CN104365673B - Vegetable seedling damping-off control agent and application method thereof - Google Patents

Vegetable seedling damping-off control agent and application method thereof Download PDF

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CN104365673B
CN104365673B CN201410712770.9A CN201410712770A CN104365673B CN 104365673 B CN104365673 B CN 104365673B CN 201410712770 A CN201410712770 A CN 201410712770A CN 104365673 B CN104365673 B CN 104365673B
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dimethylamine
diimine
phenyl
albefaction
seedling
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CN104365673A (en
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郭兆武
谭碧林
邵亚楠
李红飞
张宏喜
胡勇屏
荣霞
李嘉欣
孙楠
汤仁杰
李珂
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Changsha University of Science and Technology
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Abstract

The invention discloses a vegetable seedling damping-off control agent and an application method thereof. The control agent is a mixture obtained by compatibility of calcium quicklime powder, whitened grass and tree ashes and a [4-(dimethylamine)phenyl]-diimine sulphonate assistant in a ratio of (5000.0-6000.0) : (8000.0-9000.0) : (1.0-1.5), preferably, in a ratio of 5500.0 : 8500.0 : 1.2; the [4-(dimethylamine) phenyl]-diimine sulphonate assistant is calculated according to 100% purity mass, the calcium quicklime powder and the whitened grass and tree ashes are calculated according to water-free dry ash mass, and the three are subjected to compatibility according to the ratio to have a remarkable synergistic effect to control effect. In a vegetable seedling stage, when and before damping-off symptoms appear, 40-60kg of the control agent is evenly sprayed onto each 667m<2> of seedbeds when dew forms on vegetable seedling leaves in early morning. The control agent is convenient to use in terms of production, simple to operate, low in cost and remarkable in control effect.

Description

A kind of vegetable seedling damping off control agent and its using method
Technical field
The invention belongs to agricultural practicality new technique research and development and application;The present invention relates to a kind of vegetable seedling damping off control agent Research and development and production application method.
Background technology
Vegetable seedling damping off, is commonly called as " Seedling ", " mould ", " bound feet pestilence ", belongs to fungal disease, by Mastigomycotina melon Fruit pythium (Pythium), Phytophthora (Phytophthora), silk core belong to the Seedling that fungal attack such as (Rhizoctonia) causes Phase plant disease, is the disease of early spring vegetable in seedling period most serious, can affect growth of seedling, cause to be short of seedling or even ruin when serious Kind.
Vegetable seedling damping off pathogenic bacteria host range is very wide, including vegetables such as leaf vegetabless, melon, solanaceous vegetables, beans, root vegetableses The seedbed disease of dish seedling, can cause dead seedling in blocks when serious.Southern area winter-spring season air and soil moisture are all very big, especially It is that in hot house, humidity many places, in hypersaturated state, are particularly suitable for the generation of damping off, some this diseases of vegetable grower Chang Yin and damage Lose heavy, thus, govern the development of southern area booth vegetable.
It is in water stain shape deliquescing that vegetable seedling damping off infects the basal part of stem that Symptoms are seedling, wilts rapidly therewith, Basal part of stem is hung in wire contracting afterwards;Sometimes cotyledon not yet shows symptom and lodges, and therefore named dampings off.Most common with 3-5 leaf seedling.By The seedling diseases that rhizoctonia causes is commonly referred to as damping-off, and aggrieved seedling basal part of stem produces brown scab, gradually make young stem atrophy until Seedling is withered, is infected cotyledon and also can produce the difform scab of brown, seedling is mostly susceptible from basal part of stem(Also have from stem Patient is felt in portion), just for water stain shape, and extension, contracting of overflowing attenuate such as " line " sample quickly, sick portion invariant color or be in yellowish-brown, and patient's condition is sent out Exhibition is rapid, i.e. from basal part of stem before cotyledon is still green, wilts(Or in the middle part of stem)Lodge and be affixed on bed surface.During the high humidity of seedbed, One fleece shape white mould can be given birth on invalid body and surrounding bed soil.Catch an illness before emerging, cause cotyledon, young root and young stem browning to rot, that is, For rotten kind or rotten bud.Disease starts often only indivedual seedling morbidities, when condition is suitable for centered on these diseased plants, rapidly to surrounding Extension spreads, and forms one piece one piece of lesion.There is relatively universal, pythium spp in the damping-off of Solanaceae, crop in cruciferae and cotton Seedling It is all soil inhabitant with Rhizoctonia solani Kuhn, is a class weak parasite, host range is wider.Damping off pathogenic bacteria is with mycelium or bacterium Core saprophytic or survival in invalid tissue in soil, as the primary infection source of Infection cycie.Pythium spp and phytophthora also may be used Survived the winter in residuum or in soil by oospore or akinete and tide over bad environmental condition.Pathogenic bacteria mainly pass through pour water or Soil cultivation is propagated.The growth suitable temperature range of pathogen is larger.When seedling bearing status are bad, resistance is poor, with regard to susceptible disease.Sudden Fall disease sometimes even the moon cruelly fine, suddenly throw off covering when unexpected large area occur.Damping off is often to send out, extensively in various vegetables seedling stage Send out, one of multiple most serious disease, all there is generation all parts of the country, and the loss causing is very big.
At present, although the domestic research to the preventing and treating of vegetable seedling damping off is many with report, its effective means is subject to many Limitation, effect is also not satisfactory.Traditional prophylactico-therapeutic measuress are mainly by good soil cultivation;Avoid soil's being over wet;Strengthen seedling stage pipe Reason;Strengthen seedling resistance;Broadcast front soil disinfection;Chemical pesticide is sprayed after emerging;Rationally heavy seeding;Timely and appropriate discovery topdresses, waters; Avoid using old bed soil nursery simultaneously, note seedbed cleaning and carry out soil disinfection;Just can only spray various once morbidity Chemical pesticide, but its effect is very poor, and it is observed that sometimes even not seeing effect, disease continues to quickly spread.
The above cultivation step is not only time-consuming to take a lot of work, and its effect is often not satisfactory;Apply after particularly falling ill Pure chemistry pesticide and antibacterial, often cannot stop disease continue spread.The pre- of this vegetable seedling damping off control agent controls effect Fruit is all extremely notable, and premorbid uses, and can prevent to fall ill;Apply after morbidity, can comparatively fast stop disease from spreading, seedling recovers normally to give birth to Long fast.This vegetable seedling damping off control agent is the achievement through research for many years and production application, and it both can be prevented, can control again, and make With convenient, simple to operate, low cost, prevention effect is notable, this be other about medicament or measure cannoted than.
Need it is emphasized that the calcareous quick lime powder of this vegetable seedling damping off control agent can not use calcareous ripe stone instead Grey powder or magnesium lime or containing the lime particle that overdoes, albefaction vegetation ashes can not use instead it has often been said that plant ash(Black), Otherwise, its effect will be had a greatly reduced quality, the pure chemistry pesticide that might as well commonly use now and antibacterial.
Content of the invention
The purpose of the present invention aims to provide a kind of vegetable seedling damping off control agent, easy to use, simple to operate, cost Low, prevention effect is notable.Another object of the present invention aims to provide the preferably use of above-mentioned vegetable seedling damping off control agent Method.The purpose of the present invention is achieved in the following ways:
The control agent of the present invention is calcareous quick lime powder, albefaction vegetation ashes and auxiliary agent [4-(dimethylamine) phenyl]-two Imines sulfonate sodium ([4- (dimethylamino) phenyl]-diazenesulfonic acid, sodium salt) group Become (hereinafter referred to as [4-(dimethylamine) phenyl]-diimine sodium sulfonate), wherein calcareous quick lime powder:Albefaction vegetation ashes Dry ash mass ratio is 5.0~6.0:8.0~9.0, calcareous quick lime powder, albefaction vegetation ashes press anhydrous dry ash Mass Calculation.
[4-(dimethylamine) phenyl]-diimine sodium sulfonate in control agent is mainly used as auxiliary agent, rises and promotes its prevention effect Effect, can be added according to production application.Inventor's research finds to add auxiliary agent [4-(dimethylamine) phenyl]-two sub- Amine sodium sulfonate and calcareous quick lime powder:The mass ratio 1.0~1.5 of albefaction vegetation ashes:5000.0~6000.0: 8000.0 ~9000.0 is preferred ratio, and [4-(dimethylamine) phenyl]-diimine sodium sulfonate is pressed 100% purity Coriolis mass and calculated, calcareous life Lime powder, albefaction vegetation ashes press anhydrous dry ash Mass Calculation.
