Summary of the invention
For the deficiencies in the prior art, a kind of fire prevention is the object of the present invention is to provide to inhale ripple plate.
Making step of the present invention comprises:
(1) cornstalk is purified
(2) pulverize and sieve cornstalk powder
Cornstalk powder footpath is 30 ~ 40 orders.
(3) carbonization cornstalk powder
Loaded by cornstalk powder in HIGH PRESSURE TREATMENT tank, subsequently to people's high-pressure saturated steam logical in tank, pressure is risen to 0.25MPa, heat-insulation pressure keeping 4 hours, last release, carries out drift ice taking-up after release.
(4) dry cornstalk powder
Be placed in the defibrator drying that temperature has been preheated to 100 DEG C.
(5) fire retardant and cementing agent Lauxite is added, and defibrator process cornstalk powder
Fire-retardant FRW technique adopts as follows: dicyandiamide, phosphoric acid, triethanolamine and water, by heating for dissolving after 5: 3: 2: 10 mass ratio mixing, 3 ~ 4 hours are incubated under 85 ~ 95 DEG C of conditions, after being cooled to 60 ~ 70 DEG C, add boric acid, borax, ammoniacal liquor that mass ratio is 6: 4: 3, boric acid quality is 6% of dicyandiamide quality, and it is for subsequent use that rear discharging is dissolved in insulation.Fire retardant and cementing agent Lauxite mass ratio are 3: 10, and fire retardant is 8% of cornstalk opaque amount.
Fire retardant and cementing agent Lauxite are added in defibrator mill room, together with cornstalk powder after mill mechanism, in mixing infiltration cornstalk fibers.Saturated vapour pressure 0.8 ~ 0.9MPa, mill chamber pressure is 0.7 ~ 0.8MPa, and digestion time is 3 ~ 5min, and the sound Disc grinding plate side clearance of mill is 0.2mm, and the degree of balance is 0.04mm.
(6) carborundum and titanate coupling agent is added
Carborundum is 12% of cornstalk opaque amount, and titanate coupling agent is 1.2% of cornstalk opaque amount.Carborundum particle diameter is 60 ~ 80 orders.
Carborundum and titanate coupling agent are stirred 5min at homogenizer mix, and then adds in ball mill, mix with cornstalk powder, and utilize sonic oscillation instrument to make carborundum dispersed in cornstalk matrix.
Because carborundum very easily electrostatic occurs, especially under the effect of fricting shearing, caking of therefore easily uniting, not easily disperses.In homogenizer, can electrostatic be prevented by titanate coupling agent carbon coated SiClx, carborundum is uniformly dispersed.In addition, titanate coupling agent carries out activation process to the surface of carborundum, improves the compatibility of carborundum and cornstalk powder.
Rational carborundum particle diameter can fill up the space between cornstalk fibers, and be conducive to the binding ability improving plate, the intensity of reinforcement plate and density, and meticulous carborundum particle diameter will cause plate intensity to reduce, carborundum particle diameter is determined according to test.
(7) ripple plate is inhaled in fire prevention of mating formation
(8) ripple plate is inhaled in pressurization fire prevention
Pressure is 3MPa, and temperature is 170 DEG C, and pressing time is 12min.
(9) shaping
Carry out cutting fire prevention according to product requirement and inhale ripple plate.
The present invention has good flame resistance, wave-sucking performance is strong, wearability is high feature.
Detailed description of the invention
The present embodiment making step comprises:
(1) cornstalk is purified
(2) pulverize and sieve cornstalk powder
Cornstalk powder footpath is 30 ~ 40 orders.
(3) carbonization cornstalk powder
Loaded by cornstalk powder in HIGH PRESSURE TREATMENT tank, subsequently to people's high-pressure saturated steam logical in tank, pressure is risen to 0.25MPa, heat-insulation pressure keeping 4 hours, last release, carries out drift ice taking-up after release.
(4) dry cornstalk powder
Be placed in the defibrator drying that temperature has been preheated to 100 DEG C.
(5) fire retardant and cementing agent Lauxite is added, and defibrator process cornstalk powder
Fire-retardant FRW technique adopts as follows: dicyandiamide, phosphoric acid, triethanolamine and water, by heating for dissolving after 5: 3: 2: 10 mass ratio mixing, 3 ~ 4h is incubated under 85 ~ 95 DEG C of conditions, after being cooled to 60 ~ 70 DEG C, add boric acid, borax, ammoniacal liquor that mass ratio is 6: 4: 3, boric acid quality is 6% of dicyandiamide quality, and it is for subsequent use that rear discharging is dissolved in insulation.Fire retardant and cementing agent Lauxite mass ratio are 3: 10, and fire retardant is 8% of cornstalk opaque amount.
Fire retardant and cementing agent Lauxite are added in defibrator mill room, together with cornstalk powder after mill mechanism, in mixing infiltration cornstalk fibers.Saturated vapour pressure 0.8 ~ 0.9MPa, mill chamber pressure is 0.7 ~ 0.8MPa, and digestion time is 3 ~ 5min, and the sound Disc grinding plate side clearance of mill is 0.2mm, and the degree of balance is 0.04mm.
(6) carborundum and titanate coupling agent is added
Carborundum is 12% of cornstalk opaque amount, and titanate coupling agent is 1.2% of cornstalk opaque amount.Carborundum particle diameter is 60 ~ 80 orders.
Carborundum and titanate coupling agent are stirred 5min at homogenizer mix, and then adds in ball mill, mix with cornstalk powder, and utilize sonic oscillation instrument to make carborundum dispersed in cornstalk matrix.
(7) ripple plate is inhaled in fire prevention of mating formation
(8) ripple plate is inhaled in pressurization fire prevention
Pressure is 3MPa, and temperature is 170 DEG C, and pressing time is 12min.
(9) shaping
Carry out cutting fire prevention according to product requirement and inhale ripple plate.