CN104403140A - Rubber material for agriculture vehicle tire - Google Patents
Rubber material for agriculture vehicle tire Download PDFInfo
- Publication number
- CN104403140A CN104403140A CN201410724032.6A CN201410724032A CN104403140A CN 104403140 A CN104403140 A CN 104403140A CN 201410724032 A CN201410724032 A CN 201410724032A CN 104403140 A CN104403140 A CN 104403140A
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- rubber
- natural rubber
- oxide
- rubber material
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Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L7/00—Compositions of natural rubber
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B60—VEHICLES IN GENERAL
- B60C—VEHICLE TYRES; TYRE INFLATION; TYRE CHANGING; CONNECTING VALVES TO INFLATABLE ELASTIC BODIES IN GENERAL; DEVICES OR ARRANGEMENTS RELATED TO TYRES
- B60C1/00—Tyres characterised by the chemical composition or the physical arrangement or mixture of the composition
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention discloses a rubber material for agriculture vehicle tires. The rubber material is prepared from the following raw materials in parts by weight: 40-50 parts of natural rubber, 10-14 parts of epoxy natural rubber, 15-20 parts of silicon dioxide, 2-4 parts of a silane coupling agent, 20-30 parts of brominated butyl rubber, 20-30 parts of superfine glass bead, 30-40 parts of carbon black N660, 20-30 parts of light calcium carbonate, 1-2 parts of tetramethyl thiuram disulfide, 1-2 parts of diisopropylbenzene peroxide, 2-3 parts of N-cyclohexyl-2-benzothiazole sulfonamide, 2-4 parts of zinc oxide, 1-2 parts of an accelerant DM, 0.5-1.0 part of an accelerant CZ, 1-2 parts of N-phenyl-N'-(1,3-dimethyl)-p-phenylenediamine, 1-2 parts of 2,2'-methylene-bi(4-methyl-6-tertiary butyl phenol), 1-2 parts of petroleum oil, 2-5 parts of stearic acid, 1-2 parts of protecting wax OK5194, 5-6 parts of rubber tackifying resin A-90, 5-8 parts of antimonous oxide, 5-10 parts of molybdenum trioxide and 20-30 parts of aluminium hydroxide.
Description
Technical field
The present invention relates to rubber for tire technical field, particularly relate to a kind of agricultural locomotive tyre rubber material.
Background technology
Agricultural locomotive travel speed increases substantially in recent years, overloading is general, tire more and more can not adapt at a high speed, the condition of overload, under some hot conditions, along with the prolongation of duration of service, rub between tire and ground, the use temperature of tire is constantly raised, surface of tyre is destroyed even loses original performance, and raise along with the temperature of tire used environment, ageing of rubber, easily discharge poisonous and corrosive gas, high temperature resistant to tire of current user, namely environmental protection and long-time steady operation propose requirements at the higher level, how to prepare a kind of resistance to elevated temperatures good, environmental protection, wear-resisting, and there is the agricultural locomotive Tire rubber material better drawing high intensity and tear strength become the current technical issues that need to address.
Summary of the invention
In order to solve the technical problem existed in background technology, the present invention proposes a kind of agricultural locomotive tyre rubber material, environmental protection, wear-resisting, high temperature resistant, and have and excellent draw high intensity and tear strength.
A kind of agricultural locomotive tyre rubber material that the present invention proposes, its raw material comprises by weight: natural rubber 40-50 part, epoxy natural rubber 10-14 part, silica 1 5-20 part, silane coupling agent 2-4 part containing sulfydryl, brominated butyl rubber 20-30 part, ultra tiny cenosphere 20-30 part, carbon black N660 30-40 part, light calcium carbonate 20-30 part, tetramethyl-thiuram disulfide 1-2 part, dicumyl peroxide 1-2 part, N cyclohexyl 2 benzothiazole sulfenamide 2-3 part, zinc oxide 2-4 part, altax 1-2 part, accelerant CZ 0.5-1.0 part, N-phenyl-N '-(1, 3-dimethyl)-Ursol D 1-2 part, 2, 2 '-methylene radical-bis-(4-methyl-6-tert-butylphenol) 1-2 part, petroleum-type oil 1-2 part, stearic acid 2-5 part, protection wax OK 5194 1-2 part, rubber tackifying resin A-90 5-6 part, antimonous oxide 5-8 part, molybdic oxide 5-10 part, aluminium hydroxide 20-30 part.
Preferably, in above-mentioned agricultural locomotive tyre rubber material, the weight ratio of natural rubber, brominated butyl rubber, epoxy natural rubber is 42-48:24-26:12-14.