The most preferred mass ratio of above three is 1.2:5500.0:8500.0, [4-(dimethylamine) phenyl]-diimine Sodium sulfonate is pressed 100% purity Coriolis mass and is calculated, and calcareous quick lime powder, albefaction vegetation ashes press anhydrous dry ash Mass Calculation.
Control agent presses every 667m240~60kg uniformly spreads fertilizer over the fields in seedbed, and wherein auxiliary agent [4-(dimethylamine) phenyl]-two is sub- Amine sodium sulfonate and calcareous quick lime powder:100% purity dry ash mass ratio of albefaction vegetation ashes is 1.0~1.5:5000.0~ 6000.0:8000.0~9000.0, [4-(dimethylamine) phenyl]-diimine sodium sulfonate is pressed 100% purity Coriolis mass and is calculated, calcareous Quick lime powder, albefaction vegetation ashes press anhydrous dry ash Mass Calculation.I.e. the excellent and again economic amount of application of prevention effect is every 667m250kg.
The present invention selects the calcareous quick lime powder of control agent, albefaction vegetation ashes and auxiliary agent [4-(dimethylamine) phenyl]-two Imines sodium sulfonate, employs the compatibility of suitable concentration, is configured to commercial control agent, and it both can be prevented, can control, it is to vegetable seedling again Damping off has significant preventive and therapeutic effect.Applying this vegetable seedling damping off control agent is it compared with one of effective measures.This is anti- Control agent easy to use, simple to operate, low cost, prevention effect is notable, this be other about medicament or measure cannoted than.
Vegetable seedling damping off preventing and treating agent prescription is calcareous quick lime powder, albefaction vegetation ashes and [4-(dimethylamine) benzene Base]-diimine sodium sulfonate press above-mentioned mass ratio ratio mix, plastic bag sealing pack, cool place be dried at lucifuge preserve, guarantee the quality 1 year phase.Dry ash mass ratio is pressed when calcareous quick lime powder, albefaction vegetation ashes proportioning.[4-(dimethylamine) phenyl]-two The pure percentage composition of imines sodium sulfonate does not have particular/special requirement, and its impurity, on the premise of not affecting its stability, reaches during compatibility Net content required by formula.The following is the comparative test of its regulating effect.
The vegetable seedling damping off control agent of the present invention has no the report of like product at present, the present invention be inventor for many years The result of the test that research work and practical work are drawn, and be verified in the production of long period, effect is preferable.And The formula of the present invention also has that technology content is higher, and dosage form is more stable, abundant raw material source, easy and simple to handle, such as develops into commodity, Low price.Easy to use aborning, prevention effect is notable, and use cost is low, is that a kind of good vegetable seedling is sudden Sick control agent.Vegetable seedling damping off preventing and treating agent prescription can carry out factorial praluction, and its exploitation not only will commercially Increase a kind of novel vegetable seedling damping off control agent, also the problem not good for current vegetable seedling damping off prevention effect is carried Approach for a solution.
The using method of the present invention is:In the vegetable seedling phase, occur dampinging off disease symptoms when or before, anti- mixed Control agent by every 667m240~60kg uniformly spreads fertilizer over the fields in seedbed.Control agent hermetic bag will disposably be finished after opening bag.Auxiliary agent [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.0~1.5: 5000.0~6000.0:8000.0~9000.0, [4-(dimethylamine) phenyl]-diimine sodium sulfonate is based on 100% purity Coriolis mass Calculate, calcareous quick lime powder, albefaction vegetation ashes press anhydrous dry ash Mass Calculation.Select there is dew on vegetable seedling blade in the morning Spread fertilizer over the fields during water, to strengthen prevention effect.After administration, 3d can not sprinkle water or apply fertilizer, routine rich water quality management and pest and disease damage after 3d Preventing and treating, if outdoor seedbed, selects fine day or the cloudy day that will not rain within nearly 3d, if rained within 3d after applying, Then need after rain again to process.
The following is inventor and realize the purpose of the present invention, constantly pass through test and select and from the vegetable being suitable for the present invention The comparative test of the prevention effect that the proportioning of raw material and its correlation that dish seedling damping off prevents and treats agent prescription is done.
Single dose is tested
Single dose test is mainly the single effect examination that each single dose of qualitative determination is prevented and treated to vegetable seedling damping off Test.
Materials and methods
1.1.1 test material
Test vegetable species are Amaranthus mangostanus L., the seedling of Fructus Cucumidis sativi, Caulis et Folium Ipomoeae aquaticae and four kinds of vegetables of Fructus Cucurbitae moschatae.Test ingredients is:Calcareous life Lime powder, albefaction vegetation ashes and [4-(dimethylamine) phenyl]-diimine sodium sulfonate.
Test method
Test is carried out in Yiyang proving ground.From former years regular incidence humidity be in hypersaturated state early spring plastics big Carry out in canopy.Preventing and treating as described herein refers to stop disease from continuing to spread, rather than the treatment to strain of falling ill, because falling ill Even if being also there is no use value after strain treatment is good.Carry out when damping off in Amaranthus mangostanus L., Fructus Cucumidis sativi, Caulis et Folium Ipomoeae aquaticae and Fructus Cucurbitae moschatae seedling Prevention effect is tested;Comparison is located at same seedbed.Test effect is mainly with, after the morbidity of same vegetable seedling, being subtracted with normal strain Few percentage ratio is counting and statistical analysiss(Do not include after diseased plant is treated, leaving the shoot of symptom vestige), in combination with Seedling Bed is observed.
Amaranthus mangostanus L., Fructus Cucumidis sativi, Caulis et Folium Ipomoeae aquaticae and four kinds of vegetables of Fructus Cucurbitae moschatae, in Seedling Stage, during damping off outburst, select vegetable seedling in the morning Processed when dew is had on blade.Each single dose amount of application:Calcareous quick lime powder presses every 667m240kg、50kg、 Tri- kinds of amounts of application of 60kg, by anhydrous dry ash Mass Calculation;Albefaction vegetation ashes press every 667m2Tri- kinds of 40kg, 50kg, 60kg applies Consumption, by anhydrous dry ash Mass Calculation;[4-(dimethylamine) phenyl]-diimine sodium sulfonate presses every 667m23.0g、4.0g、 Tri- kinds of amounts of application of 5.0g, are calculated by 100% purity Coriolis mass.After administration, 3d does not sprinkle water or applies fertilizer, and is observed and count during 3d. Routine rich water quality management and the prevention and control of plant diseases, pest control after 3d.
40 process of test setting(Including comparison), each processes 3 repetitions, and each repeats 0.10m2, random distribution.The During 0d, normal strain is carried out counting 1 time, during 3d, normal strain is carried out counting 1 time again, the strain number percentage ratio being reduced with normal strain As the effect processing, do not counted with diseased plant and be because after diseased plant 1~2d just disappearing in native bed it is difficult to count.Normal strain refers to The seedling of any disease symptoms of dampinging off does not occur.In the vegetable seedling phase, occur dampinging off disease symptoms when, control agent single dose press following place Reason is uniformly spread fertilizer over the fields in seedbed.
