizer Download PDFInfo
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- CN1044112C CN1044112C CN 96120685 CN96120685A CN1044112C CN 1044112 C CN1044112 C CN 1044112C CN 96120685 CN96120685 CN 96120685 CN 96120685 A CN96120685 A CN 96120685A CN 1044112 C CN1044112 C CN 1044112C
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- potassium hydroxide
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Abstract
The present invention discloses a method for producing a high-energy organic fertilizer. The method is mainly characterized in that the processing waste materials of agricultural products are expanded and then mixed with the trace element compound of nitro humic acid and an enhancer so as to obtain a high-energy organic fertilizer which has the obvious effect on increasing yield and improving soil.
Description
The present invention relates to the preparation method of high-energy organic fertilizer, relate in particular to the puffing of fertilizer and the preparation method of intensive treatment.Various fertilizers can both increase the organic matter in the soil, can fertilize the soil, improve the soil, change the physicochemical property of soil, but wherein nitrogen, phosphorus, potassium content are all low, do not satisfy the volume increase needs of crop, so the peasant also will remedy a large amount of chemical fertilizer, cause soil to covet lean hardening, polluted surface water destroys the eubiosis.High-energy organic fertilizer is that organism is handled through science, again through strengthening nitrogen, phosphorus, potassium processing, make it nitrogen, phosphorus, potassium total content to reach 〉=25%, the advantage of so promptly having brought into play fertilizer has also remedied the defective of fertilizer, can reach volume increase infertile field effect and can improve the physicochemical property of soil again, alleviate soil compaction and pollution because of causing to fertilize.
This fertilizer is as base fertilizer, and my another patent of invention (states such as Japan have been put and exported in batches to product on market) " humic acid type compound spray fertilizers " (ZL92103265X) is done to topdress and is used the evil that can thoroughly free " chemical fertilizer ".
Manure type is too many at present, and handle mostly comparatively simple the early stage of natural organic fertilizer, does not even just handle and directly uses, and the utilization ratio of fertilizer and turnover ratio all are subjected to certain influence like this.
In order to overcome above-mentioned defective and the advantage that makes full use of humic acids, the object of the present invention is to provide a kind of preparation method of high-energy organic fertilizer.Purpose of the present invention adopts following technical scheme to realize.A kind of preparation method of high-energy organic fertilizer is characterized in that this method comprises the steps:
1. the preparation of reinforcer
To slowly inject 70 parts of water in parts by weight potassium hydroxide 60-100 part, mix obtaining potassium hydroxide solution until dissolving;
To inject 70 parts of water lentamente in parts by weight strong phosphoric acid 70-120 part, mix obtaining phosphoric acid solution;
Then, above-mentioned potassium hydroxide solution is poured in the above-mentioned phosphoric acid solution lentamente, because neutralization reaction is emitted a large amount of heats, should stir while adding, after treating that whole potassium hydroxide solutions add, add 40-60 part urea while hot, continue to stir and all dissolve, obtain described reinforcer until urea.
2. one or more mixing in vinasse, soy sauce slag, beet pulp or cottonseed meal, the leached tea oil slag are air-dry, pulverizing, mix with wet chicken manure again, the water-content of its mixture should be controlled at 10-30% (weight), preferably be controlled at 10-20% (weight), more preferably be controlled at 12-18% (weight), the ratio of chicken manure is not critical in its mixture, but preferred chicken manure content is counted 20-40% (weight) with mixture weight; More preferably chicken manure content is 25-35% (weight).
3. said mixture is carried out puffing, after organism placed puffing apparatus, rising along with temperature and pressure, moisture is in superheat state in the organism, it is soft that particle itself becomes, when reaching certain temperature and pressure in the puffing apparatus, open the puffing apparatus lid, pressure will reduce rapidly, until reaching normal pressure, at this moment the moisture that is in superheat state in the organism is just issued blast in instant vaporization, inflatable hundreds of times of the volume of water, and even thousands of times, huge bulking pressure has not only destroyed organic formalness, and broken organism intrinsic molecular structure, insoluble long-chain organism is broken into the short chain organism of water-soluble, after organism is expanded, insoluble composition has reduced in the organism, water miscible composition has increased, and therefore, puffing has changed the physical condition of raw material, it is loose that material becomes, improve organic B surface greatly, be convenient to strengthen nitrogen like this, phosphorus, potassium, this puffing also influences organic chemical property.The expanded physical method of a kind of usefulness that Here it is replaces the enhanced processing method of biochemical methods such as fermentation, and this treatment process is more simple and efficient, economical and practical than chemical process or fermentation biochemical method.Described puffing is carried out under the following conditions:
Bulking machine can adopt dry method bulking machine, wet-process puffing machine or high-temperature high-pressure swelling machine.