Preferably, in above-mentioned agricultural locomotive tyre rubber material, the weight ratio of epoxy natural rubber, silicon-dioxide and the silane coupling agent containing sulfydryl is 12-14:16-18:3-4.
Preferably, in above-mentioned agricultural locomotive tyre rubber material, the weight ratio of tetramethyl-thiuram disulfide, dicumyl peroxide and N cyclohexyl 2 benzothiazole sulfenamide is 1-1.5:1-1.5:2.5-3.
Preferably, in above-mentioned agricultural locomotive tyre rubber material, the weight ratio of light calcium carbonate, antimonous oxide and aluminium hydroxide is 24-26:6-8:24-26.
Preferably, above-mentioned agricultural locomotive tyre rubber material, its raw material comprises by weight: natural rubber 42-48 part, epoxy natural rubber 12-14 part, silica 1 6-18 part, silane coupling agent 3-4 part containing sulfydryl, brominated butyl rubber 24-26 part, ultra tiny cenosphere 22-25 part, carbon black N660 34-36 part, light calcium carbonate 24-26 part, tetramethyl-thiuram disulfide 1-1.5 part, dicumyl peroxide 1-1.5 part, N cyclohexyl 2 benzothiazole sulfenamide 2.5-3 part, zinc oxide 3-4 part, altax 1-2 part, accelerant CZ 0.5-1.0 part, N-phenyl-N '-(1, 3-dimethyl)-Ursol D 1-2 part, 2, 2 '-methylene radical-bis-(4-methyl-6-tert-butylphenol) 1-2 part, petroleum-type oil 1-2 part, stearic acid 3-4 part, protection wax OK 5194 1-2 part, rubber tackifying resin A-90 5-6 part, antimonous oxide 6-8 part, molybdic oxide 6-8 part, aluminium hydroxide 24-26 part.
Preferably, above-mentioned agricultural locomotive tyre rubber material, its raw material comprises by weight: natural rubber 43 parts, epoxy natural rubber 13 parts, silica 17 parts, silane coupling agent containing sulfydryl 3.4 parts, brominated butyl rubber 25 parts, ultra tiny cenosphere 24 parts, carbon black N660 35 parts, light calcium carbonate 25 parts, tetramethyl-thiuram disulfide 1.2 parts, dicumyl peroxide 1.2 parts, N cyclohexyl 2 benzothiazole sulfenamide 2.8 parts, 3.4 parts, zinc oxide, altax 1.5 parts, accelerant CZ 0.8 part, N-phenyl-N '-(1, 3-dimethyl)-Ursol D 1.5 parts, 2, 2 '-methylene radical-bis-(4-methyl-6-tert-butylphenol) 1.7 parts, petroleum-type oil 1 part, stearic acid 3.4 parts, protection wax OK 5,194 1.2 parts, rubber tackifying resin A-90 5.6 parts, antimonous oxide 7 parts, molybdic oxide 7 parts, 25 parts, aluminium hydroxide.
In the present invention, the use of natural rubber improves tensile strength and the tear strength of tire, improve weight-carrying ability, the air-tightness of brominated butyl rubber is better, adopt natural rubber and brominated butyl rubber, epoxy natural rubber is major ingredient, the tire wear of preparation is good, wet earth-catching property, dry adherence properties and splitting resistance, warp resistance crack growth performance is excellent, and promote tensile strength and tear strength further, add silane coupling agent containing sulfydryl as coupling agent and ultra tiny cenosphere, silicon-dioxide, light calcium carbonate, carbon black N660, antimonous oxide, molybdic oxide, aluminium hydroxide effect, silicon-dioxide excellent dispersion, material dispersion is good, comprehensive action can not only promote tyre air tightness further, wear resisting property, tensile strength and tear strength, and the flame-retardant smoke inhibition system of antimonous oxide and molybdic oxide, not only be easy to rubber compounding, and properties of rubber can be improved preferably, light calcium carbonate can improve sizing material extrusion performance, reduce the burst size of hydrogenchloride, environmental friendliness, coordinate wherein and add appropriate aluminium hydroxide, it is cheap, not only can reduce costs, and tire can be applicable to the occasion comparatively harsh to high temperature requirement, tire hot is stablized, flame retardant effect is excellent, and halogen-free environmental, add petroleum-type oil, stearic acid, both weather resistances are good, stability is excellent, its harmful substance contents is minimum, the low temperature tolerance characteristics of further raising tire and resistance to burnup performance, in above-mentioned material, use tetramethyl-thiuram disulfide, dicumyl peroxide, N cyclohexyl 2 benzothiazole sulfenamide is as natural rubber, the vulcanizing agent of epoxy natural rubber and brominated butyl rubber, the generation of nitrosamine can be made to minimize, there is good environment protecting, and do not affect sulfuration facilitation effect, coordinate and add altax, accelerant CZ carries out helping vulcanization reaction, curing time is short and abundant, and goods rubber has good wear-resisting, solvent resistant and corrosion resistance nature, add N-phenyl-N '-(1, 3-dimethyl)-Ursol D, 2, 2 '-methylene radical-bis-(4-methyl-6-tert-butylphenol) with the use of, synergy significantly, antioxidant effect is good, stability is high, and low toxicity, can further improve the heat-resisting of tire, light aging resisting property.