Process 1:The calcareous quick lime powder of Amaranthus mangostanus L. seedling damping off presses every 667m240kg applies;Process 2:Amaranthus mangostanus L. children The calcareous quick lime powder of Seedling damping off presses every 667m250kg applies;Process 3:The calcareous calculogenesis of Amaranthus mangostanus L. seedling damping off Grey powder presses every 667m260kg applies;Process 4:Amaranthus mangostanus L. seedling damping off albefaction vegetation ashes press every 667m240kg applies With;Process 5:Amaranthus mangostanus L. seedling damping off albefaction vegetation ashes press every 667m250kg applies;Process 6:Amaranthus mangostanus L. seedling is dampinged off Sick albefaction vegetation ashes press every 667m260kg applies;Process 7:Amaranthus mangostanus L. seedling damping off [4-(dimethylamine) benzene Base]-diimine sodium sulfonate press every 667m23.0g applying;Process 8:Amaranthus mangostanus L. seedling damping off [4-(dimethylamine) phenyl]- Diimine sodium sulfonate presses every 667m24.0g applying;Process 9:Amaranthus mangostanus L. seedling damping off [4-(dimethylamine) phenyl]-two is sub- Amine sodium sulfonate presses every 667m25.0g applying;CK1:Amaranthus mangostanus L. seedling damping off compares, and does not apply ingredients.Process 10:Cucumber seedling The calcareous quick lime powder of damping off presses every 667m240kg applies;Process 11:The calcareous calculogenesis of cucumber seedling damping off Grey powder presses every 667m250kg applies;Process 12:The calcareous quick lime powder of cucumber seedling damping off presses every 667m260kg Apply;Process 13:Cucumber seedling damping off albefaction vegetation ashes press every 667m240kg applies;Process 14:Cucumber seedling Damping off albefaction vegetation ashes press every 667m250kg applies;Process 15:Cucumber seedling damping off albefaction plant ash Cinder presses every 667m260kg applies;Process 16:Cucumber seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate By every 667m23.0g applying;Process 17:Cucumber seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate is pressed Every 667m24.0g applying;Process 18:Cucumber seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate is pressed every 667m25.0g applying;CK2:Cucumber seedling damping off compares, and does not apply ingredients.Process 19:Caulis et Folium Ipomoeae aquaticae seedling damping off calcium Matter quick lime powder presses every 667m240kg applies;Process 20:The calcareous quick lime powder of Caulis et Folium Ipomoeae aquaticae seedling damping off is pressed every 667m250kg applies;Process 21:The calcareous quick lime powder of Caulis et Folium Ipomoeae aquaticae seedling damping off presses every 667m260kg applies;Process 22:Caulis et Folium Ipomoeae aquaticae seedling damping off albefaction vegetation ashes press every 667m240kg applies;Process 23:Caulis et Folium Ipomoeae aquaticae seedling damping off Albefaction vegetation ashes press every 667m250kg applies;Process 24:Caulis et Folium Ipomoeae aquaticae seedling damping off albefaction vegetation ashes press every 667m2 60kg applies;Process 25:Caulis et Folium Ipomoeae aquaticae seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate presses every 667m2 3.0g applying;Process 26:Caulis et Folium Ipomoeae aquaticae seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate presses every 667m2 4.0g applying;Process 27:Caulis et Folium Ipomoeae aquaticae seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate presses every 667m2 5.0g applying;CK3:Caulis et Folium Ipomoeae aquaticae seedling damping off compares, and does not apply ingredients.Process 28:The calcareous calculogenesis of Fructus Cucurbitae moschatae seedling damping off Grey powder presses every 667m240kg applies;Process 29:The calcareous quick lime powder of Fructus Cucurbitae moschatae seedling damping off presses every 667m250kg Apply;Process 30:The calcareous quick lime powder of Fructus Cucurbitae moschatae seedling damping off presses every 667m260kg applies;Process 31:Fructus Cucurbitae moschatae children Seedling damping off albefaction vegetation ashes press every 667m240kg applies;Process 32:Fructus Cucurbitae moschatae seedling damping off albefaction vegetation Ashes press every 667m250kg applies;Process 33:Fructus Cucurbitae moschatae seedling damping off albefaction vegetation ashes press every 667m260kg applies With;Process 34:Fructus Cucurbitae moschatae seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate presses every 667m23.0g applying; Process 35:Fructus Cucurbitae moschatae seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate presses every 667m24.0g applying;Place Reason 36:Fructus Cucurbitae moschatae seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate presses every 667m25.0g applying;CK4: Fructus Cucurbitae moschatae seedling damping off compares, and does not apply ingredients.
Statistical analysiss
SAS is adopted to test data(6.12)Carry out statistical analysiss.The effect that after processing 3d, each is processed is shown in Table 1.Test Result shows(Table 1), process 1-6,8 effect is significant is better than CK1, the effect processing 2-3 is significantly better than process 1 again, processes 5-6 Effect be significantly better than process 4 again.I.e. the prevention effect of calcareous calcium lime powder foot couple Amaranthus mangostanus L. seedling damping off presses every 667m250- 60kg applies ratio by every 667m2The prevention effect that 40kg applies will be got well;The preventing and treating to Amaranthus mangostanus L. seedling damping off for the albefaction vegetation ashes Effect presses every 667m250-60kg applies ratio by every 667m2The prevention effect that 40kg applies will be got well;Auxiliary agent [4-(dimethylamine) benzene Base]-diimine sodium sulfonate press every 667m2The prevention effect that 4.0g applies is preferable.
Process 10-16,17 effect is significant is better than CK2, the effect processing 11-12 is significantly better than process 10 again, processes 14- 15 effect is significantly better than process 14 again.I.e. the prevention effect of calcareous calcium lime powder foot couple cucumber seedling damping off presses every 667m2 50-60kg applies ratio by every 667m2The prevention effect that 40kg applies will be got well;Albefaction vegetation ashes are to cucumber seedling damping off Prevention effect presses every 667m250-60kg applies ratio by every 667m2The prevention effect that 40kg applies will be got well;Auxiliary agent [4-(diformazan Amine) phenyl]-diimine sodium sulfonate press every 667m24.0g applies has certain prevention effect to cucumber seedling damping off.
The strain number of normal strain during table 1. single dose test process 3d reduces percentage ratio(Unit:%)
Process 15d Process 15d Process 15d Process 15d
Process 1 25.03±1.24c Process 10 21.37±1.27c Process 19 35.93±2.18c Process 28 20.27±1.08b
Process 2 22.09±0.83c Process 11 19.56±0.35d Process 20 32.68±0.91cd Process 29 19.50±0.91b
Process 3 21.76±2.07c Process 12 20.34±2.03cd Process 21 31.80±1.30d Process 30 21.87±0.67b
Process 4 16.87±1.19d Process 13 14.30±1.60e Process 22 25.72±2.15e Process 31 16.43±1.37c
Process 5 14.31±0.57e Process 14 12.84±1.31f Process 23 23.81±0.97ef Process 32 15.39±2.15cd
Process 6 13.72±0.31e Process 15 13.15±0.81ef Process 24 23.17±1.61f Process 33 12.80±0.62d
Process 7 34.29±1.34a Process 16 32.39±2.38ab Process 25 42.61±0.91b Process 34 24.17±1.27a
Process 8 32.46±0.61b Process 17 31.50±1.07b Process 26 39.40±1.28b Process 35 23.64±0.38a
Process 9 33.83±1.42ab Process 18 32.16±0.69ab Process 27 41.15±2.19b Process 36 24.20±0.90a
CK1 35.18±1.97a CK2 33.85±0.38a CK3 46.27±1.07a CK4 24.17±1.08a
Note:Lower case is 0.05 level, same row difference letter representation significant difference, similarly hereinafter.
The effect is significant processing 19-27 is better than CK3, and the effect processing 21 is significantly better than process 19-20 again, processes 24 effect Fruit is significantly better than process 22-23 again.I.e. the prevention effect of calcareous calcium lime powder foot couple Caulis et Folium Ipomoeae aquaticae seedling damping off presses every 667m2 60kg applies ratio by every 667m2The prevention effect that 40-50kg applies will be got well;Albefaction vegetation ashes are to Caulis et Folium Ipomoeae aquaticae seedling damping off Prevention effect presses every 667m260kg applies ratio by every 667m2The prevention effect that 40-50kg applies will be got well;Auxiliary agent [4-(diformazan Amine) phenyl]-diimine sodium sulfonate press every 667m23.0-5.0g applies has certain preventing and treating effect to Caulis et Folium Ipomoeae aquaticae seedling damping off Really.
The effect is significant processing 28-33 is better than processing 34-36, CK4, and the effect processing 29 is better than process 28,30 again, processes 33 effect is significantly better than process 31-32 again.I.e. the prevention effect of calcareous calcium lime powder foot couple Fructus Cucurbitae moschatae seedling damping off is pressed often 667m250kg applies ratio by every 667m240th, the prevention effect that 60kg applies will be got well;Albefaction vegetation ashes are dampinged off to Fructus Cucurbitae moschatae seedling The prevention effect of disease presses every 667m260kg applies ratio by every 667m2The prevention effect that 40-50kg applies will be got well;Auxiliary agent [4- (dimethylamine) phenyl]-diimine sodium sulfonate press every 667m23.0-5.0g applies the prevention effect to Fructus Cucurbitae moschatae seedling damping off not Significantly.
Above test shows, presses every 667m with albefaction vegetation ashes2The effect is significant that 40-60kg applies is better than calcareous life Lime powder presses every 667m2The effect that 40-60kg applies, calcareous quick lime powder is significantly better than CK and [4-(dimethylamine) again Phenyl]-diimine sodium sulfonate administration effect.Its effect when [4-(dimethylamine) phenyl]-diimine sodium sulfonate is used alone Effect not as albefaction vegetation ashes and calcareous quick lime powder.
