Summary of the invention
For the deficiencies in the prior art, the object of the present invention is to provide a kind of fire prevention to inhale ripple plate.
Making step of the present invention comprises:
(1) purify cornstalk
(2) pulverize and sieve cornstalk powder
Cornstalk powder footpath is 30~40 orders.
(3) carbonization cornstalk powder
Cornstalk powder is packed in HIGH PRESSURE TREATMENT tank, with passing into high-pressure saturated steam in backward tank, pressure is risen to0.25MPa, heat-insulation pressure keeping 4 hours, last release, carries out drift ice taking-up after release.
(4) dry cornstalk powder
Cornstalk powder is placed in to temperature, and to be preheated to the defibrator of 100 DEG C dry.
(5) add fire retardant and cementing agent Lauxite, and defibrator process cornstalk powder
Fire retardant synthesis technique adopts as follows: dicyandiamide, phosphoric acid, triethanolamine and water, and by 5: 3: 2: 10 qualityRatio is mixed rear heating for dissolving, under 85~95 DEG C of conditions, is incubated 3~4 hours, be cooled to after 60~70 DEG C,Boric acid, borax, ammoniacal liquor that interpolation mass ratio is 6: 4: 3, boric acid quality is 6% of dicyandiamide quality, protectsIt is for subsequent use that temperature is dissolved rear discharging. Fire retardant and cementing agent Lauxite mass ratio are 3: 10, and fire retardant is corn8% of stalk opaque amount.
Fire retardant and cementing agent Lauxite are added in defibrator mill chamber, together with cornstalk powder through mill machineryAfter effect, mix in infiltration cornstalk fiber. Saturated vapour pressure 0.8~0.9MPa, mill chamber pressure is 0.7~0.8MPa, digestion time is 3~5min, the sound Disc grinding plate side clearance of mill is 0.2mm, the degree of balanceFor 0.04mm.
(6) add carborundum and titanate coupling agent
Carborundum is 12% of cornstalk opaque amount, and titanate coupling agent is 1.2% of cornstalk opaque amount. CarbonizationSilicon particle diameter is 60~80 orders.
By carborundum and titanate coupling agent, mix in homogenizer stirs 5min, and then adds ball millingIn machine, mix with cornstalk powder, and utilize sonic oscillation instrument that carborundum is evenly divided in cornstalk matrixLoose.
Because static very easily occurs carborundum, especially under the effect of fricting shearing, the caking of therefore easily uniting, noEasily disperse. In homogenizer, can prevent static by titanate coupling agent carbon coated SiClx, make carborundumBe uniformly dispersed. In addition, titanate coupling agent carries out activation processing to the surface of carborundum, improved carborundum andThe compatibility of cornstalk powder.
Reasonably carborundum particle diameter can be filled up the space between cornstalk fiber, is conducive to improve the associativity of plateCan, the intensity of reinforcement plate and density, and meticulous carborundum particle diameter will cause plate strength decreased, carborundum particle diameter isDetermine according to test.
(7) ripple plate is inhaled in the fire prevention of mating formation
(8) ripple plate is inhaled in pressurization fire prevention
Pressure is 3MPa, and temperature is 170 DEG C, and be 12min pressing time.
(9) moulding
Cut fire prevention according to product requirement and inhale ripple plate.
The present invention has good flame resistance, wave-sucking performance is strong, wearability is high feature.
Detailed description of the invention
The present embodiment making step comprises:
(1) purify cornstalk
(2) pulverize and sieve cornstalk powder
Cornstalk powder footpath is 30~40 orders.
(3) carbonization cornstalk powder
Cornstalk powder is packed in HIGH PRESSURE TREATMENT tank, with passing into high-pressure saturated steam in backward tank, pressure is risen to0.25MPa, heat-insulation pressure keeping 4 hours, last release, carries out drift ice taking-up after release.
(4) dry cornstalk powder
Cornstalk powder is placed in to temperature, and to be preheated to the defibrator of 100 DEG C dry.
(5) add fire retardant and cementing agent Lauxite, and defibrator process cornstalk powder
Fire retardant synthesis technique adopts as follows: dicyandiamide, phosphoric acid, triethanolamine and water, and by 5: 3: 2: 10 mass ratiosHeating for dissolving after mixing is incubated 3~4h under 85~95 DEG C of conditions, is cooled to after 60~70 DEG C, adds matterAmount ratio is boric acid, borax, the ammoniacal liquor of 6: 4: 3, and boric acid quality is 6% of dicyandiamide quality, and insulation is dissolvedRear discharging is for subsequent use. Fire retardant and cementing agent Lauxite mass ratio are 3: 10, and fire retardant is cornstalk opaque8% of amount.
Fire retardant and cementing agent Lauxite are added in defibrator mill chamber, together with cornstalk powder through mill machineryAfter effect, mix in infiltration cornstalk fiber. Saturated vapour pressure 0.8~0.9MPa, mill chamber pressure is 0.7~0.8MPa, digestion time is 3~5min, the sound Disc grinding plate side clearance of mill is 0.2mm, the degree of balanceFor 0.04mm.
(6) add carborundum and titanate coupling agent
Carborundum is 12% of cornstalk opaque amount, and titanate coupling agent is 1.2% of cornstalk opaque amount. CarbonizationSilicon particle diameter is 60~80 orders.
By carborundum and titanate coupling agent, mix in homogenizer stirs 5min, and then adds ball millingIn machine, mix with cornstalk powder, and utilize sonic oscillation instrument that carborundum is evenly divided in cornstalk matrixLoose.
(7) ripple plate is inhaled in the fire prevention of mating formation
(8) ripple plate is inhaled in pressurization fire prevention
Pressure is 3MPa, and temperature is 170 DEG C, and be 12min pressing time.
(9) moulding
Cut fire prevention according to product requirement and inhale ripple plate.