Embodiment
Embodiment 1
A kind of agricultural locomotive tyre rubber material, its raw material comprises by weight: natural rubber 40 parts, epoxy natural rubber 14 parts, silica 15 parts, silane coupling agent containing sulfydryl 4 parts, brominated butyl rubber 20 parts, ultra tiny cenosphere 30 parts, carbon black N660 30 parts, light calcium carbonate 30 parts, tetramethyl-thiuram disulfide 1 part, dicumyl peroxide 2 parts, N cyclohexyl 2 benzothiazole sulfenamide 2 parts, 4 parts, zinc oxide, altax 1 part, accelerant CZ 1.0 parts, N-phenyl-N '-(1, 3-dimethyl)-Ursol D 1 part, 2, 2 '-methylene radical-bis-(4-methyl-6-tert-butylphenol) 2 parts, petroleum-type oil 1 part, stearic acid 5 parts, protection wax OK 5,194 1 parts, rubber tackifying resin A-90 6 parts, antimonous oxide 5 parts, molybdic oxide 10 parts, 20 parts, aluminium hydroxide.
Embodiment 2
A kind of agricultural locomotive tyre rubber material, its raw material comprises by weight: natural rubber 50 parts, epoxy natural rubber 10 parts, silicon-dioxide 20 parts, silane coupling agent containing sulfydryl 2 parts, brominated butyl rubber 30 parts, ultra tiny cenosphere 20 parts, carbon black N660 40 parts, light calcium carbonate 20 parts, tetramethyl-thiuram disulfide 2 parts, dicumyl peroxide 1 part, N cyclohexyl 2 benzothiazole sulfenamide 3 parts, 2 parts, zinc oxide, altax 2 parts, accelerant CZ 0.5 part, N-phenyl-N '-(1, 3-dimethyl)-Ursol D 2 parts, 2, 2 '-methylene radical-bis-(4-methyl-6-tert-butylphenol) 1 part, petroleum-type oil 2 parts, stearic acid 2 parts, protection wax OK 5,194 2 parts, rubber tackifying resin A-90 5 parts, antimonous oxide 8 parts, molybdic oxide 5 parts, 30 parts, aluminium hydroxide.
Embodiment 3
A kind of agricultural locomotive tyre rubber material, its raw material comprises by weight: natural rubber 42 parts, epoxy natural rubber 14 parts, silica 16 parts, silane coupling agent containing sulfydryl 4 parts, brominated butyl rubber 24 parts, ultra tiny cenosphere 25 parts, carbon black N660 34 parts, light calcium carbonate 26 parts, tetramethyl-thiuram disulfide 1 part, dicumyl peroxide 1.5 parts, N cyclohexyl 2 benzothiazole sulfenamide 2.5 parts, 4 parts, zinc oxide, altax 1 part, accelerant CZ 1.0 parts, N-phenyl-N '-(1, 3-dimethyl)-Ursol D 1 part, 2, 2 '-methylene radical-bis-(4-methyl-6-tert-butylphenol) 2 parts, petroleum-type oil 1 part, stearic acid 4 parts, protection wax OK 5,194 1 parts, rubber tackifying resin A-90 6 parts, antimonous oxide 6 parts, molybdic oxide 8 parts, 24 parts, aluminium hydroxide.
Embodiment 4
A kind of agricultural locomotive tyre rubber material, its raw material comprises by weight: natural rubber 48 parts, epoxy natural rubber 12 parts, silica 18 parts, silane coupling agent containing sulfydryl 3 parts, brominated butyl rubber 26 parts, ultra tiny cenosphere 22 parts, carbon black N660 36 parts, light calcium carbonate 24 parts, tetramethyl-thiuram disulfide 1.5 parts, dicumyl peroxide 1 part, N cyclohexyl 2 benzothiazole sulfenamide 3 parts, 3 parts, zinc oxide, altax 2 parts, accelerant CZ 0.5 part, N-phenyl-N '-(1, 3-dimethyl)-Ursol D 2 parts, 2, 2 '-methylene radical-bis-(4-methyl-6-tert-butylphenol) 1 part, petroleum-type oil 2 parts, stearic acid 3 parts, protection wax OK 5,194 2 parts, rubber tackifying resin A-90 5 parts, antimonous oxide 8 parts, molybdic oxide 6 parts, 26 parts, aluminium hydroxide.