Compatibility mechanism
Compatibility mechanism is mainly qualitative and quantitative and measures the effect that each ingredients is prevented and treated to vegetable seedling damping off Test.
Materials and methods
2.1.1 test material
Test vegetable species are Amaranthus mangostanus L., the seedling of Fructus Cucumidis sativi, Caulis et Folium Ipomoeae aquaticae and four kinds of vegetables of Fructus Cucurbitae moschatae.Test ingredients is:Calcareous life Lime powder, albefaction vegetation ashes and [4-(dimethylamine) phenyl]-diimine sodium sulfonate.
Test method
Test is carried out in Yiyang proving ground.From former years regular incidence humidity be in hypersaturated state early spring plastics big Carry out in canopy.Preventing and treating as described herein refers to stop disease from continuing to spread, rather than the treatment to strain of falling ill, because falling ill Even if being also there is no use value after strain treatment is good.Enter when damping off in the seedling such as Amaranthus mangostanus L., Fructus Cucumidis sativi, Caulis et Folium Ipomoeae aquaticae and Fructus Cucurbitae moschatae Row prevention effect is tested;Comparison is located at same seedbed.After test effect is mainly fallen ill with same vegetable seedling, with normal strain The percentage ratio reducing is counting and statistical analysiss(Do not include after diseased plant is treated, leaving the shoot of symptom vestige), in combination with Seedbed is observed.
Amaranthus mangostanus L., Fructus Cucumidis sativi, Caulis et Folium Ipomoeae aquaticae and four kinds of vegetables of Fructus Cucurbitae moschatae, in Seedling Stage, during damping off outburst, select vegetable seedling in the morning Processed when dew is had on blade.Each ingredients is applied proportional quantity and is seen the description to each process:Calcareous quick lime powder is pressed no Water dry ash Mass Calculation, albefaction vegetation ashes press anhydrous dry ash Mass Calculation, [4-(dimethylamine) phenyl]-diimine sodium sulfonate Calculate by 100% purity Coriolis mass.After administration, 3d does not sprinkle water or applies fertilizer, and is observed and count during 3d.Conventional fertilizer water pipe after 3d Reason and the prevention and control of plant diseases, pest control.
40 process of test setting(Including comparison), each processes 3 repetitions, and each repeats 0.10m2, random distribution.The During 0d, normal strain is carried out counting 1 time, during 3d, normal strain is carried out counting 1 time again, the strain number percentage ratio being reduced with normal strain As the effect processing, do not counted with diseased plant and be because after diseased plant 1~2d just disappearing in native bed it is difficult to count.Normal strain refers to The seedling of any disease symptoms of dampinging off does not occur.In the vegetable seedling phase, when a large amount of damping off diseased plant occurs, i.e. the damping off outbreak period (Basal part of stem is in water stain shape), ingredients is uniformly spread fertilizer over the fields in seedbed by following process.
Process 1:Amaranthus mangostanus L. seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous calcium lime powder End:The mass ratio of albefaction vegetation ashes is 1.0: 5000.0:8000.0 press every 667m240kg applies;Process 2:Amaranthus mangostanus L. seedling Damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes For 1.0: 5000.0:8000.0 press every 667m250kg applies;Process 3:Amaranthus mangostanus L. seedling damping off [4-(dimethylamine) Phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.0: 5000.0:8000.0 pressing Every 667m260kg applies;Process 4:Amaranthus mangostanus L. seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous Quick lime powder:The mass ratio of albefaction vegetation ashes is 1.2:5500.0:8500.0 press every 667m240kg applies;Process 5: Amaranthus mangostanus L. seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:Albefaction vegetation ashes Mass ratio be 1.2:5500.0:8500.0 press every 667m250kg applies;Process 6:Amaranthus mangostanus L. seedling damping off [4- (dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.2:5500.0: 8500.0 press every 667m260kg applies;Process 7:Amaranthus mangostanus L. seedling damping off [4-(dimethylamine) phenyl]-diimine sulfonic acid Sodium:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.5: 6000.0:9000.0 press every 667m240g applies; Process 8:Amaranthus mangostanus L. seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:Albefaction grass The mass ratio of wood ash cinder is 1.5: 6000.0:9000.0 press every 667m250g applies;Process 9:Amaranthus mangostanus L. seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.5: 6000.0:9000.0 press every 667m260g applies;CK1:Amaranthus mangostanus L. seedling compares, and does not apply ingredients.Process 10:Cucumber seedling is sudden Sick [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.0: 5000.0:8000.0 press every 667m240kg applies;Process 11:Cucumber seedling damping off [4-(dimethylamine) benzene Base]-diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.0: 5000.0:8000.0 by every 667m250kg applies;Process 12:Cucumber seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous life Lime powder:The mass ratio of albefaction vegetation ashes is 1.0: 5000.0:8000.0 press every 667m260kg applies;Process 13: Cucumber seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:Albefaction vegetation ashes Mass ratio be 1.2:5500.0:8500.0 press every 667m240kg applies;Process 14:Cucumber seedling damping off [4- (dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.2:5500.0: 8500.0 press every 667m250kg applies;Process 15:Cucumber seedling damping off [4-(dimethylamine) phenyl]-diimine sulphur Sour sodium:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.2:5500.0:8500.0 press every 667m260kg applies With;Process 16:Cucumber seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:In vain The mass ratio changing vegetation ashes is 1.5: 6000.0:9000.0 press every 667m240g applies;Process 17:Cucumber seedling is dampinged off Sick [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.5: 6000.0:9000.0 press every 667m250g applies;Process 18:Cucumber seedling damping off [4-(dimethylamine) benzene Base]-diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.5: 6000.0:9000.0 by every 667m260g applies;CK2:Cucumber seedling compares, and does not apply ingredients.Process 19:Caulis et Folium Ipomoeae aquaticae seedling damping off [4-(diformazan Amine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.0: 5000.0: 8000.0 press every 667m240kg applies;Process 20:Caulis et Folium Ipomoeae aquaticae seedling damping off [4-(dimethylamine) phenyl]-diimine sulphur Sour sodium:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.0: 5000.0:8000.0 press every 667m250kg applies With;Process 21:Caulis et Folium Ipomoeae aquaticae seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:In vain The mass ratio changing vegetation ashes is 1.0: 5000.0:8000.0 press every 667m260kg applies;Process 22:Caulis et Folium Ipomoeae aquaticae seedling is dampinged off Sick [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.2:5500.0:8500.0 press every 667m240kg applies;Process 23:Caulis et Folium Ipomoeae aquaticae seedling damping off [4-(dimethylamine) benzene Base]-diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.2:5500.0:8500.0 by every 667m250kg applies;Process 24:Caulis et Folium Ipomoeae aquaticae seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous life Lime powder:The mass ratio of albefaction vegetation ashes is 1.2:5500.0:8500.0 press every 667m260kg applies;Process 25:Water spinach Dish seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:Albefaction vegetation ashes Mass ratio is 1.5: 6000.0:9000.0 press every 667m240g applies;Process 26:Caulis et Folium Ipomoeae aquaticae seedling damping off [4-(two Methylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.5: 6000.0: 9000.0 press every 667m250g applies;Process 27:Caulis et Folium Ipomoeae aquaticae seedling damping off [4-(dimethylamine) phenyl]-diimine sulfonic acid Sodium:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.5: 6000.0:9000.0 press every 667m260g applies; CK3:Caulis et Folium Ipomoeae aquaticae seedling compares, and does not apply ingredients.Process 28:Fructus Cucurbitae moschatae seedling damping off [4-(dimethylamine) phenyl]-diimine Sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.0: 5000.0:8000.0 press every 667m240kg Apply;Process 29:Fructus Cucurbitae moschatae seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder: The mass ratio of albefaction vegetation ashes is 1.0: 5000.0:8000.0 press every 667m250kg applies;Process 30:Fructus Cucurbitae moschatae seedling is sudden Sick [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.0: 5000.0:8000.0 press every 667m260kg applies;Process 31:Fructus Cucurbitae moschatae seedling damping off [4-(dimethylamine) benzene Base]-diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.2:5500.0:8500.0 by every 667m240kg applies;Process 32:Fructus Cucurbitae moschatae seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous life Lime powder:The mass ratio of albefaction vegetation ashes is 1.2:5500.0:8500.0 press every 667m250kg applies;Process 33:South Melon seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:Albefaction vegetation ashes Mass ratio is 1.2:5500.0:8500.0 press every 667m260kg applies;Process 34:Fructus Cucurbitae moschatae seedling damping off [4-(two Methylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.5: 6000.0: 9000.0 press every 667m240g applies;Process 35:Fructus Cucurbitae moschatae seedling damping off [4-(dimethylamine) phenyl]-diimine sulfonic acid Sodium:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.5: 6000.0:9000.0 press every 667m250g applies; Process 36:Fructus Cucurbitae moschatae seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:Albefaction grass The mass ratio of wood ash cinder is 1.5: 6000.0:9000.0 press every 667m260g applies;CK4:Fructus Cucurbitae moschatae seedling compares, and does not apply Ingredients.
