CN104306415A - Preparation method of radix angelicae wall-broken decoction pieces - Google Patents
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- CN104306415A CN104306415A CN201410492327.5A CN201410492327A CN104306415A CN 104306415 A CN104306415 A CN 104306415A CN 201410492327 A CN201410492327 A CN 201410492327A CN 104306415 A CN104306415 A CN 104306415A
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
- A61K36/232—Angelica
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Abstract
The invention discloses a preparation method of radix angelicae wall-broken decoction pieces, wherein the radix angelicae wall-breaking decoction pieces are obtained through the steps of selecting fresh and alive radix angelicae, cleaning, drying, slicing, crushing, carrying out ultrafine grinding, granulating, sub-packaging and the like. The drug is promoted to be fully absorbed in a body, so that the utilization rate of effective components in radix angelicae is improved, and the drug efficacy performance is enhanced. In addition, the decoction pieces prepared through the preparation method are easy to store and stable in quality.
Description
Technical field
The present invention relates to Manufacture of medicinal slices of TCM technical field, particularly relate to a kind of preparation method of Radix Angelicae Dahuricae breaking cellular wall decoction pieces.
Background technology
The Radix Angelicae Dahuricae is Umbelliferae archangel.Be distributed in the ground such as northeast and North China of China's Mainland, be grown on the area of height above sea level 200 meters to 1,500 meters, be generally born in by sylvan life, border, small stream, shrubbery and meadow, mountain valley.The Radix Angelicae Dahuricae has wind-damp dispelling, evacuation of pus of invigorating blood circulation, effect of granulation promoting pain relieving, is usually used in the treatment of the symptoms such as headache, toothache, nasal sinusitis, hemorrhoidal hamorrhage anal fistula, leucorrhea with red and white discharge, ulcer sores, skin pruritus.
A kind of preparation method of angelica dahurica decoction pieces of the disclosure of the invention of CN102258552; obtaining particle diameter by cutting into slices to the Radix Angelicae Dahuricae, pulverizing is 300-350 object Radix Angelicae Dahuricae granule; 60 DEG C, dry Radix Angelicae Dahuricae granule under constant temperature, protect the effective ingredient of the Radix Angelicae Dahuricae preferably in manufacturing process.
Compared with above-mentioned prior art, the present invention is intended to the protection improving Radix Angelicae Dahuricae effective ingredient further, and under existence conditions, this has very large difficulty; In addition, the Radix Angelicae Dahuricae breaking cellular wall decoction pieces obtained by the inventive method stores convenience, steady quality, long shelf-life, can preserve the active ingredient of former medicine to greatest extent and go back the performance of crude drug in whole, effective ingredient more fully being absorbed, thus increase operation rate.
Summary of the invention
The technical problem solved:
In order to farthest protect the effective ingredient of the Radix Angelicae Dahuricae, improving the medical value of the Radix Angelicae Dahuricae, stablize quality of medicinal material, extend the shelf life, the invention provides a kind of preparation method of Radix Angelicae Dahuricae breaking cellular wall decoction pieces.
Technical scheme:
A preparation method for Radix Angelicae Dahuricae breaking cellular wall decoction pieces, comprises the following steps:
(1) select the fresh and alive Radix Angelicae Dahuricae, clean, naturally dry, section;
(2) adsorption type low temperature dried Radix Angelicae Dahuricae section: rotary dehumidifier rotating speed is 7-10r/h, process wind and regeneration wind flow are than being 3-5:1, and regeneration air temperature is 102-125 DEG C, process air temperature is 24-36 DEG C, process wind speed is 1.5-2.7m/s, process wind relative humidity 5-8%, air quantity 90-135m
3/ h, drying time 280-350 minute;
(3) tentatively pulverize: carry out wall breaking pulverization under Radix Angelicae Dahuricae section normal temperature condition step (2) drying completed, sieve, 105-150 order coarse powder;
(4) superfine grinding: the coarse powder of step (3) gained is placed in super micron mill, pulverizes 25-40 minute under 15-22 DEG C of condition, be crushed to 400-600 order, obtain Radix Angelicae Dahuricae micropowder;
(5) granulate: the Radix Angelicae Dahuricae micropowder of step (4) gained is spent ionized water and makes soft material, obtained soft material is put into rotary granulator, obtain Radix Angelicae Dahuricae granule;
(6) subpackage and packaging: the Radix Angelicae Dahuricae granule aseptically subpackage obtained by step (5), can obtain finished product.
As a preferred technical solution of the present invention, in step (1), the slice thickness of the fresh and alive Radix Angelicae Dahuricae is 2-5mm.