Embodiment 5
A kind of agricultural locomotive tyre rubber material, its raw material comprises by weight: natural rubber 43 parts, epoxy natural rubber 13 parts, silica 17 parts, silane coupling agent containing sulfydryl 3.4 parts, brominated butyl rubber 25 parts, ultra tiny cenosphere 24 parts, carbon black N660 35 parts, light calcium carbonate 25 parts, tetramethyl-thiuram disulfide 1.2 parts, dicumyl peroxide 1.2 parts, N cyclohexyl 2 benzothiazole sulfenamide 2.8 parts, 3.4 parts, zinc oxide, altax 1.5 parts, accelerant CZ 0.8 part, N-phenyl-N '-(1, 3-dimethyl)-Ursol D 1.5 parts, 2, 2 '-methylene radical-bis-(4-methyl-6-tert-butylphenol) 1.7 parts, petroleum-type oil 1 part, stearic acid 3.4 parts, protection wax OK 5,194 1.2 parts, rubber tackifying resin A-90 5.6 parts, antimonous oxide 7 parts, molybdic oxide 7 parts, 25 parts, aluminium hydroxide.
The above; be only the present invention's preferably embodiment; but protection scope of the present invention is not limited thereto; anyly be familiar with those skilled in the art in the technical scope that the present invention discloses; be equal to according to technical scheme of the present invention and inventive concept thereof and replace or change, all should be encompassed within protection scope of the present invention.
Claims (7)
1. an agricultural locomotive tyre rubber material, it is characterized in that, its raw material comprises by weight: natural rubber 40-50 part, epoxy natural rubber 10-14 part, silica 1 5-20 part, silane coupling agent 2-4 part containing sulfydryl, brominated butyl rubber 20-30 part, ultra tiny cenosphere 20-30 part, carbon black N660 30-40 part, light calcium carbonate 20-30 part, tetramethyl-thiuram disulfide 1-2 part, dicumyl peroxide 1-2 part, N cyclohexyl 2 benzothiazole sulfenamide 2-3 part, zinc oxide 2-4 part, altax 1-2 part, accelerant CZ 0.5-1.0 part, N-phenyl-N '-(1, 3-dimethyl)-Ursol D 1-2 part, 2, 2 '-methylene radical-bis-(4-methyl-6-tert-butylphenol) 1-2 part, petroleum-type oil 1-2 part, stearic acid 2-5 part, protection wax OK 5194 1-2 part, rubber tackifying resin A-90 5-6 part, antimonous oxide 5-8 part, molybdic oxide 5-10 part, aluminium hydroxide 20-30 part.
2. agricultural locomotive tyre rubber material according to claim 1, is characterized in that, the weight ratio of natural rubber, brominated butyl rubber, epoxy natural rubber is 42-48:24-26:12-14.
3. agricultural locomotive tyre rubber material according to claim 1, is characterized in that, the weight ratio of epoxy natural rubber, silicon-dioxide and the silane coupling agent containing sulfydryl is 12-14:16-18:3-4.
4. agricultural locomotive tyre rubber material according to claim 1, is characterized in that, the weight ratio of tetramethyl-thiuram disulfide, dicumyl peroxide and N cyclohexyl 2 benzothiazole sulfenamide is 1-1.5:1-1.5:2.5-3.
5. agricultural locomotive tyre rubber material according to claim 1, is characterized in that, the weight ratio of light calcium carbonate, antimonous oxide and aluminium hydroxide is 24-26:6-8:24-26.
6. agricultural locomotive tyre rubber material according to claim 1, it is characterized in that, it is characterized in that, its raw material comprises by weight: natural rubber 42-48 part, epoxy natural rubber 12-14 part, silica 1 6-18 part, silane coupling agent 3-4 part containing sulfydryl, brominated butyl rubber 24-26 part, ultra tiny cenosphere 22-25 part, carbon black N660 34-36 part, light calcium carbonate 24-26 part, tetramethyl-thiuram disulfide 1-1.5 part, dicumyl peroxide 1-1.5 part, N cyclohexyl 2 benzothiazole sulfenamide 2.5-3 part, zinc oxide 3-4 part, altax 1-2 part, accelerant CZ 0.5-1.0 part, N-phenyl-N '-(1, 3-dimethyl)-Ursol D 1-2 part, 2, 2 '-methylene radical-bis-(4-methyl-6-tert-butylphenol) 1-2 part, petroleum-type oil 1-2 part, stearic acid 3-4 part, protection wax OK 5194 1-2 part, rubber tackifying resin A-90 5-6 part, antimonous oxide 6-8 part, molybdic oxide 6-8 part, aluminium hydroxide 24-26 part.