Statistical analysiss
SAS is adopted to test data(6.12)Carry out statistical analysiss.As known from Table 2, process 1-9 prevents and treats Amaranthus mangostanus L. seedling and dampings off The effect is significant of disease is better than CK1, and the effect processing 5-6 is significantly better than process 1-3,7-9, i.e. [4-(dimethylamine) phenyl]-two again Imines sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.2:5500.0:The ingredients of 8500.0 compatibilities Prevention effect be significantly better than 1.0: 5000.0:The ingredients of 8000.0 compatibilities and 1.5: 6000.0:The joining of 9000.0 compatibilities The prevention effect of agent.
Process the effect no significant difference of 2-3, process the effect no significant difference of 5-6, process the effect no significance difference of 8-9 Different, that is, press every 667m250kg and 667m2The effect that 60kg administration prevents and treats Amaranthus mangostanus L. seedling damping off is essentially identical.From Financial cost Consider, with by every 667m2It is preferably consumption that 50kg applies.The effect is significant processing 10-18 preventing and treating cucumber seedling damping off is excellent In CK2, the effect processing 14-15 is significantly better than process 10-12,16-18, i.e. [4-(dimethylamine) phenyl]-diimine sulfonic acid again Sodium:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.2:5500.0:The preventing and treating effect of the ingredients of 8500.0 compatibilities Fruit is significantly better than 1.0: 5000.0:The ingredients of 8000.0 compatibilities and 1.5: 6000.0:The preventing and treating of the ingredients of 9000.0 compatibilities Effect.
Process the effect no significant difference of 11-12, process the effect no significant difference of 14-15, process, the effect of 17-18 No significant difference, that is, press every 667m250kg and 667m2The effect that 60kg applies preventing and treating cucumber seedling damping off is essentially identical.From Financial cost considers, with by every 667m2It is preferably consumption that 50kg applies.
When table 2. compatibility mechanism processes 3d, the strain number of normal strain reduces percentage ratio(Unit:%)
Process 15d Process 15d Process 15d Process 15d
Process 1 10.46±2.57b Process 10 7.61±1.64b Process 19 5.98±1.26c Process 28 4.92±0.64bc
Process 2 7.38±1.24c Process 11 6.26±2.17c Process 20 4.65±0.60d Process 29 2.61±0.38c
Process 3 7.87±0.86c Process 12 6.84±0.53c Process 21 5.44±1.33cd Process 30 3.19±0.52c
Process 4 2.94±0.39d Process 13 2.61±0.67d Process 22 1.81±0.38e Process 31 1.27±0.29d
Process 5 1.27±0.43e Process 14 1.50±0.35e Process 23 0.92±0.60e Process 32 0.70±0.41d
Process 6 1.60±0.61e Process 15 1.28±0.49e Process 24 1.12±0.47e Process 33 1.08±0.39d
Process 7 2.51±0.50d Process 16 7.84±0.82b Process 25 7.50±0.39b Process 34 5.81±0.41b
Process 8 2.14±2.72d Process 17 3.28±0.39d Process 26 4.64±0.65d Process 35 3.74±0.38c
Process 9 2.70±0.64d Process 18 3.19±0.42d Process 27 4.27±0.81d Process 36 3.30±0.27c
CK1 35.18±3.65a CK2 33.85±4.27a CK3 46.27±3.19a CK4 24.17±5.14a
Note:Lower case is 0.05 level, same row difference letter representation significant difference, similarly hereinafter.
Table 2 shows, processes 19-27 and prevents and treats the effect is significant of Caulis et Folium Ipomoeae aquaticae seedling damping off better than CK3, processes the effect of 22-24 It is significantly better than process 19-21,25-27, i.e. [4-(dimethylamine) phenyl]-diimine sodium sulfonate again:Calcareous quick lime powder:In vain The mass ratio changing vegetation ashes is 1.2:5500.0:The prevention effect of the ingredients of 8500.0 compatibilities is significantly better than 1.0: 5000.0:The ingredients of 8000.0 compatibilities and 1.5: 6000.0:The prevention effect of the ingredients of 9000.0 compatibilities.Process 20-21's Effect no significant difference, processes the effect no significant difference of 23-24, processes, the effect no significant difference of 26-27, that is, press every 667m250kg and 667m2The effect that 60kg applies preventing and treating Caulis et Folium Ipomoeae aquaticae seedling damping off is essentially identical.Consider from Financial cost, with pressing Every 667m2It is preferably consumption that 50kg applies.
Process 28-36 and prevent and treat the effect is significant of Fructus Cucurbitae moschatae seedling damping off better than CK4, the effect processing 31-33 is again significantly excellent In process 28-30,34-36, i.e. [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:Albefaction plant ash The mass ratio of cinder is 1.2:5500.0:The prevention effect of the ingredients of 8500.0 compatibilities is significantly better than 1.0: 5000.0: 8000.0 The ingredients of compatibility and 1.5: 6000.0:The prevention effect of the ingredients of 9000.0 compatibilities.Process the effect no significance difference of 29-30 Different, process the effect no significant difference of 32-33, process, the effect no significant difference of 35-36, that is, press every 667m250kg with 667m2The effect that 60kg applies preventing and treating Fructus Cucurbitae moschatae seedling damping off is essentially identical.Consider from Financial cost, with by every 667m250kg Administration is preferably consumption.Thus also can learn, the process of 3 kinds of different compatibility ratios is not only all significantly better than comparison CK(Table 2), It is significantly better than the effect that each ingredients composition is used alone(Table 1), three has significant association in this ratio compatibility to prevention effect Same-action.
Above test shows, the process of 3 kinds of different compatibility ratios is all significantly better than comparison CK.But [4-(dimethylamine) phenyl]- Diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.2:5500.0:8500.0 press every 667m2 The effect is significant that 50kg applies preventing and treating vegetable seedling damping off is better than CK and other process, and the best cost of its effect is again economical.
Auxiliary agent is tested
Auxiliary agent test is mainly the impact that qualitative and quantitative measures the prevention effect to whole ingredients for the auxiliary agent.
Materials and methods
3.1.1 test material
Test vegetable species are Amaranthus mangostanus L., the seedling of Fructus Cucumidis sativi, Caulis et Folium Ipomoeae aquaticae and four kinds of vegetables of Fructus Cucurbitae moschatae.Test ingredients is calcareous calculogenesis Grey powder, albefaction vegetation ashes, auxiliary agent is [4-(dimethylamine) phenyl]-diimine sodium sulfonate.
Test method
Test is carried out in Yiyang proving ground.From former years regular incidence humidity be in hypersaturated state early spring plastics big Carry out in canopy.Preventing and treating as described herein refers to stop disease from continuing to spread, rather than the treatment to strain of falling ill, because falling ill Even if being also there is no use value after strain treatment is good.Enter when damping off in the seedling such as Amaranthus mangostanus L., Fructus Cucumidis sativi, Caulis et Folium Ipomoeae aquaticae and Fructus Cucurbitae moschatae Row prevention effect is tested;Comparison is located at same seedbed.After test effect is mainly fallen ill with same vegetable seedling, with normal strain The percentage ratio reducing is counting and statistical analysiss(Do not include after diseased plant is treated, leaving the shoot of symptom vestige), in combination with Seedbed is observed.
Amaranthus mangostanus L., Fructus Cucumidis sativi, Caulis et Folium Ipomoeae aquaticae and four kinds of vegetables of Fructus Cucurbitae moschatae, in Seedling Stage, during damping off outburst, select vegetable seedling in the morning Processed when dew is had on blade.Each ingredients is applied proportional quantity and is seen the description to each process:Calcareous quick lime powder is pressed no Water dry ash Mass Calculation, albefaction vegetation ashes press anhydrous dry ash Mass Calculation, [4-(dimethylamine) phenyl]-diimine sodium sulfonate Calculate by 100% purity Coriolis mass.After administration, 3d does not sprinkle water or applies fertilizer, and is observed and count during 3d.Conventional fertilizer water pipe after 3d Reason and the prevention and control of plant diseases, pest control.