As a preferred technical solution of the present invention, in step (1), the slice thickness of the fresh and alive Radix Angelicae Dahuricae is 2-4mm.
As a preferred technical solution of the present invention, the dry run of step (2) comprises metamorphosis stage, constant rate drying period and falling rate drying period.
As a preferred technical solution of the present invention, in the making of the middle soft material of step (5), add 50-90 ml deionized water mix homogeneously in every 100g Radix Angelicae Dahuricae micropowder and make.
As a preferred technical solution of the present invention, in the making of the middle soft material of step (5), add 60-85 ml deionized water mix homogeneously in every 100g Radix Angelicae Dahuricae micropowder and make.
As a preferred technical solution of the present invention, step (6) subpackage and packaging process complete in sterilizing room, and the temperature of sterilizing room controls at 16-22 DEG C, and relative humidity is 40-60%.
As a preferred technical solution of the present invention, step (6) subpackage and packaging process complete in sterilizing room, and the temperature of sterilizing room controls at 16-20 DEG C, and relative humidity is 35-55%.
Beneficial effect
The Radix Angelicae Dahuricae breaking cellular wall decoction pieces that the preparation method of a kind of Radix Angelicae Dahuricae breaking cellular wall decoction pieces of the present invention is obtained has following beneficial effect: 2mg Radix Angelicae Dahuricae breaking cellular wall decoction pieces is rabbit gavage, have trivial solution heat effect to the rabbit generated heat caused by dorsal sc injection peptone, its effect is better than the aspirin of 0.15g/kg; The suppression ratio reacted mice acetic acid twisting is 69-78%; Also obvious inhibitory action is had to mouse ear inflammation.
Detailed description of the invention
Embodiment 1:
A preparation method for Radix Angelicae Dahuricae breaking cellular wall decoction pieces, comprises the following steps:
(1) select the fresh and alive Radix Angelicae Dahuricae, clean, naturally dry, section;
(2) adsorption type low temperature dried Radix Angelicae Dahuricae section: rotary dehumidifier rotating speed is 7r/h, process wind and regeneration wind flow are than being 3:1, and regeneration air temperature is 102 DEG C, and process air temperature is 24 DEG C, and process wind speed is 1.5m/s, process wind relative humidity 5%, air quantity 90m
3/ h, 280 minutes drying times;
(3) tentatively pulverize: carry out wall breaking pulverization under Radix Angelicae Dahuricae section normal temperature condition step (2) drying completed, sieve, 105 order coarse powder;
(4) superfine grinding: the coarse powder of step (3) gained is placed in super micron mill, pulverizes 25 minutes, is crushed to 400 orders, obtains Radix Angelicae Dahuricae micropowder under 15 DEG C of conditions;
(5) granulate: the Radix Angelicae Dahuricae micropowder of step (4) gained is spent ionized water and makes soft material, obtained soft material is put into rotary granulator, obtain Radix Angelicae Dahuricae granule;
(6) subpackage and packaging: the Radix Angelicae Dahuricae granule aseptically subpackage obtained by step (5), can obtain finished product.
As a preferred technical solution of the present invention, in step (1), the slice thickness of the fresh and alive Radix Angelicae Dahuricae is 2mm.
As a preferred technical solution of the present invention, the dry run of step (2) comprises metamorphosis stage, constant rate drying period and falling rate drying period.
As a preferred technical solution of the present invention, in the making of the middle soft material of step (5), add 90 ml deionized water mix homogeneously in every 100g Radix Angelicae Dahuricae micropowder and make.
As a preferred technical solution of the present invention, step (6) subpackage and packaging process complete in sterilizing room, and the temperature of sterilizing room controls at 16 DEG C, and relative humidity is 40%.
Embodiment 2:
A preparation method for Radix Angelicae Dahuricae breaking cellular wall decoction pieces, comprises the following steps:
(1) select the fresh and alive Radix Angelicae Dahuricae, clean, naturally dry, section;
(2) adsorption type low temperature dried Radix Angelicae Dahuricae section: rotary dehumidifier rotating speed is 8r/h, process wind and regeneration wind flow are than being 4:1, and regeneration air temperature is 110 DEG C, and process air temperature is 28 DEG C, and process wind speed is 1.8m/s, process wind relative humidity 6%, air quantity 110m
3/ h, 300 minutes drying times;
(3) tentatively pulverize: carry out wall breaking pulverization under Radix Angelicae Dahuricae section normal temperature condition step (2) drying completed, sieve, 125 order coarse powder;
(4) superfine grinding: the coarse powder of step (3) gained is placed in super micron mill, pulverizes 30 minutes, is crushed to 480 orders, obtains Radix Angelicae Dahuricae micropowder under 18 DEG C of conditions;
(5) granulate: the Radix Angelicae Dahuricae micropowder of step (4) gained is spent ionized water and makes soft material, obtained soft material is put into rotary granulator, obtain Radix Angelicae Dahuricae granule;
(6) subpackage and packaging: the Radix Angelicae Dahuricae granule aseptically subpackage obtained by step (5), can obtain finished product.