Temperature 250-400 ℃, pressure 10-15kg/cm of the puffing of high-temperature high-pressure swelling machine
2, in the bulking machine filler than volume of material and bulking machine expansion chamber volume fraction below 0.4,30-50 minute puffing time;
Preferably, the temperature 250-350 of puffing ℃, pressure 10-12kg/cm
2, the bulking machine filler than 0.35,40-50 minute puffing time;
More preferably, the temperature 280-300 of puffing ℃, pressure 10kg/cm
2, the bulking machine filler than 0.3,40-45 minute puffing time.
Adopt dry method bulking machine or wet-process puffing machine to carry out puffing humidity and be controlled at 15-20 °.
4. the material of above-mentioned steps (3) puffing is pulverized, mix with nitro humic acid with zinc, copper, iron, manganese, magnesium sulfate hydrate and ammonium molybdate, borax or boric acid trace compound then, add the described reinforcer of step (1) preparation during remix;
The amount of wherein said trace compound is counted 1-5% (weight) with the finished product weight, and the anharmonic ratio of compounds such as zinc, copper, iron, magnesium, manganese, molybdenum, boron is: 2-4: 1-2: 2-6: 0.5-1: 0.5-1: 0.2-0.5: 2-6;
Described expanded organic weight is counted 60-74% (weight) with the finished product weight;
The amount of described nitro humic acid is counted 5-15% (weight) with the finished product weight, and humic acids content is 2-5% (weight) in the nitro humic acid;
Described nitrogen, phosphorus, potassium are measured by force, count 20-30% (weight) with the finished product weight.
The mixing said mixture obtains product of the present invention through granulation, oven dry.
Adopt the resulting product of the inventive method can meet and exceed Ministry of Agriculture's specified standards, promptly organonitrogen is greater than 2%, and nitrogen, phosphorus, potassium total amount are 25%, wherein full nitrogen 〉=13%, full phosphorus 〉=6%, full potassium 〉=6%, organic 〉=40%, and product is a black particle.High-energy organic fertilizer of the present invention has following positively effect:
1. method of the present invention be utilize the waste material of agricultural processing to be processed into to have nitrogen, fertilizer that phosphorus, potassium and micronutrient levels height, organic abundant quick-acting and normal effect combine, because science has been handled organic matter, make nitrogen, phosphorus, potassium be difficult for running off, the utilization ratio of nitrogen, phosphorus, potassium can be improved like this, quick-acting and normal effect of imitating can be played.
2. use fertilizer of the present invention, also can roll up the organic matter of soil, because expanded organic constructional feature of the present invention so fertilizer of the present invention helps soil fertilizer, water conservation, helps improving the structure of soil, thereby is beneficial to the benign cycle of soil.
3. with the chemical fertilizer of amount or fertilizer commonly used compare, obvious effect of increasing production, general food crop volume increase is more than 10%, and vegetables are increased production 20-30%, and fruit increases production more than 15%, and can improve and improve fruit quality.
Fertilizer of the present invention is squeezed into particulate state by tablets press; be fit to do base fertilizer and base manure; the mu consumption is 30-50kg; evenly spread in the ground prior to seeding and get final product; (ZL92103265X) do to topdress and be used with the applicant's patent of invention " humic acid type compound spray fertilizers ", effect of increasing production is more obvious.
The present invention is further illustrated below in conjunction with embodiment:
1. the preparation of reinforcer
Get 70kg potassium hydroxide solid and be added at leisure in the 70kg water, slowly stir, allow its potassium hydroxide solid all dissolve, obtain potassium hydroxide solution;
Get the 80kg strong phosphoric acid again and slowly pour in the 70kg water, mix obtaining phosphate aqueous solution;
Then, above-mentioned potassium hydroxide solution is poured in the above-mentioned phosphate aqueous solution continuous the stirring, because neutralization reaction can be emitted a large amount of heats, so potassium hydroxide solution should stir bit by bit slowly adding, liquid splash comes out when preventing to mix.In case all potassium hydroxide solutions add, just take advantage of solution still heat just add 50 kilogram weights of urea, continue to stir and all dissolve, so that standby until urea.