16 process of test setting(Including comparison), each processes 3 repetitions, and each repeats 0.10m2, random distribution.The During 0d, normal strain is carried out counting 1 time, during 3d, normal strain is carried out counting 1 time again, the strain number percentage ratio being reduced with normal strain As the effect processing, do not counted with diseased plant and be because after diseased plant 1~2d just disappearing in native bed it is difficult to count.Normal strain refers to The seedling of any disease symptoms of dampinging off does not occur.In the vegetable seedling phase, when a large amount of damping off diseased plant occurs, i.e. the damping off outbreak period (Basal part of stem is in water stain shape), ingredients is uniformly spread fertilizer over the fields in seedbed by following process.
Process 1:Amaranthus mangostanus L. seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous calcium lime powder End:The mass ratio of albefaction vegetation ashes is 1.2:5500.0:8500.0 press every 667m250kg applies;Process 2:Amaranthus mangostanus L. seedling The calcareous quick lime powder of damping off:The mass ratio of albefaction vegetation ashes is 5.5:8.5 press every 667m250kg applies;Place Reason 3:Amaranthus mangostanus L. seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate presses every 667m24.0g applying;CK1:Herba Amaranthi tricoloriss Dish seedling compares, and does not apply ingredients.Process 4:Cucumber seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate: Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.2:5500.0:8500.0 press every 667m250kg applies;Place Reason 5:The calcareous quick lime powder of cucumber seedling damping off:The mass ratio of albefaction vegetation ashes is 5.5:8.5 press every 667m2 50kg applies;Process 6:Cucumber seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate presses every 667m24.0g Apply;CK2:Cucumber seedling compares, and does not apply ingredients.Process 7:Caulis et Folium Ipomoeae aquaticae seedling damping off [4-(dimethylamine) phenyl]-two Imines sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.2:5500.0:8500.0 press every 667m2 50kg applies;Process 8:The calcareous quick lime powder of Caulis et Folium Ipomoeae aquaticae seedling damping off:The mass ratio of albefaction vegetation ashes is 5.5: 8.5 press every 667m250kg applies;Process 9:Caulis et Folium Ipomoeae aquaticae seedling damping off [4-(dimethylamine) phenyl]-diimine sodium sulfonate By every 667m24.0g applying;CK3:Caulis et Folium Ipomoeae aquaticae seedling compares, and does not apply ingredients.Process 10:Fructus Cucurbitae moschatae seedling damping off [4- (dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.2:5500.0: 8500.0 press every 667m250kg applies;Process 11:The calcareous quick lime powder of Fructus Cucurbitae moschatae seedling damping off:Albefaction vegetation ashes Mass ratio be 5.5:8.5 press every 667m250kg applies;Process 12:Fructus Cucurbitae moschatae seedling damping off [4-(dimethylamine) benzene Base]-diimine sodium sulfonate press every 667m24.0g applying;CK4:Fructus Cucurbitae moschatae seedling compares, and does not apply ingredients.
Statistical analysiss
SAS is adopted to test data(6.12)Carry out statistical analysiss.As known from Table 3, process 1 and prevent and treat Amaranthus mangostanus L. seedling damping off Effect is significant be better than CK1 with process 2-3, process 2 effect be significantly better than process 3 again, i.e. [4-(dimethylamine) phenyl]-two Imines sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.2:5500.0:The ingredients of 8500.0 compatibilities Prevention effect preferably, be secondly calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 5.5:The ingredients of 8.5 compatibilities Prevention effect, thirdly for [4-(dimethylamine) phenyl]-diimine sodium sulfonate press every 667m2The preventing and treating effect that 4.0g applies Really.Test shows, only auxiliary agent [4-(dimethylamine) phenyl] though-diimine sodium sulfonate also has significant prevention effect, remote not And ingredients processes the prevention effect of 1-2;The prevention effect of the no process 2 of auxiliary agent ingredients is again far away from the process 1 having auxiliary agent ingredients Prevention effect.Thus illustrate, auxiliary agent [4-(dimethylamine) phenyl]-diimine sodium sulfonate is for having in this ingredients significantly Potentiation.
Process 4 effect is significants preventing and treating cucumber seedling damping ofies to be better than CK2 and process 5-6, process 5 effect and significantly excellent In process 6, i.e. [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes For 1.2:5500.0:The prevention effect of the ingredients of 8500.0 compatibilities preferably, is secondly calcareous quick lime powder:Albefaction plant ash The mass ratio of cinder is 5.5:The prevention effect of the ingredients of 8.5 compatibilities, thirdly for [4-(dimethylamine) phenyl]-diimine sulfonic acid Sodium presses every 667m2The prevention effect that 4.0g applies.Test shows, only auxiliary agent [4-(dimethylamine) phenyl]-diimine sulfonic acid The prevention effect of 4-5 though sodium also has significant prevention effect, is processed far away from ingredients;The preventing and treating of the no process 5 of auxiliary agent ingredients Effect is again far away from the prevention effect of the process 4 having auxiliary agent ingredients.Thus illustrate, auxiliary agent [4-(dimethylamine) phenyl]-diimine Sodium sulfonate is used in this ingredients, preventing and treating cucumber seedling damping off being had significant synergies.
The strain number of normal strain during table 3. auxiliary agent test process 3d reduces percentage ratio(Unit:%)
Process 15d Process 15d Process 15d Process 15d
Process 1 1.27±1.24d Process 4 1.50±2.41d Process 7 0.92±0.55d Process 10 0.70±3.27c
Process 2 8.50±2.29c Process 5 6.29±4.08c Process 8 12.64±6.81c Process 11 9.61±1.34b
Process 3 32.46±0.94b Process 6 31.50±1.53b Process 9 39.40±2.09b Process 12 23.64±4.39a
CK1 35.18±2.08a CK2 33.85±1.17a CK3 46.27±4.11a CK4 24.17±5.14a
Note:Lower case is 0.05 level, same row difference letter representation significant difference, similarly hereinafter.
Process 7 effect is significants preventing and treating Caulis et Folium Ipomoeae aquaticae seedling damping ofies to be better than CK3 and process 8-9, process 8 effect and significantly excellent In process 9, i.e. [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes For 1.2:5500.0:The prevention effect of the ingredients of 8500.0 compatibilities preferably, is secondly calcareous quick lime powder:Albefaction plant ash The mass ratio of cinder is 5.5:The prevention effect of the ingredients of 8.5 compatibilities, thirdly for [4-(dimethylamine) phenyl]-diimine sulfonic acid Sodium presses every 667m2The prevention effect that 4.0g applies.Test shows, only auxiliary agent [4-(dimethylamine) phenyl]-diimine sulfonic acid The prevention effect of 7-8 though sodium also has significant prevention effect, is processed far away from ingredients;The preventing and treating of the no process 8 of auxiliary agent ingredients Effect is again far away from the prevention effect of the process 7 having auxiliary agent ingredients.Thus illustrate, auxiliary agent [4-(dimethylamine) phenyl]-diimine Sodium sulfonate is used in this ingredients, preventing and treating Caulis et Folium Ipomoeae aquaticae seedling damping off being had significant synergies.
The effect is significants of process 10 preventing and treating Fructus Cucurbitae moschatae seedling damping ofies are better than CK4 and process 11-12, and the effect of process 11 shows again Write and be better than process 12, i.e. [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:The matter of albefaction vegetation ashes Amount ratio is 1.2:5500.0:The prevention effect of the ingredients of 8500.0 compatibilities preferably, is secondly calcareous quick lime powder:Albefaction grass The mass ratio of wood ash cinder is 5.5:The prevention effect of the ingredients of 8.5 compatibilities, thirdly for [4-(dimethylamine) phenyl]-diimine Sodium sulfonate presses every 667m2The prevention effect that 4.0g applies.Test shows, only auxiliary agent [4-(dimethylamine) phenyl]-diimine The no significant prevention effect of sodium sulfonate and CK4;But the prevention effect of the no process 11 of auxiliary agent ingredients is again far away from there being auxiliary agent ingredients Process 10 prevention effect.Thus illustrate, auxiliary agent [4-(dimethylamine) phenyl]-diimine sodium sulfonate is used for right in this ingredients Preventing and treating Fructus Cucurbitae moschatae seedling damping off has significant synergies.
Above test shows(Table 3), significantly, the effect is significant of adding assistant is better than the difference on effect of adding assistant and not adding assistant The not effect of adding assistant, not its effect is significant of adding assistant reduction.