As a preferred technical solution of the present invention, in step (1), the slice thickness of the fresh and alive Radix Angelicae Dahuricae is 3mm.
As a preferred technical solution of the present invention, the dry run of step (2) comprises metamorphosis stage, constant rate drying period and falling rate drying period.
As a preferred technical solution of the present invention, in the making of the middle soft material of step (5), add 80 ml deionized water mix homogeneously in every 100g Radix Angelicae Dahuricae micropowder and make.
As a preferred technical solution of the present invention, step (6) subpackage and packaging process complete in sterilizing room, and the temperature of sterilizing room controls at 19 DEG C, and relative humidity is 48%.
Embodiment 3:
A preparation method for Radix Angelicae Dahuricae breaking cellular wall decoction pieces, comprises the following steps:
(1) select the fresh and alive Radix Angelicae Dahuricae, clean, naturally dry, section;
(2) adsorption type low temperature dried Radix Angelicae Dahuricae section: rotary dehumidifier rotating speed is 9r/h, process wind and regeneration wind flow are than being 4:1, and regeneration air temperature is 118 DEG C, and process air temperature is 32 DEG C, and process wind speed is 2.2m/s, process wind relative humidity 7%, air quantity 120m
3/ h, 320 minutes drying times;
(3) tentatively pulverize: carry out wall breaking pulverization under Radix Angelicae Dahuricae section normal temperature condition step (2) drying completed, sieve, 135 order coarse powder;
(4) superfine grinding: the coarse powder of step (3) gained is placed in super micron mill, pulverizes 35 minutes, is crushed to 550 orders, obtains Radix Angelicae Dahuricae micropowder under 20 DEG C of conditions;
(5) granulate: the Radix Angelicae Dahuricae micropowder of step (4) gained is spent ionized water and makes soft material, obtained soft material is put into rotary granulator, obtain Radix Angelicae Dahuricae granule;
(6) subpackage and packaging: the Radix Angelicae Dahuricae granule aseptically subpackage obtained by step (5), can obtain finished product.
As a preferred technical solution of the present invention, in step (1), the slice thickness of the fresh and alive Radix Angelicae Dahuricae is 4mm.
As a preferred technical solution of the present invention, the dry run of step (2) comprises metamorphosis stage, constant rate drying period and falling rate drying period.
As a preferred technical solution of the present invention, in the making of the middle soft material of step (5), add 70 ml deionized water mix homogeneously in every 100g Radix Angelicae Dahuricae micropowder and make.
As a preferred technical solution of the present invention, step (6) subpackage and packaging process complete in sterilizing room, and the temperature of sterilizing room controls at 22 DEG C, and relative humidity is 48%.
Embodiment 4:
A preparation method for Radix Angelicae Dahuricae breaking cellular wall decoction pieces, comprises the following steps:
(1) select the fresh and alive Radix Angelicae Dahuricae, clean, naturally dry, section;
(2) adsorption type low temperature dried Radix Angelicae Dahuricae section: rotary dehumidifier rotating speed is 10r/h, process wind and regeneration wind flow are than being 4.5:1, and regeneration air temperature is 121 DEG C, process air temperature is 34 DEG C, process wind speed is 2.5m/s, process wind relative humidity 8%, air quantity 130m
3/ h, 330 minutes drying times;
(3) tentatively pulverize: carry out wall breaking pulverization under Radix Angelicae Dahuricae section normal temperature condition step (2) drying completed, sieve, 140 order coarse powder;
(4) superfine grinding: the coarse powder of step (3) gained is placed in super micron mill, pulverizes 40 minutes, is crushed to 600 orders, obtains Radix Angelicae Dahuricae micropowder under 22 DEG C of conditions;
(5) granulate: the Radix Angelicae Dahuricae micropowder of step (4) gained is spent ionized water and makes soft material, obtained soft material is put into rotary granulator, obtain Radix Angelicae Dahuricae granule;
(6) subpackage and packaging: the Radix Angelicae Dahuricae granule aseptically subpackage obtained by step (5), can obtain finished product.