7. agricultural locomotive tyre rubber material according to claim 6, it is characterized in that, its raw material comprises by weight: natural rubber 43 parts, epoxy natural rubber 13 parts, silica 17 parts, silane coupling agent containing sulfydryl 3.4 parts, brominated butyl rubber 25 parts, ultra tiny cenosphere 24 parts, carbon black N660 35 parts, light calcium carbonate 25 parts, tetramethyl-thiuram disulfide 1.2 parts, dicumyl peroxide 1.2 parts, N cyclohexyl 2 benzothiazole sulfenamide 2.8 parts, 3.4 parts, zinc oxide, altax 1.5 parts, accelerant CZ 0.8 part, N-phenyl-N '-(1, 3-dimethyl)-Ursol D 1.5 parts, 2, 2 '-methylene radical-bis-(4-methyl-6-tert-butylphenol) 1.7 parts, petroleum-type oil 1 part, stearic acid 3.4 parts, protection wax OK 5,194 1.2 parts, rubber tackifying resin A-90 5.6 parts, antimonous oxide 7 parts, molybdic oxide 7 parts, 25 parts, aluminium hydroxide.
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CN201410724032.6A CN104403140A (en) | 2014-12-04 | 2014-12-04 | Rubber material for agriculture vehicle tire |
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CN201410724032.6A CN104403140A (en) | 2014-12-04 | 2014-12-04 | Rubber material for agriculture vehicle tire |
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Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104987608A (en) * | 2015-06-29 | 2015-10-21 | 安徽育安实验室装备有限公司 | Heat-proof chemical-resistant pad for laboratory table board |
CN105440380A (en) * | 2015-12-16 | 2016-03-30 | 宁国市开源橡塑汽车零部件有限公司 | High strength wear resistant rubber material |
CN105837872A (en) * | 2016-06-07 | 2016-08-10 | 沈阳化工大学 | Flame-retardant modified natural rubber material and preparation method thereof |
JP2017075275A (en) * | 2015-10-16 | 2017-04-20 | 横浜ゴム株式会社 | Tire rubber composition |
CN108102235A (en) * | 2017-12-20 | 2018-06-01 | 青岛科技大学 | The crawler belt rubber material and preparation method used under a kind of particular surroundings |
CN109370074A (en) * | 2018-10-29 | 2019-02-22 | 扬中市华亿电器有限公司 | A kind of cable protective sleeve preparation formula |
CN111073067A (en) * | 2020-01-20 | 2020-04-28 | 中国化工集团曙光橡胶工业研究设计院有限公司 | Antistatic and wear-resistant aircraft tire tread rubber material and preparation method thereof |
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JP5044381B2 (en) * | 2007-12-07 | 2012-10-10 | 住友ゴム工業株式会社 | Rubber composition for inner liner and tire having inner liner using the same |
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Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104987608A (en) * | 2015-06-29 | 2015-10-21 | 安徽育安实验室装备有限公司 | Heat-proof chemical-resistant pad for laboratory table board |
JP2017075275A (en) * | 2015-10-16 | 2017-04-20 | 横浜ゴム株式会社 | Tire rubber composition |
CN105440380A (en) * | 2015-12-16 | 2016-03-30 | 宁国市开源橡塑汽车零部件有限公司 | High strength wear resistant rubber material |
CN105837872A (en) * | 2016-06-07 | 2016-08-10 | 沈阳化工大学 | Flame-retardant modified natural rubber material and preparation method thereof |
CN108102235A (en) * | 2017-12-20 | 2018-06-01 | 青岛科技大学 | The crawler belt rubber material and preparation method used under a kind of particular surroundings |
CN108102235B (en) * | 2017-12-20 | 2020-03-10 | 青岛科技大学 | Rubber material for crawler belt used in special environment and preparation method thereof |
CN109370074A (en) * | 2018-10-29 | 2019-02-22 | 扬中市华亿电器有限公司 | A kind of cable protective sleeve preparation formula |
CN111073067A (en) * | 2020-01-20 | 2020-04-28 | 中国化工集团曙光橡胶工业研究设计院有限公司 | Antistatic and wear-resistant aircraft tire tread rubber material and preparation method thereof |
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