2. get air-dry, the pulverizing of vinasse, allow it not lump, mix with wet chicken manure, the water-content of its mixture reaches 15%, and the chicken manure amount accounts for 30% (weight) of amount of the mixture.
3. said mixture is placed dry method bulking machine or wet-process puffing machine, humidity be carry out under 10-25 ° expanded.Obtain expanded organism, pulverize the 20-40 order then.
4. expanded organism 700kg, the nitro humic acid 100kg (containing humic acids 5%), Zinc Sulphate Heptahydrate 2kg, cupric sulfate pentahydrate 1kg, green vitriol 4kg, three water manganous sulfate 0.5kg, magnesium sulfate heptahydrate 0.5kg, ammonium molybdate 0.2kg, the borax 4kg that get above-mentioned steps (3) mix, the reinforcer solution that slowly adds step (1) in mixing process obtains the 1000kg fertilizer product through extruder grain, oven dry again.Determine that through chemical analysis this product contains:
Nitrogen 〉=13%
Phosphorus 〉=6%
Potassium 〉=6%
Organic 〉=40%
This embodiment instruction is obtained product high-energy organic fertilizer ground Different Crop for it and soil has carried out pot experiment, its test-results such as table 1.Result by table 1 can be clearly seen that no matter at cold husky yellow mud, the result who obtains on purple mud or the little colour of loess mud is higher than the result who uses chemical fertilizer significantly.
The high-energy organic fertilizer that adopts present embodiment to prepare is used on vegetables and be the results are shown in table 2, can be seen that by table 2 it also is very significant using high-energy organic fertilizer effect of increasing production of the present invention.
The invention discloses a kind of preparation method of high-energy organic fertilizer.The principal character of its method is that the processing of farm products waste material mixes with nitro humic acid trace compound and reinforcer and obtains high-energy organic fertilizer after puffing.The unusual effect that this fertilizer has volume increase, improves the soil.
The effect of high-energy organic fertilizer on Different Crop and soil
| Soil is made product place amount reason | Cold husky yellow mud | Purple mud | Little colour of loess mud | |||
| Paddy rice | Wheat | Paddy rice | Wheat | Paddy rice | Wheat | |
| Gram/basin | Gram/basin | Gram/basin | ||||
| Contrast | 15.8 | 3.2 | 26.9 | 4.2 | 35.4 | 5.7 |
| Chemical fertilizer | 44.4 | 17.0 | 53.7 | 16.6 | 55.5 | 14.7 |
| High-energy organic fertilizer | 56.7 | 23.5 | 67.2 | 19.2 | 59.4 | 18.5 |
The effect of increasing production (jin/mu) of high-energy organic fertilizer on vegetables
| Work place physics | Capsicum | Chinese cabbage | Blue or green bamboo shoot | Pachyrhizus | ||||
| Output | Volume increase | Output | Volume increase | Output | Volume increase | Output | Volume increase | |
| 1. contrast | 1369.0 | / | 5525.0 | / | 5935.0 | / | 5460.0 | / |
| 2. chemical fertilizer | 1785.0 | 416.0 | 11315.0 | 5790.0 | / | / | / | / |
| 3. high-energy organic fertilizer | 1999.0 | 630.0 | 1407.5 | 5882.5 | 6469.0 | 534.0 | 5820.0 | 360.0 |
Claims (4)
1, a kind of preparation method of high-energy organic fertilizer is characterized in that this method is made up of following step:
(1) preparation of reinforcer
To be dissolved in 70 parts of water in parts by weight potassium hydroxide 60-100 part and obtain potassium hydroxide solution;
To inject 70 parts of water in parts by weight strong phosphoric acid 70-120 part and obtain phosphoric acid solution;
Described potassium hydroxide solution is slowly added in the described phosphoric acid solution, treat that whole potassium hydroxide solutions add after, add 40-60 part urea, obtain described reinforcer;
(2) one or more mixing in vinasse, soy sauce slag, beet pulp or cottonseed meal and the leached tea oil slag are air-dry, pulverizing mixes with wet chicken manure again, and the water-content of controlling its mixture is 10-30% (weight), and chicken manure content is 20-40% (weight);
(3) mixture that above-mentioned steps (2) is obtained is at temperature 250-400 ℃, pressure 10-15kg/cm
2Under the condition puffing 30-50 minute; Adopt dry method bulking machine, wet method sprayization machine or high-temperature high-pressure swelling machine;
(4) above-mentioned steps (3) material of puffing is pulverized, contained thing and ammonium molybdate, borax or boric acid trace compound with zinc, copper iron, manganese, sulfuric acid salt solution then, mix, add the reinforcer of step (1) preparation during mixing with nitro humic acid;
The amount of described trace compound is counted 1-5% (weight) with the finished product weight;
The amount of described nitro humic acid is counted 5-15% (weight) with the finished product weight;
Described expanded organic amount is counted 60-74% (weight) with the finished product weight;
Described nitrogen, phosphorus, potash fertilizer total amount are counted 20-30% (weight) with the finished product weight; Wherein full nitrogen 〉=13%, full phosphorus 〉=6%, full potassium 〉=6%, the mixing said mixture obtains described product through the granulation oven dry.