Test also shows(Table 1-3), vegetable seedling damping off calcareous quick lime powder, albefaction vegetation ashes compatibility are whether Effect be all significantly higher than CK;The effect of used additives has significant prevention effect to some vegetable seedling damping ofies, to indivedual Vegetable seedling damping off and CK are not significantly different from;Auxiliary agent [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime Powder:The mass ratio of albefaction vegetation ashes is 1.2:5500.0:8500.0 press every 667m2The compatibility that 50kg applies is most preferably to join 5, effect is best(Table 1-3).
It has often been said that plant ash typically refer to black rice husk or the stalk of carbonization, imperfect combustion clean, still leave big The carbon of amount, so be in black.And albefaction vegetation ashes, it is the greyish white of formation after the faggots such as Cereal rice husk, stalk burn completely The ashes of color, remaining carbon electrode is few, belongs to alkalescence, rather than the black plant ash of carbonization.Plant ash and albefaction vegetation ashes are to vegetable children The prevention effect of Seedling damping off is completely different, so it is impossible to substituting albefaction vegetation ashes with plant ash.Albefaction vegetation ashes contain The various nutrient elements that crops need, such as phosphorus, potassium, calcium, magnesium, sulfur, boron, zinc, molybdenum, copper etc., wherein with potassium, calcium content for Many, typically contain 5% to 15% effective potassium it is adaptable to soil in addition to salt-soda soil, be particularly suited for acid ground.It is made With having:1. improve the soil moisture:The soil moisture can be effectively improved, keep loosing soil, the damage to plants caused by sudden drop in temperature effect low to soil temperature is notable. 2. accelerate to take root:The absorbability of fertilizer can be increased using albefaction vegetation ashes, promote wound healing, rotten in wound and root Fasten plant ash, can control rotten, inspire new root, recover its growing way, seedling has been inspired with new root effect notable.3 preventing disease pest controls: Preventing and treating root maggot, rhizosphere nematode etc.;The albefaction vegetation ashes attaching on blade also have the effect preventing and treating blade pest and disease damage.To rotten It is notable that seedling sends out new root effect.4. strengthen resistance:Because containing, in albefaction vegetation ashes, the potassium ion dissociating in a large number, can drop The Transpiration Intensity of low blades, strengthens the ability of drought resisting high temperature resistance, and potassium ion can also promote the operating of carbohydrate, improves vegetable The resistance of dish seedling.5. prevent bleeding:The vegetable seedling damping off of rotten root easily produces bleeding, and albefaction vegetation ashes can control Bleeding, prevents wound infection from rotting, promotes healing.6. reduce rhizosphere soil pH value, the harmful gass such as hydrogen sulfide in suppression soil Generation.
Calcareous quick lime powder refers to powder rather than the Calx [Ca (OH) that its main component is CaO2] powder, magnesia stone Ash, without the lime particle that overdoes.The prevention effect of calcareous quick lime powder and hydrated lime in powder foot couple vegetable seedling damping off is completely Difference, so it is impossible to substitute calcareous quick lime powder with calcareous Calx powder.Calcareous quick lime powder is applied to seedbed, its One, can leniently improve early spring nursery bed temperature, and seedling will not be injured;Second, water absorption is strong, seedbed can be dried, be unfavorable for disease The growth and breeding of opportunistic pathogen.Calcium in calcareous quick lime powder is one of nutrient that vegetable seedling needs, and Rational Application is calcareous Quick lime powder can not only meet the needs to calcium constituent for the vegetable seedling, and, play the role of much beneficial:Calcareous calcium lime powder End is the acid good raw material of sweetening of the soil, can promote Aluminium in Soil, Fe and Mn precipitation, eliminate and poison;Calcareous quick lime powder The organic matter decomposition such as straw-returning can be promoted, the organic acid producing during neutralization organic matter decomposition, it is to avoid organic hyper acid and Cause vegetable seedling that the symptoms such as damping off occur;Apply calcareous quick lime powder and can improve Soil structure, increase effective ingredient, energy Activating soil fertility, parasite killing deweeding, mitigate disease pest harm, prevent damping off, promote vegetable seedling early growth and quick tiller.
[4-(dimethylamine) phenyl]-diimine sulfonate sodium is white particle, powder or crystalline powder, soluble in water, Belong to strong base weak acid sodium salt, retention is stable at a high ph, produce after hydrolysis [4-(dimethylamine) phenyl]-diimine sulphur from Son and sodium ion, its [4-(dimethylamine) phenyl]-diimine sulphur ion can be combined with bacterium protein, changes bacterium protein Property, so that growth and sporulation is obstructed, play bactericidal action;[4-(dimethylamine) phenyl]-diimine sulphur ion also whitening Vegetation ashes, the sterilization of calcareous quick lime have very strong potentiation;The growth of plant seedlings can also effectively utilizes diimine Ion;[4-(dimethylamine) phenyl]-diimine sulfonate sodium and albefaction vegetation ashes, calcareous quick lime powder have good mixing Joining property, application effect is preferable.So, [4-(dimethylamine) phenyl]-diimine sulfonate sodium and albefaction vegetation ashes, calcareous life Lime powder mixture, can promote bactericidal action, and the root growth that improvement causes because of damping off is bad, promote the morning of root system raw fast Send out, whitening vegetation ashes, the effect of calcareous quick lime powder have potentiation, are its good auxiliary agents.
This control agent has significant preventive and therapeutic effect to vegetable seedling damping off, not only to soil noresidue, also improves The effect of Soil structure, is a kind of preferable vegetable seedling damping off control agent.
Specific embodiment
Implementation below and embodiment are intended to further illustrate the present invention, rather than limitation of the present invention.
Calcareous quick lime powder, albefaction vegetation ashes carry out compatibility with anhydrous dry ash, and [4-(dimethylamine) phenyl]-two is sub- The pure percentage composition of amine sodium sulfonate does not have particular/special requirement, and its impurity, on the premise of not affecting its stability, reaches during compatibility Net content required by formula.Calcareous for vegetable seedling damping off control agent quick lime powder:Albefaction vegetation ashes:[4 - (dimethylamine) phenyl]-diimine sodium sulfonate net content press 1.0~1.5:5000.0~6000.0:8000.0~9000.0 Ratio mixes, and preferably 1.2:5500.0:8500.0, [4-(dimethylamine) phenyl]-diimine sodium sulfonate presses 100% purity Coriolis mass Calculate, calcareous quick lime powder, albefaction vegetation ashes press anhydrous dry ash Mass Calculation.Plastic bag sealing is packed, and shady and cool drying keeps away Preserve at light, preserve 1 year.
Using method:In the vegetable seedling phase, before the disease symptoms that occur dampinging off or during damping off outburst, anti- mixed Control agent by every 667m240~60kg uniformly spreads fertilizer over the fields in seedbed.Select to have on vegetable seedling blade in the morning and carry out during dew Spread fertilizer over the fields, strengthen prevention effect.
Embodiment 1:
Auxiliary agent [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:The quality of albefaction vegetation ashes Than for 1.0: 5000.0:8000.0 press every 667m2The prevention effect that 50kg applies:
Test is in the early spring hot house of Yiyang proving ground of hypersaturated state from former years regular incidence humidity OK.Test material:Test vegetable seedling species is Amaranthus mangostanus L., Fructus Cucumidis sativi, Caulis et Folium Ipomoeae aquaticae, 4 kinds of vegetable seedlings of Fructus Cucurbitae moschatae.Test ingredients is: Calcareous quick lime powder, albefaction vegetation ashes and [4-(dimethylamine) phenyl]-diimine sodium sulfonate, auxiliary agent [4-(dimethylamine) Phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.0: 5000.0:8000.0, [4-(dimethylamine) phenyl]-diimine sodium sulfonate is pressed 100% purity Coriolis mass and is calculated, calcareous quick lime powder, albefaction vegetation ashes By anhydrous dry ash Mass Calculation.Being selected in the vegetable seedling damping off outbreak period is prevented and treated;Comparison is arranged on same seedbed.
Auxiliary agent [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:Albefaction vegetation ashes three press Hereinafter process 1.0: 2000.0:1500.0 mixing(Calcareous quick lime powder, albefaction vegetation ashes are based on anhydrous dry ash quality Calculate;[4-(dimethylamine) phenyl]-diimine sodium sulfonate is pressed 100% purity Coriolis mass and is calculated), plastic bag sealing packaging, shady and cool lucifuge After place preserves 1 year, open packaging, in the vegetable seedling phase, during damping off outburst, control agent is pressed every 667m250kg uniformly spreads fertilizer over the fields In seedbed.Select to have on vegetable seedling blade in the morning and spread fertilizer over the fields during dew, to strengthen prevention effect.