As a preferred technical solution of the present invention, in step (1), the slice thickness of the fresh and alive Radix Angelicae Dahuricae is 3mm.
As a preferred technical solution of the present invention, the dry run of step (2) comprises metamorphosis stage, constant rate drying period and falling rate drying period.
As a preferred technical solution of the present invention, in the making of the middle soft material of step (5), add 65 ml deionized water mix homogeneously in every 100g Radix Angelicae Dahuricae micropowder and make.
As a preferred technical solution of the present invention, step (6) subpackage and packaging process complete in sterilizing room, and the temperature of sterilizing room controls at 22 DEG C, and relative humidity is 55%.
Embodiment 5:
A preparation method for Radix Angelicae Dahuricae breaking cellular wall decoction pieces, comprises the following steps:
(1) select the fresh and alive Radix Angelicae Dahuricae, clean, naturally dry, section;
(2) adsorption type low temperature dried Radix Angelicae Dahuricae section: rotary dehumidifier rotating speed is 10r/h, process wind and regeneration wind flow are than being 5:1, and regeneration air temperature is 125 DEG C, and process air temperature is 36 DEG C, and process wind speed is 2.7m/s, process wind relative humidity 8%, air quantity 135m
3/ h, 350 minutes drying times;
(3) tentatively pulverize: carry out wall breaking pulverization under Radix Angelicae Dahuricae section normal temperature condition step (2) drying completed, sieve, 150 order coarse powder;
(4) superfine grinding: the coarse powder of step (3) gained is placed in super micron mill, pulverizes 40 minutes, is crushed to 600 orders, obtains Radix Angelicae Dahuricae micropowder under 22 DEG C of conditions;
(5) granulate: the Radix Angelicae Dahuricae micropowder of step (4) gained is spent ionized water and makes soft material, obtained soft material is put into rotary granulator, obtain Radix Angelicae Dahuricae granule;
(6) subpackage and packaging: the Radix Angelicae Dahuricae granule aseptically subpackage obtained by step (5), can obtain finished product.
As a preferred technical solution of the present invention, in step (1), the slice thickness of the fresh and alive Radix Angelicae Dahuricae is 5mm.
As a preferred technical solution of the present invention, the dry run of step (2) comprises metamorphosis stage, constant rate drying period and falling rate drying period.
As a preferred technical solution of the present invention, in the making of the middle soft material of step (5), add 50 ml deionized water mix homogeneously in every 100g Radix Angelicae Dahuricae micropowder and make.
As a preferred technical solution of the present invention, step (6) subpackage and packaging process complete in sterilizing room, and the temperature of sterilizing room controls at 22 DEG C, and relative humidity is 60%.
Zoopery discovery is carried out: 2mg Radix Angelicae Dahuricae breaking cellular wall decoction pieces is rabbit gavage according to the Radix Angelicae Dahuricae breaking cellular wall decoction pieces that the method for above-described embodiment 1-5 prepares, have trivial solution heat effect to the rabbit generated heat caused by dorsal sc injection peptone, its effect is better than the aspirin of 0.15g/kg; The suppression ratio of mice acetic acid twisting reaction is significantly increased; Also obvious inhibitory action is had to mouse ear inflammation.
Specific experiment result is as follows:
Claims (8)
1. a preparation method for Radix Angelicae Dahuricae breaking cellular wall decoction pieces, is characterized in that, comprises the following steps:
(1) select the fresh and alive Radix Angelicae Dahuricae, clean, naturally dry, section;
(2) adsorption type low temperature dried Radix Angelicae Dahuricae section: rotary dehumidifier rotating speed is 7-10r/h, process wind and regeneration wind flow are than being 3-5:1, and regeneration air temperature is 102-125 DEG C, process air temperature is 24-36 DEG C, process wind speed is 1.5-2.7m/s, process wind relative humidity 5-8%, air quantity 90-135m
3/ h, drying time 280-350 minute;
(3) tentatively pulverize: carry out wall breaking pulverization under Radix Angelicae Dahuricae section normal temperature condition step (2) drying completed, sieve, 105-150 order coarse powder;
(4) superfine grinding: the coarse powder of step (3) gained is placed in super micron mill, pulverizes 25-40 minute under 15-22 DEG C of condition, be crushed to 400-600 order, obtain Radix Angelicae Dahuricae micropowder;
(5) granulate: the Radix Angelicae Dahuricae micropowder of step (4) gained is spent ionized water and makes soft material, obtained soft material is put into rotary granulator, obtain Radix Angelicae Dahuricae granule;
(6) subpackage and packaging: the Radix Angelicae Dahuricae granule aseptically subpackage obtained by step (5), can obtain finished product.