2, method according to claim 1 is characterized in that temperature 280-300 ℃, pressure 10kg/cm of puffing
2, 40-50 minute puffing time or employing dry method bulking machine, wet-process puffing machine carry out puffing.The humidity sky is built in 15-20 °.
3, method according to claim 1.It is characterized in that described chicken manure content counts 25-35% (weight) with mixture weight.
4. method according to claim 1, the weight ratio that it is characterized in that trace compound zinc, copper, iron, manganese, magnesium, molybdenum, boron compound is 2-4: 1-2: 2-6: 0.5-1: 0.5-1: 0.2-0.5: 2-6.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 96120685 CN1044112C (en) | 1996-11-20 | 1996-11-20 | High-energy organic fertilizer |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 96120685 CN1044112C (en) | 1996-11-20 | 1996-11-20 | High-energy organic fertilizer |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1157810A CN1157810A (en) | 1997-08-27 |
| CN1044112C true CN1044112C (en) | 1999-07-14 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 96120685 Expired - Fee Related CN1044112C (en) | 1996-11-20 | 1996-11-20 | High-energy organic fertilizer |
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| Country | Link |
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| CN (1) | CN1044112C (en) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1100484C (en) * | 1998-11-06 | 2003-02-05 | 王恒源 | Environment protective plant protecting agent and preparation thereof |
| CN1297521C (en) * | 2005-10-28 | 2007-01-31 | 天津理工大学 | Biodegradable swelling slow releasing fertilizer and its manufacturing method |
| CN1865195B (en) * | 2006-05-31 | 2010-07-21 | 刘凡 | Method for preparing fertilizer dedicated to alkaline land |
| CN100460365C (en) * | 2007-12-03 | 2009-02-11 | 贵州圣济堂制药有限公司 | Nano biological organic and inorganic composite fertilizer |
| CN101993317B (en) * | 2009-08-12 | 2014-09-17 | 深圳市芭田生态工程股份有限公司 | Manufacturing method of puffed particle compound fertilizer and product thereof |
| CN101691317B (en) * | 2009-09-25 | 2012-07-25 | 广东新大地生物科技股份有限公司 | Efficient snail-killing type organic fertilizer produced from tea seed cakes and preparation method thereof |
| CN101774845B (en) * | 2009-12-17 | 2013-08-14 | 赵东科 | High-efficient microbial organic fertilizer and production technology thereof |
| CN102180716B (en) * | 2011-03-11 | 2014-04-16 | 赵鲁 | Method for producing organic compound fertilizer by fermenting animal manure |
| CN102924149A (en) * | 2012-10-24 | 2013-02-13 | 曹丽莉 | Organic and inorganic matter compound fertilizer prepared from wine waste and preparation method thereof |
| CN102992915B (en) * | 2012-11-30 | 2014-07-09 | 张有聪 | Method for preparing environment-friendly and high-efficiency biological organic fertilizer by using distilled spirit vinasse |
| CN103146796B (en) * | 2013-02-04 | 2015-07-22 | 重庆百奥帝克微生态科技有限公司 | Preparing method of humic acid based on vinasse and application thereof |
| CN103553774A (en) * | 2013-10-24 | 2014-02-05 | 安徽环绿生态农业投资发展有限公司 | Special fertilizer for honey locust |
| CN106748208A (en) * | 2016-12-29 | 2017-05-31 | 常熟市添源环保科技有限公司 | A kind of preparation method of vinasse composite highly effective biological organic fertilizer |
-
1996
- 1996-11-20 CN CN 96120685 patent/CN1044112C/en not_active Expired - Fee Related
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| Publication number | Publication date |
|---|---|
| CN1157810A (en) | 1997-08-27 |
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Granted publication date: 19990714 |