When processing 3d, count normal strain decrement, normal strain reduces percentage ratio and is respectively:Amaranthus mangostanus L. for 7.38%, CK is 35.18%, few 4.77 times than CK of normal strain decrement;Fructus Cucumidis sativi is 6.26%, CK is 33.85%, and normal strain decrement is few 5.41 than CK Times;Caulis et Folium Ipomoeae aquaticae is 4.65%, CK is 46.27%, few 9.95 times than CK of normal strain decrement;Fructus Cucurbitae moschatae is 2.61%, CK is 24.17%, just Often strain decrement is few 9.26 times than CK.
Result of implementation shows, [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:Albefaction plant ash Cinder three presses 1.0: 5000.0:The vegetable seedling damping off control agent of 8000.0 compatibilities, to preventing and treating vegetable seedling damping off effect Fruit is notable.
Embodiment 2:
Auxiliary agent [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:The quality of albefaction vegetation ashes Than for 1.2:5500.0:8500.0 press every 667m2The prevention effect that 50kg applies:
Test is in the early spring hot house of Yiyang proving ground of hypersaturated state from former years regular incidence humidity OK.Test material:Test vegetable seedling species is Amaranthus mangostanus L., Fructus Cucumidis sativi, Caulis et Folium Ipomoeae aquaticae, 4 kinds of vegetable seedlings of Fructus Cucurbitae moschatae.Test ingredients is: Calcareous quick lime powder, albefaction vegetation ashes and [4-(dimethylamine) phenyl]-diimine sodium sulfonate, auxiliary agent [4-(dimethylamine) Phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.2:5500.0:8500.0, [4 - (dimethylamine) phenyl]-diimine sodium sulfonate by 100% purity Coriolis mass calculating, press no by calcareous quick lime powder, albefaction vegetation ashes Water dry ash Mass Calculation.Being selected in the vegetable seedling damping off outbreak period is prevented and treated;Comparison is arranged on same seedbed.
Auxiliary agent [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:Albefaction vegetation ashes three press Hereinafter process 1.2:5500.0:8500.0 mixing(Calcareous quick lime powder, albefaction vegetation ashes press anhydrous dry ash Mass Calculation; [4-(dimethylamine) phenyl]-diimine sodium sulfonate is pressed 100% purity Coriolis mass and is calculated), plastic bag sealing is packed, and protects at shady and cool lucifuge After depositing 1 year, open packaging, in the vegetable seedling phase, during damping off outburst, control agent is pressed every 667m250kg uniformly spreads fertilizer over the fields in Seedling Bed.Select to have on vegetable seedling blade in the morning and spread fertilizer over the fields during dew, to strengthen prevention effect.
When processing 3d, count normal strain decrement, normal strain reduces percentage ratio and is respectively:Amaranthus mangostanus L. for 1.27%, CK is 35.18%, few 27.70 times than CK of normal strain decrement;Fructus Cucumidis sativi is 1.50%, CK is 33.85%, and normal strain decrement is fewer than CK 22.57 times;Caulis et Folium Ipomoeae aquaticae is 0.92%, CK is 46.27%, few 50.29 times than CK of normal strain decrement;Fructus Cucurbitae moschatae for 0.70%, CK is 24.17%, few 34.53 times than CK of normal strain decrement.
Result of implementation shows, [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:Albefaction plant ash Cinder three presses 1.2:5500.0:The vegetable seedling damping off control agent of 8500.0 compatibilities, to preventing and treating vegetable seedling damping off effect Significantly.
Embodiment 3:
Auxiliary agent [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:The quality of albefaction vegetation ashes Than for 1.5:6000.0:9000.0 press every 667m2The prevention effect that 50kg applies:
Test is in the early spring hot house of Yiyang proving ground of hypersaturated state from former years regular incidence humidity OK.Test material:Test vegetable seedling species is Amaranthus mangostanus L., Fructus Cucumidis sativi, Caulis et Folium Ipomoeae aquaticae, 4 kinds of vegetable seedlings of Fructus Cucurbitae moschatae.Test ingredients is: Calcareous quick lime powder, albefaction vegetation ashes and [4-(dimethylamine) phenyl]-diimine sodium sulfonate, auxiliary agent [4-(dimethylamine) Phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:The mass ratio of albefaction vegetation ashes is 1.5:6000.0:9000.0, [4 - (dimethylamine) phenyl]-diimine sodium sulfonate by 100% purity Coriolis mass calculating, press no by calcareous quick lime powder, albefaction vegetation ashes Water dry ash Mass Calculation.Being selected in the vegetable seedling damping off outbreak period is prevented and treated;Comparison is arranged on same seedbed.
Auxiliary agent [4-(dimethylamine) phenyl]-diimine sodium sulfonate:Calcareous quick lime powder:Albefaction vegetation ashes three press Hereinafter process 1.5:6000.0:9000.0 mixing(Calcareous quick lime powder, albefaction vegetation ashes press anhydrous dry ash Mass Calculation; [4-(dimethylamine) phenyl]-diimine sodium sulfonate is pressed 100% purity Coriolis mass and is calculated), plastic bag sealing is packed, and protects at shady and cool lucifuge After depositing 1 year, open packaging, in the vegetable seedling phase, during damping off outburst, control agent is pressed every 667m250kg uniformly spreads fertilizer over the fields in Seedling Bed.Select to have on vegetable seedling blade in the morning and spread fertilizer over the fields during dew, to strengthen prevention effect.
When processing 3d, count normal strain decrement, normal strain reduces percentage ratio and is respectively:Amaranthus mangostanus L. for 2.14%, CK is 35.18%, few 16.44 times than CK of normal strain decrement;Fructus Cucumidis sativi is 3.28%, CK is 33.85%, and normal strain decrement is fewer than CK 10.32 times;Caulis et Folium Ipomoeae aquaticae is 4.64%, CK is 46.27%, few 9.97 times than CK of normal strain decrement;Fructus Cucurbitae moschatae for 3.74%, CK is 24.17%, few 6.46 times than CK of normal strain decrement.Result of implementation shows, [4-(dimethylamine) phenyl]-diimine sodium sulfonate: Calcareous quick lime powder:Albefaction vegetation ashes three presses 1.5:6000.0:The vegetable seedling damping off control agent of 9000.0 compatibilities, To preventing and treating vegetable seedling damping off effect is significant.

Claims (3)

1. a kind of vegetable seedling damping off control agent is it is characterised in that described vegetable seedling damping off control agent is by calcareous calculogenesis Grey powder, albefaction vegetation ashes and auxiliary agent [4-(dimethylamine) phenyl]-diimine sulfonate sodium ([4- (dimethylamino) Phenyl]-diazenesulfonic acid, sodium salt) compatibility composition, wherein auxiliary agent [4-(dimethylamine) benzene Base]-diimine sulfonate sodium:Calcareous quick lime powder:The compatibility mass ratio of albefaction vegetation ashes is 1.0~1.5: 5000.0~6000.0:8000.0~9000.0, [4-(dimethylamine) phenyl]-diimine sulfonate sodium presses 100% purity Coriolis mass Calculate, calcareous quick lime powder, albefaction vegetation ashes press anhydrous dry ash Mass Calculation.
2. a kind of vegetable seedling damping off control agent according to claim 1 is it is characterised in that auxiliary agent [4-(dimethylamine) Phenyl]-diimine sulfonate sodium:Calcareous quick lime powder:The compatibility mass ratio of albefaction vegetation ashes is 1.2:5500.0: 8500.
3. a kind of using method of vegetable seedling damping off control agent as claimed in claim 2 it is characterised in that vegetable children Seedling stage, occur dampinging off disease symptoms when or before, the control agent having mixed by every 667m240~60kg uniformly spreads fertilizer over the fields in Seedling Bed, selects in the morning or has on dusk vegetable seedling blade and spread fertilizer over the fields during dew, to strengthen prevention effect, after administration, 3d can not Watering or fertilising, routine rich water quality management and the prevention and control of plant diseases, pest control after 3d, if outdoor seedbed, select will not rain within nearly 3d Fine day or the cloudy day, if rained within 3d after applying, then need after rain again to process.
CN201410712770.9A 2014-12-02 2014-12-02 Vegetable seedling damping-off control agent and application method thereof Expired - Fee Related CN104365673B (en)

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