2. the preparation method of a kind of Radix Angelicae Dahuricae breaking cellular wall decoction pieces according to claim 1, it is characterized in that, in step (1), the slice thickness of the fresh and alive Radix Angelicae Dahuricae is 2-5mm.
3. the preparation method of a kind of Radix Angelicae Dahuricae breaking cellular wall decoction pieces according to claim 1, it is characterized in that, in step (1), the slice thickness of the fresh and alive Radix Angelicae Dahuricae is 2-4mm.
4. the preparation method of a kind of Radix Angelicae Dahuricae breaking cellular wall decoction pieces according to claim 1, it is characterized in that, the dry run of step (2) comprises metamorphosis stage, constant rate drying period and falling rate drying period.
5. the preparation method of a kind of Radix Angelicae Dahuricae breaking cellular wall decoction pieces according to claim 1, is characterized in that, in step (5) soft material making in, add 50-90 ml deionized water mix homogeneously in every 100g Radix Angelicae Dahuricae micropowder and make.
6. the preparation method of a kind of Radix Angelicae Dahuricae breaking cellular wall decoction pieces according to claim 1, is characterized in that, in step (5) soft material making in, add 60-85 ml deionized water mix homogeneously in every 100g Radix Angelicae Dahuricae micropowder and make.
7. the preparation method of a kind of Radix Angelicae Dahuricae breaking cellular wall decoction pieces according to claim 1, it is characterized in that, step (6) subpackage and packaging process complete in sterilizing room, and the temperature of sterilizing room controls at 16-22 DEG C, and relative humidity is 40-60%.
8. the preparation method of a kind of Radix Angelicae Dahuricae breaking cellular wall decoction pieces according to claim 1, it is characterized in that, step (6) subpackage and packaging process complete in sterilizing room, and the temperature of sterilizing room controls at 16-20 DEG C, and relative humidity is 35-55%.
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| CN201410492327.5A CN104306415B (en) | 2014-09-24 | 2014-09-24 | A kind of preparation method of root of Dahurain angelica broken wall medicine materical crude slice |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105999317A (en) * | 2016-08-08 | 2016-10-12 | 湖南盟合投资管理有限公司 | Crude medicine powder intermittent sterilization method |
| CN106109508A (en) * | 2016-08-08 | 2016-11-16 | 湖南盟合投资管理有限公司 | The preparation method of ganoderma lucidum wall-broken decoction pieces |
| CN110227132A (en) * | 2019-07-04 | 2019-09-13 | 亳州职业技术学院 | A kind of medicine materical crude slice preparation process for promoting stomach to absorb containing the root of Dahurain angelica |
| CN111035664A (en) * | 2019-12-31 | 2020-04-21 | 普洱淞茂滇草六味制药股份有限公司 | Preparation method of radix angelicae wall-broken decoction pieces |
| CN111249335A (en) * | 2019-12-14 | 2020-06-09 | 天马（安徽）国药科技股份有限公司 | Preparation method of radix angelicae and radix salviae miltiorrhizae wall-broken decoction pieces |
| CN116059109A (en) * | 2021-11-01 | 2023-05-05 | 广东美的生活电器制造有限公司 | Chinese medicinal material processing method, cooking equipment, device and storage medium |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105999317A (en) * | 2016-08-08 | 2016-10-12 | 湖南盟合投资管理有限公司 | Crude medicine powder intermittent sterilization method |
| CN106109508A (en) * | 2016-08-08 | 2016-11-16 | 湖南盟合投资管理有限公司 | The preparation method of ganoderma lucidum wall-broken decoction pieces |
| CN110227132A (en) * | 2019-07-04 | 2019-09-13 | 亳州职业技术学院 | A kind of medicine materical crude slice preparation process for promoting stomach to absorb containing the root of Dahurain angelica |
| CN111249335A (en) * | 2019-12-14 | 2020-06-09 | 天马（安徽）国药科技股份有限公司 | Preparation method of radix angelicae and radix salviae miltiorrhizae wall-broken decoction pieces |
| CN111035664A (en) * | 2019-12-31 | 2020-04-21 | 普洱淞茂滇草六味制药股份有限公司 | Preparation method of radix angelicae wall-broken decoction pieces |
| CN116059109A (en) * | 2021-11-01 | 2023-05-05 | 广东美的生活电器制造有限公司 | Chinese medicinal material processing method, cooking equipment, device and storage medium |
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| CN104306415B (en) | 2017-08-22 |
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